Farm Level Milk Adulteration: Changes in the Physicochemical Properties of Raw Cow’s Milk after the Addition of Water and NaCl

Sustainable food security assumes the elimination of food resources adulteration that is already present on farms. This paper is focused on changes in physical and chemical properties of raw cow’s milk treated by the addition of water and NaCl. The main studied factor is the freezing point of milk,...

Full description

Bibliographic Details
Main Authors: Iveta Fehér Pindešová, Alexander Fehér, Piotr Prus, Peter Zajác, Martin Prčík
Format: Article
Language:English
Published: MDPI AG 2022-01-01
Series:Agriculture
Subjects:
Online Access:https://www.mdpi.com/2077-0472/12/2/136
_version_ 1797483868001927168
author Iveta Fehér Pindešová
Alexander Fehér
Piotr Prus
Peter Zajác
Martin Prčík
author_facet Iveta Fehér Pindešová
Alexander Fehér
Piotr Prus
Peter Zajác
Martin Prčík
author_sort Iveta Fehér Pindešová
collection DOAJ
description Sustainable food security assumes the elimination of food resources adulteration that is already present on farms. This paper is focused on changes in physical and chemical properties of raw cow’s milk treated by the addition of water and NaCl. The main studied factor is the freezing point of milk, which is strongly influenced by the chosen treatment. Adulteration of milk by water can be detected by the changed freezing point of the milk, but this can be brought within the range of standardized limits by the addition of NaCl. Determining the concentration of chloride ions in milk by the titration method is a proxy for the added NaCl. The analysis of raw cow’s milk from 17 agricultural farms in Southwest Slovakia revealed a negative correlation between the content of chlorides and the freezing point. In another laboratory experiment, the differences in the milk freezing points were statistically significant in the samples treated with different amounts of NaCl. The relationship of chlorides and the freezing point to other milk components (minerals, lipids, proteins, solids-not-fat, lactose, pH, and milk acidity after Soxhlet–Henkel) were analysed, as well. The results showed that the chosen method of chlorides detection to identify the adulteration of milk, by added water and NaCl, was not effective due to the unstable composition of milk and uncertainty in measurements (the coefficient of determination was very low, <i>R</i><sup>2</sup> = 0.3022).
first_indexed 2024-03-09T22:53:15Z
format Article
id doaj.art-6f5e33ac246a475cbcb3fc9460f168d6
institution Directory Open Access Journal
issn 2077-0472
language English
last_indexed 2024-03-09T22:53:15Z
publishDate 2022-01-01
publisher MDPI AG
record_format Article
series Agriculture
spelling doaj.art-6f5e33ac246a475cbcb3fc9460f168d62023-11-23T18:15:11ZengMDPI AGAgriculture2077-04722022-01-0112213610.3390/agriculture12020136Farm Level Milk Adulteration: Changes in the Physicochemical Properties of Raw Cow’s Milk after the Addition of Water and NaClIveta Fehér Pindešová0Alexander Fehér1Piotr Prus2Peter Zajác3Martin Prčík4State Veterinary and Food Administration in Dolný Kubín, Detached Testing Laboratory, Hlohovecká 5, SK-941 41 Lužianky, SlovakiaFaculty of European Studies and Regional Development, Institute of Environmental Management, The Slovak University of Agriculture in Nitra, Mariánska 10, SK-949 76 Nitra, SlovakiaDepartment of Agronomy, Faculty of Agriculture and Biotechnology, Bydgoszcz University of Science and Technology, Al. Prof. S. Kaliskiego 7, 85-796 Bydgoszcz, PolandFaculty of Biotechnology and Food Sciences, Institute of Food Sciences, The Slovak University of Agriculture in Nitra, Tr. A. Hlinku 2, SK-949 01 Nitra, SlovakiaFaculty of European Studies and Regional Development, Institute of Environmental Management, The Slovak University of Agriculture in Nitra, Mariánska 10, SK-949 76 Nitra, SlovakiaSustainable food security assumes the elimination of food resources adulteration that is already present on farms. This paper is focused on changes in physical and chemical properties of raw cow’s milk treated by the addition of water and NaCl. The main studied factor is the freezing point of milk, which is strongly influenced by the chosen treatment. Adulteration of milk by water can be detected by the changed freezing point of the milk, but this can be brought within the range of standardized limits by the addition of NaCl. Determining the concentration of chloride ions in milk by the titration method is a proxy for the added NaCl. The analysis of raw cow’s milk from 17 agricultural farms in Southwest Slovakia revealed a negative correlation between the content of chlorides and the freezing point. In another laboratory experiment, the differences in the milk freezing points were statistically significant in the samples treated with different amounts of NaCl. The relationship of chlorides and the freezing point to other milk components (minerals, lipids, proteins, solids-not-fat, lactose, pH, and milk acidity after Soxhlet–Henkel) were analysed, as well. The results showed that the chosen method of chlorides detection to identify the adulteration of milk, by added water and NaCl, was not effective due to the unstable composition of milk and uncertainty in measurements (the coefficient of determination was very low, <i>R</i><sup>2</sup> = 0.3022).https://www.mdpi.com/2077-0472/12/2/136sustainable food securitymilk adulterationraw cow’s milkfreezing point of milkmilk qualitysodium chloride
spellingShingle Iveta Fehér Pindešová
Alexander Fehér
Piotr Prus
Peter Zajác
Martin Prčík
Farm Level Milk Adulteration: Changes in the Physicochemical Properties of Raw Cow’s Milk after the Addition of Water and NaCl
Agriculture
sustainable food security
milk adulteration
raw cow’s milk
freezing point of milk
milk quality
sodium chloride
title Farm Level Milk Adulteration: Changes in the Physicochemical Properties of Raw Cow’s Milk after the Addition of Water and NaCl
title_full Farm Level Milk Adulteration: Changes in the Physicochemical Properties of Raw Cow’s Milk after the Addition of Water and NaCl
title_fullStr Farm Level Milk Adulteration: Changes in the Physicochemical Properties of Raw Cow’s Milk after the Addition of Water and NaCl
title_full_unstemmed Farm Level Milk Adulteration: Changes in the Physicochemical Properties of Raw Cow’s Milk after the Addition of Water and NaCl
title_short Farm Level Milk Adulteration: Changes in the Physicochemical Properties of Raw Cow’s Milk after the Addition of Water and NaCl
title_sort farm level milk adulteration changes in the physicochemical properties of raw cow s milk after the addition of water and nacl
topic sustainable food security
milk adulteration
raw cow’s milk
freezing point of milk
milk quality
sodium chloride
url https://www.mdpi.com/2077-0472/12/2/136
work_keys_str_mv AT ivetafeherpindesova farmlevelmilkadulterationchangesinthephysicochemicalpropertiesofrawcowsmilkaftertheadditionofwaterandnacl
AT alexanderfeher farmlevelmilkadulterationchangesinthephysicochemicalpropertiesofrawcowsmilkaftertheadditionofwaterandnacl
AT piotrprus farmlevelmilkadulterationchangesinthephysicochemicalpropertiesofrawcowsmilkaftertheadditionofwaterandnacl
AT peterzajac farmlevelmilkadulterationchangesinthephysicochemicalpropertiesofrawcowsmilkaftertheadditionofwaterandnacl
AT martinprcik farmlevelmilkadulterationchangesinthephysicochemicalpropertiesofrawcowsmilkaftertheadditionofwaterandnacl