CAPILLARY IMBIBITION TECHNIQUES USED TO CHARACTERIZE THESTRUCTURAL CHANGES IN MICROCRYSTALLINE CELLULOSE DUE TO WET AND DRY PROCESS
In this work we study the change on the wettability and solid properties of microcrystalline cellulose (Avicel PH101)after it was wet and dried, through drop penetration experiments in slightly compacted porous beds. We perform these experiments with water and a silicone oil, (Polidimethilsyloxane–P...
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CEILAP-UNIDEF-CONICET-CITEDEF
2024-03-01
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Series: | Anales (Asociación Física Argentina) |
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Online Access: | https://anales.fisica.org.ar/index.php/analesafa/article/view/2410/2948 |
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author | P. D. Ravazzoli M. C. Balbi N. E. Ceschan G. Callegari G. Drazer |
author_facet | P. D. Ravazzoli M. C. Balbi N. E. Ceschan G. Callegari G. Drazer |
author_sort | P. D. Ravazzoli |
collection | DOAJ |
description | In this work we study the change on the wettability and solid properties of microcrystalline cellulose (Avicel PH101)after it was wet and dried, through drop penetration experiments in slightly compacted porous beds. We perform these experiments with water and a silicone oil, (Polidimethilsyloxane–PDMS) and we determine a dimensionless parameter that takes into account all the water penetration factors, including wettability and swelling. We consider three different scenarios, original MCC, and after one and two wetting and drying cycles. For each case we study the particle size effects by considering two subset samples SiA)25<φ<75μm and SiB)75<φ<125μm. We were able to determine, as it was expected, that PDMS penetration dynamics is not affected by the wetting–drying cycles but water is. The penetration rate goes down after cellulose was wet. Finally, we discuss how these behavior may affect the different processes where microcrystalline cellulose is used. |
first_indexed | 2024-04-24T15:44:57Z |
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institution | Directory Open Access Journal |
issn | 1850-1168 |
language | Spanish |
last_indexed | 2024-04-24T15:44:57Z |
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series | Anales (Asociación Física Argentina) |
spelling | doaj.art-6ff18c2c351b4971bfdca1a9fcacb5b42024-04-01T15:59:31ZspaCEILAP-UNIDEF-CONICET-CITEDEFAnales (Asociación Física Argentina)1850-11682024-03-01351101410.31527/analesafa.2024.35.1.10CAPILLARY IMBIBITION TECHNIQUES USED TO CHARACTERIZE THESTRUCTURAL CHANGES IN MICROCRYSTALLINE CELLULOSE DUE TO WET AND DRY PROCESSP. D. Ravazzoli0 M. C. Balbi1 N. E. Ceschan2G. Callegari3 G. Drazer4nstituto de Física Arroyo Seco, Universidad Nacional del Centro de la Provincia de Buenos Aires, andCIFICEN-CONICET-CICPBA, Pinto 399, (7000), Tandil, ArgentinaLaboratorio de Caracterización de Partículas, Facultad de Ingeniería Química, Universidad Nacional del Litoral. Santa Fe (3000),ArgentinaPlanta Piloto de Ingeniería Química (UNS-CONICET); Departamento de Biología, Bioquímica y Farmacia, Universidad Nacionaldel Sur. Bahía Blanca (8000), ArgentinaCenter on Structured Organic Particulate Systems (CSOPs at Rutgers), Department of Mechanical and Aerospace Engineering,Rutgers UniversityDepartment of Mechanical and Aerospace Engineering, Rutgers, The State University of New JerseyIn this work we study the change on the wettability and solid properties of microcrystalline cellulose (Avicel PH101)after it was wet and dried, through drop penetration experiments in slightly compacted porous beds. We perform these experiments with water and a silicone oil, (Polidimethilsyloxane–PDMS) and we determine a dimensionless parameter that takes into account all the water penetration factors, including wettability and swelling. We consider three different scenarios, original MCC, and after one and two wetting and drying cycles. For each case we study the particle size effects by considering two subset samples SiA)25<φ<75μm and SiB)75<φ<125μm. We were able to determine, as it was expected, that PDMS penetration dynamics is not affected by the wetting–drying cycles but water is. The penetration rate goes down after cellulose was wet. Finally, we discuss how these behavior may affect the different processes where microcrystalline cellulose is used.https://anales.fisica.org.ar/index.php/analesafa/article/view/2410/2948microcrystalline celluloseimbibitiondrops |
spellingShingle | P. D. Ravazzoli M. C. Balbi N. E. Ceschan G. Callegari G. Drazer CAPILLARY IMBIBITION TECHNIQUES USED TO CHARACTERIZE THESTRUCTURAL CHANGES IN MICROCRYSTALLINE CELLULOSE DUE TO WET AND DRY PROCESS Anales (Asociación Física Argentina) microcrystalline cellulose imbibition drops |
title | CAPILLARY IMBIBITION TECHNIQUES USED TO CHARACTERIZE THESTRUCTURAL CHANGES IN MICROCRYSTALLINE CELLULOSE DUE TO WET AND DRY PROCESS |
title_full | CAPILLARY IMBIBITION TECHNIQUES USED TO CHARACTERIZE THESTRUCTURAL CHANGES IN MICROCRYSTALLINE CELLULOSE DUE TO WET AND DRY PROCESS |
title_fullStr | CAPILLARY IMBIBITION TECHNIQUES USED TO CHARACTERIZE THESTRUCTURAL CHANGES IN MICROCRYSTALLINE CELLULOSE DUE TO WET AND DRY PROCESS |
title_full_unstemmed | CAPILLARY IMBIBITION TECHNIQUES USED TO CHARACTERIZE THESTRUCTURAL CHANGES IN MICROCRYSTALLINE CELLULOSE DUE TO WET AND DRY PROCESS |
title_short | CAPILLARY IMBIBITION TECHNIQUES USED TO CHARACTERIZE THESTRUCTURAL CHANGES IN MICROCRYSTALLINE CELLULOSE DUE TO WET AND DRY PROCESS |
title_sort | capillary imbibition techniques used to characterize thestructural changes in microcrystalline cellulose due to wet and dry process |
topic | microcrystalline cellulose imbibition drops |
url | https://anales.fisica.org.ar/index.php/analesafa/article/view/2410/2948 |
work_keys_str_mv | AT pdravazzoli capillaryimbibitiontechniquesusedtocharacterizethestructuralchangesinmicrocrystallinecelluloseduetowetanddryprocess AT mcbalbi capillaryimbibitiontechniquesusedtocharacterizethestructuralchangesinmicrocrystallinecelluloseduetowetanddryprocess AT neceschan capillaryimbibitiontechniquesusedtocharacterizethestructuralchangesinmicrocrystallinecelluloseduetowetanddryprocess AT gcallegari capillaryimbibitiontechniquesusedtocharacterizethestructuralchangesinmicrocrystallinecelluloseduetowetanddryprocess AT gdrazer capillaryimbibitiontechniquesusedtocharacterizethestructuralchangesinmicrocrystallinecelluloseduetowetanddryprocess |