Synthesis of ex-situ Al5083 reinforced with mechanically-alloyed CNTs and Fe2O3 nanoparticles using friction stir processing

Friction stir processing (FSP) was employed to synthesis ex-situ Al5083 nanocomposite reinforced with different mechanically-alloyed aluminium nanocomposites containing carbon nanotubes (CNTs) and ferric oxide (Fe2O3). The mechanically-alloyed nanocomposite reinforcements were initially prepared usi...

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Main Authors: Farhad Ostovan, Iman Azimifar, Meysam Toozandehjani, Ehsan Shafiei, Mahnaz Shamshirsaz
Format: Article
Language:English
Published: Elsevier 2021-09-01
Series:Journal of Materials Research and Technology
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2238785421007353
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author Farhad Ostovan
Iman Azimifar
Meysam Toozandehjani
Ehsan Shafiei
Mahnaz Shamshirsaz
author_facet Farhad Ostovan
Iman Azimifar
Meysam Toozandehjani
Ehsan Shafiei
Mahnaz Shamshirsaz
author_sort Farhad Ostovan
collection DOAJ
description Friction stir processing (FSP) was employed to synthesis ex-situ Al5083 nanocomposite reinforced with different mechanically-alloyed aluminium nanocomposites containing carbon nanotubes (CNTs) and ferric oxide (Fe2O3). The mechanically-alloyed nanocomposite reinforcements were initially prepared using ball milling and introduced into the stir zone (SZ) of rolled Al5083 alloy during subsequent FSP. The FSPed nanocomposites were successfully processed with uniform dispersion of CNTs and Fe2O3 nanoparticles resulting in the achievement of unique properties. Addition of nanocomposite reinforcements significantly reduces the grain size of FSPed nanocomposites. The least grain size belongs to hybrid FSP5 (Al/CNTs/Fe2O3) nanocomposite with grain size of 6.9 ± 0.4 μm which is 7.4 and 2.6 times smaller than base metal (BM) and un-reinforced FSPed (FSP1). Microstructure of FSP5 nanocomposite contain largest fraction of high angle grain boundaries (HAGBs) of 87 %. Among all FSPed nanocomposites, hybrid FSP5 nanocomposite has the best mechanical properties in the terms of microhardness, Yield strength, ultimate tensile strength and wear resistance; with 1.6, 2.7, 3.5, 3.1 times, respectively, superior to BM. The significant improvement is attributed to the desirable microstructural changes including well dispersion of nanoparticles and extensive grain refinement. Hybrid FSP5 has an excellent magnetic and electrical resistivity when compared with the BM, however, its magnetic properties is slightly slower than FSP4 specimen due to de-magnetization effect of CNTs.
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spelling doaj.art-7082b445f57c458cb5ec4eeb526e91612022-12-21T18:32:08ZengElsevierJournal of Materials Research and Technology2238-78542021-09-011416701681Synthesis of ex-situ Al5083 reinforced with mechanically-alloyed CNTs and Fe2O3 nanoparticles using friction stir processingFarhad Ostovan0Iman Azimifar1Meysam Toozandehjani2Ehsan Shafiei3Mahnaz Shamshirsaz4Department of Material Science and Engineering, Bandar Abbas Branch, Islamic Azad University, Bandar Abbas, Iran; Corresponding author.Department of Material Science and Engineering, Bandar Abbas Branch, Islamic Azad University, Bandar Abbas, IranNew Technologies Research Center, Amirkabir University of Technology, Tehran Polytechnic, 424 Hafez Ave., P.B. 15875-4413, Tehran, IranDepartment of Material Science and Engineering, Bandar Abbas Branch, Islamic Azad University, Bandar Abbas, IranNew Technologies Research Center, Amirkabir University of Technology, Tehran Polytechnic, 424 Hafez Ave., P.B. 15875-4413, Tehran, IranFriction stir processing (FSP) was employed to synthesis ex-situ Al5083 nanocomposite reinforced with different mechanically-alloyed aluminium nanocomposites containing carbon nanotubes (CNTs) and ferric oxide (Fe2O3). The mechanically-alloyed nanocomposite reinforcements were initially prepared using ball milling and introduced into the stir zone (SZ) of rolled Al5083 alloy during subsequent FSP. The FSPed nanocomposites were successfully processed with uniform dispersion of CNTs and Fe2O3 nanoparticles resulting in the achievement of unique properties. Addition of nanocomposite reinforcements significantly reduces the grain size of FSPed nanocomposites. The least grain size belongs to hybrid FSP5 (Al/CNTs/Fe2O3) nanocomposite with grain size of 6.9 ± 0.4 μm which is 7.4 and 2.6 times smaller than base metal (BM) and un-reinforced FSPed (FSP1). Microstructure of FSP5 nanocomposite contain largest fraction of high angle grain boundaries (HAGBs) of 87 %. Among all FSPed nanocomposites, hybrid FSP5 nanocomposite has the best mechanical properties in the terms of microhardness, Yield strength, ultimate tensile strength and wear resistance; with 1.6, 2.7, 3.5, 3.1 times, respectively, superior to BM. The significant improvement is attributed to the desirable microstructural changes including well dispersion of nanoparticles and extensive grain refinement. Hybrid FSP5 has an excellent magnetic and electrical resistivity when compared with the BM, however, its magnetic properties is slightly slower than FSP4 specimen due to de-magnetization effect of CNTs.http://www.sciencedirect.com/science/article/pii/S2238785421007353Aluminum-matrix surface composites (AMSCs)Friction stir processing (FSP)Ball millingAlumina (Al2O3) carbon nanotubes (CNTs)Grain size
spellingShingle Farhad Ostovan
Iman Azimifar
Meysam Toozandehjani
Ehsan Shafiei
Mahnaz Shamshirsaz
Synthesis of ex-situ Al5083 reinforced with mechanically-alloyed CNTs and Fe2O3 nanoparticles using friction stir processing
Journal of Materials Research and Technology
Aluminum-matrix surface composites (AMSCs)
Friction stir processing (FSP)
Ball milling
Alumina (Al2O3) carbon nanotubes (CNTs)
Grain size
title Synthesis of ex-situ Al5083 reinforced with mechanically-alloyed CNTs and Fe2O3 nanoparticles using friction stir processing
title_full Synthesis of ex-situ Al5083 reinforced with mechanically-alloyed CNTs and Fe2O3 nanoparticles using friction stir processing
title_fullStr Synthesis of ex-situ Al5083 reinforced with mechanically-alloyed CNTs and Fe2O3 nanoparticles using friction stir processing
title_full_unstemmed Synthesis of ex-situ Al5083 reinforced with mechanically-alloyed CNTs and Fe2O3 nanoparticles using friction stir processing
title_short Synthesis of ex-situ Al5083 reinforced with mechanically-alloyed CNTs and Fe2O3 nanoparticles using friction stir processing
title_sort synthesis of ex situ al5083 reinforced with mechanically alloyed cnts and fe2o3 nanoparticles using friction stir processing
topic Aluminum-matrix surface composites (AMSCs)
Friction stir processing (FSP)
Ball milling
Alumina (Al2O3) carbon nanotubes (CNTs)
Grain size
url http://www.sciencedirect.com/science/article/pii/S2238785421007353
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