Change in Micro-Morphology and Micro-Mechanical Properties of Thermally Modified Moso Bamboo

In recent years, saturated steam heat treatment has been considered as an environmentally friendly and cost-effective modification method compared with traditional heat treatment media. In this study, bamboo was treated by saturated steam, and the change in chemical composition, cellulose crystallin...

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Main Authors: Tiancheng Yuan, Yaqian Huang, Tao Zhang, Xinzhou Wang, Yanjun Li
Format: Article
Language:English
Published: MDPI AG 2022-02-01
Series:Polymers
Subjects:
Online Access:https://www.mdpi.com/2073-4360/14/3/646
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author Tiancheng Yuan
Yaqian Huang
Tao Zhang
Xinzhou Wang
Yanjun Li
author_facet Tiancheng Yuan
Yaqian Huang
Tao Zhang
Xinzhou Wang
Yanjun Li
author_sort Tiancheng Yuan
collection DOAJ
description In recent years, saturated steam heat treatment has been considered as an environmentally friendly and cost-effective modification method compared with traditional heat treatment media. In this study, bamboo was treated by saturated steam, and the change in chemical composition, cellulose crystallinity index, micro-morphology, and micromechanical properties were analyzed by a wet chemistry method, Fourier transform infrared (FTIR), scanning electron microscopy (SEM), X-ray diffraction (XRD), nanoindentation, and so on. Results illustrated that the parenchyma cell walls were distorted due to the decomposition of hemicellulose and cellulose in bamboo samples. As expected, the hemicellulose and cellulose content decreased, whereas the lignin content increased significantly. In addition, the cellulose crystallinity index and thus the micromechanical properties of bamboo cell walls increased. For example, the hardness increased from 0.69 GPa to 0.84 GPa owing to the enhanced crystallinity index and lignin content.
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spelling doaj.art-71d26766e76d437da86bfa2fda888f742023-11-23T17:37:27ZengMDPI AGPolymers2073-43602022-02-0114364610.3390/polym14030646Change in Micro-Morphology and Micro-Mechanical Properties of Thermally Modified Moso BambooTiancheng Yuan0Yaqian Huang1Tao Zhang2Xinzhou Wang3Yanjun Li4Jiangsu Co-Innovation Center of Efficient Processing and Utilization of Forest Resources, Nanjing Forestry University, Nanjing 210037, ChinaJiangsu Co-Innovation Center of Efficient Processing and Utilization of Forest Resources, Nanjing Forestry University, Nanjing 210037, ChinaJiangsu Co-Innovation Center of Efficient Processing and Utilization of Forest Resources, Nanjing Forestry University, Nanjing 210037, ChinaJiangsu Co-Innovation Center of Efficient Processing and Utilization of Forest Resources, Nanjing Forestry University, Nanjing 210037, ChinaJiangsu Co-Innovation Center of Efficient Processing and Utilization of Forest Resources, Nanjing Forestry University, Nanjing 210037, ChinaIn recent years, saturated steam heat treatment has been considered as an environmentally friendly and cost-effective modification method compared with traditional heat treatment media. In this study, bamboo was treated by saturated steam, and the change in chemical composition, cellulose crystallinity index, micro-morphology, and micromechanical properties were analyzed by a wet chemistry method, Fourier transform infrared (FTIR), scanning electron microscopy (SEM), X-ray diffraction (XRD), nanoindentation, and so on. Results illustrated that the parenchyma cell walls were distorted due to the decomposition of hemicellulose and cellulose in bamboo samples. As expected, the hemicellulose and cellulose content decreased, whereas the lignin content increased significantly. In addition, the cellulose crystallinity index and thus the micromechanical properties of bamboo cell walls increased. For example, the hardness increased from 0.69 GPa to 0.84 GPa owing to the enhanced crystallinity index and lignin content.https://www.mdpi.com/2073-4360/14/3/646bamboosaturated steamnanoindentationmicro-mechanical properties
spellingShingle Tiancheng Yuan
Yaqian Huang
Tao Zhang
Xinzhou Wang
Yanjun Li
Change in Micro-Morphology and Micro-Mechanical Properties of Thermally Modified Moso Bamboo
Polymers
bamboo
saturated steam
nanoindentation
micro-mechanical properties
title Change in Micro-Morphology and Micro-Mechanical Properties of Thermally Modified Moso Bamboo
title_full Change in Micro-Morphology and Micro-Mechanical Properties of Thermally Modified Moso Bamboo
title_fullStr Change in Micro-Morphology and Micro-Mechanical Properties of Thermally Modified Moso Bamboo
title_full_unstemmed Change in Micro-Morphology and Micro-Mechanical Properties of Thermally Modified Moso Bamboo
title_short Change in Micro-Morphology and Micro-Mechanical Properties of Thermally Modified Moso Bamboo
title_sort change in micro morphology and micro mechanical properties of thermally modified moso bamboo
topic bamboo
saturated steam
nanoindentation
micro-mechanical properties
url https://www.mdpi.com/2073-4360/14/3/646
work_keys_str_mv AT tianchengyuan changeinmicromorphologyandmicromechanicalpropertiesofthermallymodifiedmosobamboo
AT yaqianhuang changeinmicromorphologyandmicromechanicalpropertiesofthermallymodifiedmosobamboo
AT taozhang changeinmicromorphologyandmicromechanicalpropertiesofthermallymodifiedmosobamboo
AT xinzhouwang changeinmicromorphologyandmicromechanicalpropertiesofthermallymodifiedmosobamboo
AT yanjunli changeinmicromorphologyandmicromechanicalpropertiesofthermallymodifiedmosobamboo