100 kHz MAS Proton-Detected NMR Spectroscopy of Hepatitis B Virus Capsids

100 kHz MAS Proton-Detected NMR Spectroscopy of Hepatitis B Virus Capsids

We sequentially assigned the fully-protonated capsids made from core proteins of the Hepatitis B virus using proton detection at 100 kHz magic-angle spinning (MAS) in 0.7 mm rotors and compare sensitivity and assignment completeness to previously obtained assignments using carbon-detection technique...

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Bibliographic Details
Main Authors: Lauriane Lecoq, Maarten Schledorn, Shishan Wang, Susanne Smith-Penzel, Alexander A. Malär, Morgane Callon, Michael Nassal, Beat H. Meier, Anja Böckmann
Format: Article
Language:English
Published: Frontiers Media S.A. 2019-07-01
Series:Frontiers in Molecular Biosciences
Subjects:
solid-state NMR
fast MAS
proton detection
carbon detection
deuteration
hepatitis B virus
Online Access:https://www.frontiersin.org/article/10.3389/fmolb.2019.00058/full

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