Extraction optimization of soluble compounds of yerba maté

The objective of this research was the extraction optimization of water soluble compounds of yerba maté. Measures variables were extract concentration and weight of leaves and twigs. Controlled variables were time and temperature of extraction and water/solid relation. A surface response method of t...

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Main Authors: César Sambiassi, Andrea M. Escalada, Miguel E. Schmalko
Format: Article
Language:English
Published: Instituto de Tecnologia do Paraná (Tecpar) 2002-06-01
Series:Brazilian Archives of Biology and Technology
Subjects:
Online Access:http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-89132002000200010
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author César Sambiassi
Andrea M. Escalada
Miguel E. Schmalko
author_facet César Sambiassi
Andrea M. Escalada
Miguel E. Schmalko
author_sort César Sambiassi
collection DOAJ
description The objective of this research was the extraction optimization of water soluble compounds of yerba maté. Measures variables were extract concentration and weight of leaves and twigs. Controlled variables were time and temperature of extraction and water/solid relation. A surface response method of three variables was used as experimental design, with 20 experiences in each case. The range of each variable, defined in the experimental design, was: extraction time, 13.2 to 46.8 minutes; temperature, 48.2 to 81.8°C and water solid relation, 4.64 to 11.36 g water/100 g of dry solid. Extract weight varied from 13.14 to 29.56 g in leaves and 8.98 to 16.32 g in twigs (each one per 100 g of dry solid). Extract concentration varied between 2.17 and 3.43 g/100 ml in leaves and between 1.32 and 2.31 g/100 ml in twigs. The results were fit to a linear equation in each case.<br>O objetivo desta pesquisa foi a otimização da extração aquosa da erva mate. As variáveis medidas foram a concentração do extrato e a massa das folhas e ramos. As variáveis controladas foram: o tempo e a temperatura de extração e a relação água/sólido. Como desenho experimental foi utilizado o método de resposta superficial de três variáveis, com vinte experiências em cada caso. A faixa de variação definida para as variáveis no desenho experimental foram: tempo de extração, de 13,2 a 46,8 minutos; temperatura, de 48,2 a 81,8 °C; relação água/sólido, de 4,64 a 11,36 gramas de água por gramas de sólido seco. A massa do extrato variou de 13,14 a 29,56 gramas para as folhas desramificadas e de 8,98 a 16,32 para os ramos (cada por 100 gramas de sólido seco). A concentração de extrato variou entre 2,17 a 3,43 g/ 100 ml nas folhas e entre 1,32 e 2,31 g/ 100 ml nos ramos. Os resultados foram, em ambos casos, ajustados para uma equação linear.
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spelling doaj.art-7260b8be784c41c9b1cb2c748ecf1fa02022-12-22T03:51:29ZengInstituto de Tecnologia do Paraná (Tecpar)Brazilian Archives of Biology and Technology1516-89131678-43242002-06-0145218919310.1590/S1516-89132002000200010Extraction optimization of soluble compounds of yerba matéCésar SambiassiAndrea M. EscaladaMiguel E. SchmalkoThe objective of this research was the extraction optimization of water soluble compounds of yerba maté. Measures variables were extract concentration and weight of leaves and twigs. Controlled variables were time and temperature of extraction and water/solid relation. A surface response method of three variables was used as experimental design, with 20 experiences in each case. The range of each variable, defined in the experimental design, was: extraction time, 13.2 to 46.8 minutes; temperature, 48.2 to 81.8°C and water solid relation, 4.64 to 11.36 g water/100 g of dry solid. Extract weight varied from 13.14 to 29.56 g in leaves and 8.98 to 16.32 g in twigs (each one per 100 g of dry solid). Extract concentration varied between 2.17 and 3.43 g/100 ml in leaves and between 1.32 and 2.31 g/100 ml in twigs. The results were fit to a linear equation in each case.<br>O objetivo desta pesquisa foi a otimização da extração aquosa da erva mate. As variáveis medidas foram a concentração do extrato e a massa das folhas e ramos. As variáveis controladas foram: o tempo e a temperatura de extração e a relação água/sólido. Como desenho experimental foi utilizado o método de resposta superficial de três variáveis, com vinte experiências em cada caso. A faixa de variação definida para as variáveis no desenho experimental foram: tempo de extração, de 13,2 a 46,8 minutos; temperatura, de 48,2 a 81,8 °C; relação água/sólido, de 4,64 a 11,36 gramas de água por gramas de sólido seco. A massa do extrato variou de 13,14 a 29,56 gramas para as folhas desramificadas e de 8,98 a 16,32 para os ramos (cada por 100 gramas de sólido seco). A concentração de extrato variou entre 2,17 a 3,43 g/ 100 ml nas folhas e entre 1,32 e 2,31 g/ 100 ml nos ramos. Os resultados foram, em ambos casos, ajustados para uma equação linear.http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-89132002000200010Yerba matésoluble compoundsoptimization
spellingShingle César Sambiassi
Andrea M. Escalada
Miguel E. Schmalko
Extraction optimization of soluble compounds of yerba maté
Brazilian Archives of Biology and Technology
Yerba maté
soluble compounds
optimization
title Extraction optimization of soluble compounds of yerba maté
title_full Extraction optimization of soluble compounds of yerba maté
title_fullStr Extraction optimization of soluble compounds of yerba maté
title_full_unstemmed Extraction optimization of soluble compounds of yerba maté
title_short Extraction optimization of soluble compounds of yerba maté
title_sort extraction optimization of soluble compounds of yerba mate
topic Yerba maté
soluble compounds
optimization
url http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-89132002000200010
work_keys_str_mv AT cesarsambiassi extractionoptimizationofsolublecompoundsofyerbamate
AT andreamescalada extractionoptimizationofsolublecompoundsofyerbamate
AT migueleschmalko extractionoptimizationofsolublecompoundsofyerbamate