Validation of Pesticides Multi-Residual Testing Method on Nutmeg by Using UPLC-MS/MS
The use of pesticides in nutmeg still leaves an accumulation of pesticide residues that can endanger human health and damage the ecological balance. In addition, nutmeg with high pesticide residue content will be rejected by nutmeg export destination countries. This research was conducted to validat...
| Main Author: | |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
Department of Chemistry, Faculty of Science and Technology, Universitas Islam Negeri Walisongo Semarang
2021-12-01
|
| Series: | Walisongo Journal of Chemistry |
| Subjects: | |
| Online Access: | https://journal.walisongo.ac.id/index.php/wjc/article/view/8698 |
| _version_ | 1818481695700025344 |
|---|---|
| author | Bayu Refindra Fitriadi |
| author_facet | Bayu Refindra Fitriadi |
| author_sort | Bayu Refindra Fitriadi |
| collection | DOAJ |
| description | The use of pesticides in nutmeg still leaves an accumulation of pesticide residues that can endanger human health and damage the ecological balance. In addition, nutmeg with high pesticide residue content will be rejected by nutmeg export destination countries. This research was conducted to validate the method of testing pesticide residues of carbaryl, carbofuran, acetate, and dimethoate on nutmeg. This pesticide residue test uses the QuEChERS (Quick, Easy, Cheap, Effective, Rugged, and Safe) optimization method and is analyzed using UPLC-MS/MS (Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry). This method meets the validation requirements according to SANTE/12682/2019. The limit of quantification (LOQ) of the analyte is below the Maximum Residue Limit (MRL) set by the European Union through Regulation (EC) No. 396/2005. |
| first_indexed | 2024-12-10T11:38:30Z |
| format | Article |
| id | doaj.art-709133f4557a4283a2390693480f3fbd |
| institution | Directory Open Access Journal |
| issn | 2549-385X 2621-5985 |
| language | English |
| last_indexed | 2024-12-10T11:38:30Z |
| publishDate | 2021-12-01 |
| publisher | Department of Chemistry, Faculty of Science and Technology, Universitas Islam Negeri Walisongo Semarang |
| record_format | Article |
| series | Walisongo Journal of Chemistry |
| spelling | doaj.art-709133f4557a4283a2390693480f3fbd2022-12-22T01:50:21ZengDepartment of Chemistry, Faculty of Science and Technology, Universitas Islam Negeri Walisongo SemarangWalisongo Journal of Chemistry2549-385X2621-59852021-12-014211913010.21580/wjc.v4i2.86983354Validation of Pesticides Multi-Residual Testing Method on Nutmeg by Using UPLC-MS/MSBayu Refindra Fitriadi0Balai Besar Perbenihan dan Proteksi Tanaman Perkebunan SurabayaThe use of pesticides in nutmeg still leaves an accumulation of pesticide residues that can endanger human health and damage the ecological balance. In addition, nutmeg with high pesticide residue content will be rejected by nutmeg export destination countries. This research was conducted to validate the method of testing pesticide residues of carbaryl, carbofuran, acetate, and dimethoate on nutmeg. This pesticide residue test uses the QuEChERS (Quick, Easy, Cheap, Effective, Rugged, and Safe) optimization method and is analyzed using UPLC-MS/MS (Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry). This method meets the validation requirements according to SANTE/12682/2019. The limit of quantification (LOQ) of the analyte is below the Maximum Residue Limit (MRL) set by the European Union through Regulation (EC) No. 396/2005.https://journal.walisongo.ac.id/index.php/wjc/article/view/8698pesticide residueuplc-ms/msnutmegquechers |
| spellingShingle | Bayu Refindra Fitriadi Validation of Pesticides Multi-Residual Testing Method on Nutmeg by Using UPLC-MS/MS Walisongo Journal of Chemistry pesticide residue uplc-ms/ms nutmeg quechers |
| title | Validation of Pesticides Multi-Residual Testing Method on Nutmeg by Using UPLC-MS/MS |
| title_full | Validation of Pesticides Multi-Residual Testing Method on Nutmeg by Using UPLC-MS/MS |
| title_fullStr | Validation of Pesticides Multi-Residual Testing Method on Nutmeg by Using UPLC-MS/MS |
| title_full_unstemmed | Validation of Pesticides Multi-Residual Testing Method on Nutmeg by Using UPLC-MS/MS |
| title_short | Validation of Pesticides Multi-Residual Testing Method on Nutmeg by Using UPLC-MS/MS |
| title_sort | validation of pesticides multi residual testing method on nutmeg by using uplc ms ms |
| topic | pesticide residue uplc-ms/ms nutmeg quechers |
| url | https://journal.walisongo.ac.id/index.php/wjc/article/view/8698 |
| work_keys_str_mv | AT bayurefindrafitriadi validationofpesticidesmultiresidualtestingmethodonnutmegbyusinguplcmsms |