CAPILLARY IMBIBITION TECHNIQUES USED TO CHARACTERIZE THESTRUCTURAL CHANGES IN MICROCRYSTALLINE CELLULOSE DUE TO WET AND DRY PROCESS

In this work we study the change on the wettability and solid properties of microcrystalline cellulose (Avicel PH101)after it was wet and dried, through drop penetration experiments in slightly compacted porous beds. We perform these experiments with water and a silicone oil, (Polidimethilsyloxane–P...

Full description

Bibliographic Details
Main Authors: P. D. Ravazzoli, M. C. Balbi, N. E. Ceschan, G. Callegari, G. Drazer
Format: Article
Language:Spanish
Published: CEILAP-UNIDEF-CONICET-CITEDEF 2024-03-01
Series:Anales (Asociación Física Argentina)
Subjects:
Online Access:https://anales.fisica.org.ar/index.php/analesafa/article/view/2410/2948
_version_ 1797231474502533120
author P. D. Ravazzoli
M. C. Balbi
N. E. Ceschan
G. Callegari
G. Drazer
author_facet P. D. Ravazzoli
M. C. Balbi
N. E. Ceschan
G. Callegari
G. Drazer
author_sort P. D. Ravazzoli
collection DOAJ
description In this work we study the change on the wettability and solid properties of microcrystalline cellulose (Avicel PH101)after it was wet and dried, through drop penetration experiments in slightly compacted porous beds. We perform these experiments with water and a silicone oil, (Polidimethilsyloxane–PDMS) and we determine a dimensionless parameter that takes into account all the water penetration factors, including wettability and swelling. We consider three different scenarios, original MCC, and after one and two wetting and drying cycles. For each case we study the particle size effects by considering two subset samples SiA)25<φ<75μm and SiB)75<φ<125μm. We were able to determine, as it was expected, that PDMS penetration dynamics is not affected by the wetting–drying cycles but water is. The penetration rate goes down after cellulose was wet. Finally, we discuss how these behavior may affect the different processes where microcrystalline cellulose is used.
first_indexed 2024-04-24T15:44:57Z
format Article
id doaj.art-6ff18c2c351b4971bfdca1a9fcacb5b4
institution Directory Open Access Journal
issn 1850-1168
language Spanish
last_indexed 2024-04-24T15:44:57Z
publishDate 2024-03-01
publisher CEILAP-UNIDEF-CONICET-CITEDEF
record_format Article
series Anales (Asociación Física Argentina)
spelling doaj.art-6ff18c2c351b4971bfdca1a9fcacb5b42024-04-01T15:59:31ZspaCEILAP-UNIDEF-CONICET-CITEDEFAnales (Asociación Física Argentina)1850-11682024-03-01351101410.31527/analesafa.2024.35.1.10CAPILLARY IMBIBITION TECHNIQUES USED TO CHARACTERIZE THESTRUCTURAL CHANGES IN MICROCRYSTALLINE CELLULOSE DUE TO WET AND DRY PROCESSP. D. Ravazzoli0 M. C. Balbi1 N. E. Ceschan2G. Callegari3 G. Drazer4nstituto de Física Arroyo Seco, Universidad Nacional del Centro de la Provincia de Buenos Aires, andCIFICEN-CONICET-CICPBA, Pinto 399, (7000), Tandil, ArgentinaLaboratorio de Caracterización de Partículas, Facultad de Ingeniería Química, Universidad Nacional del Litoral. Santa Fe (3000),ArgentinaPlanta Piloto de Ingeniería Química (UNS-CONICET); Departamento de Biología, Bioquímica y Farmacia, Universidad Nacionaldel Sur. Bahía Blanca (8000), ArgentinaCenter on Structured Organic Particulate Systems (CSOPs at Rutgers), Department of Mechanical and Aerospace Engineering,Rutgers UniversityDepartment of Mechanical and Aerospace Engineering, Rutgers, The State University of New JerseyIn this work we study the change on the wettability and solid properties of microcrystalline cellulose (Avicel PH101)after it was wet and dried, through drop penetration experiments in slightly compacted porous beds. We perform these experiments with water and a silicone oil, (Polidimethilsyloxane–PDMS) and we determine a dimensionless parameter that takes into account all the water penetration factors, including wettability and swelling. We consider three different scenarios, original MCC, and after one and two wetting and drying cycles. For each case we study the particle size effects by considering two subset samples SiA)25<φ<75μm and SiB)75<φ<125μm. We were able to determine, as it was expected, that PDMS penetration dynamics is not affected by the wetting–drying cycles but water is. The penetration rate goes down after cellulose was wet. Finally, we discuss how these behavior may affect the different processes where microcrystalline cellulose is used.https://anales.fisica.org.ar/index.php/analesafa/article/view/2410/2948microcrystalline celluloseimbibitiondrops
spellingShingle P. D. Ravazzoli
M. C. Balbi
N. E. Ceschan
G. Callegari
G. Drazer
CAPILLARY IMBIBITION TECHNIQUES USED TO CHARACTERIZE THESTRUCTURAL CHANGES IN MICROCRYSTALLINE CELLULOSE DUE TO WET AND DRY PROCESS
Anales (Asociación Física Argentina)
microcrystalline cellulose
imbibition
drops
title CAPILLARY IMBIBITION TECHNIQUES USED TO CHARACTERIZE THESTRUCTURAL CHANGES IN MICROCRYSTALLINE CELLULOSE DUE TO WET AND DRY PROCESS
title_full CAPILLARY IMBIBITION TECHNIQUES USED TO CHARACTERIZE THESTRUCTURAL CHANGES IN MICROCRYSTALLINE CELLULOSE DUE TO WET AND DRY PROCESS
title_fullStr CAPILLARY IMBIBITION TECHNIQUES USED TO CHARACTERIZE THESTRUCTURAL CHANGES IN MICROCRYSTALLINE CELLULOSE DUE TO WET AND DRY PROCESS
title_full_unstemmed CAPILLARY IMBIBITION TECHNIQUES USED TO CHARACTERIZE THESTRUCTURAL CHANGES IN MICROCRYSTALLINE CELLULOSE DUE TO WET AND DRY PROCESS
title_short CAPILLARY IMBIBITION TECHNIQUES USED TO CHARACTERIZE THESTRUCTURAL CHANGES IN MICROCRYSTALLINE CELLULOSE DUE TO WET AND DRY PROCESS
title_sort capillary imbibition techniques used to characterize thestructural changes in microcrystalline cellulose due to wet and dry process
topic microcrystalline cellulose
imbibition
drops
url https://anales.fisica.org.ar/index.php/analesafa/article/view/2410/2948
work_keys_str_mv AT pdravazzoli capillaryimbibitiontechniquesusedtocharacterizethestructuralchangesinmicrocrystallinecelluloseduetowetanddryprocess
AT mcbalbi capillaryimbibitiontechniquesusedtocharacterizethestructuralchangesinmicrocrystallinecelluloseduetowetanddryprocess
AT neceschan capillaryimbibitiontechniquesusedtocharacterizethestructuralchangesinmicrocrystallinecelluloseduetowetanddryprocess
AT gcallegari capillaryimbibitiontechniquesusedtocharacterizethestructuralchangesinmicrocrystallinecelluloseduetowetanddryprocess
AT gdrazer capillaryimbibitiontechniquesusedtocharacterizethestructuralchangesinmicrocrystallinecelluloseduetowetanddryprocess