Optimising dynamic mechanical analysis experiments on soft rubbers for use in time temperature superposition

Rubbers are ubiquitous in engineering applications where they are often subjected to loading leading to high strain rate deformation. The strong rate and temperature dependence of rubbers and their composites motivates research into understanding their mechanical response under a wide range of condi...

Disgrifiad llawn

Manylion Llyfryddiaeth
Prif Awduron: Akash R. Trivedi, Nicholas Hawkins, Clive R. Siviour
Fformat: Erthygl
Iaith:English
Cyhoeddwyd: Elsevier 2022-01-01
Cyfres:MethodsX
Pynciau:
Mynediad Ar-lein:http://www.sciencedirect.com/science/article/pii/S2215016122002114
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author Akash R. Trivedi
Nicholas Hawkins
Clive R. Siviour
author_facet Akash R. Trivedi
Nicholas Hawkins
Clive R. Siviour
author_sort Akash R. Trivedi
collection DOAJ
description Rubbers are ubiquitous in engineering applications where they are often subjected to loading leading to high strain rate deformation. The strong rate and temperature dependence of rubbers and their composites motivates research into understanding their mechanical response under a wide range of conditions. However, experimental characterisation of the rate-temperature dependence of soft rubbers is challenging. In this methods paper, an improved methodology is proposed for conducting Dynamic Mechanical Analysis (DMA) experiments on rubbers. The higher quality data produced can be used in time-temperature superposition (TTS) applications to derive a more accurate definition of the rubber’s rate-temperature dependence. Overall, the improvements obtained can be summarised as follows: • Reducing clamping artefacts due to volume expansion • Ensuring high quality temperature stability • Improving the contact area between the specimen and the clamps
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spelling doaj.art-7265e901b128473fa93cccc1ab5e44d82022-12-22T03:52:10ZengElsevierMethodsX2215-01612022-01-019101831Optimising dynamic mechanical analysis experiments on soft rubbers for use in time temperature superpositionAkash R. Trivedi0Nicholas Hawkins1Clive R. Siviour2Corresponding author.; Department of Engineering Science, University of Oxford, Parks Road, OX1 3PJ, UKDepartment of Engineering Science, University of Oxford, Parks Road, OX1 3PJ, UKDepartment of Engineering Science, University of Oxford, Parks Road, OX1 3PJ, UKRubbers are ubiquitous in engineering applications where they are often subjected to loading leading to high strain rate deformation. The strong rate and temperature dependence of rubbers and their composites motivates research into understanding their mechanical response under a wide range of conditions. However, experimental characterisation of the rate-temperature dependence of soft rubbers is challenging. In this methods paper, an improved methodology is proposed for conducting Dynamic Mechanical Analysis (DMA) experiments on rubbers. The higher quality data produced can be used in time-temperature superposition (TTS) applications to derive a more accurate definition of the rubber’s rate-temperature dependence. Overall, the improvements obtained can be summarised as follows: • Reducing clamping artefacts due to volume expansion • Ensuring high quality temperature stability • Improving the contact area between the specimen and the clampshttp://www.sciencedirect.com/science/article/pii/S2215016122002114ViscoelasticityHigh strain rateThermomechanical characterisationRate and temperature dependence
spellingShingle Akash R. Trivedi
Nicholas Hawkins
Clive R. Siviour
Optimising dynamic mechanical analysis experiments on soft rubbers for use in time temperature superposition
MethodsX
Viscoelasticity
High strain rate
Thermomechanical characterisation
Rate and temperature dependence
title Optimising dynamic mechanical analysis experiments on soft rubbers for use in time temperature superposition
title_full Optimising dynamic mechanical analysis experiments on soft rubbers for use in time temperature superposition
title_fullStr Optimising dynamic mechanical analysis experiments on soft rubbers for use in time temperature superposition
title_full_unstemmed Optimising dynamic mechanical analysis experiments on soft rubbers for use in time temperature superposition
title_short Optimising dynamic mechanical analysis experiments on soft rubbers for use in time temperature superposition
title_sort optimising dynamic mechanical analysis experiments on soft rubbers for use in time temperature superposition
topic Viscoelasticity
High strain rate
Thermomechanical characterisation
Rate and temperature dependence
url http://www.sciencedirect.com/science/article/pii/S2215016122002114
work_keys_str_mv AT akashrtrivedi optimisingdynamicmechanicalanalysisexperimentsonsoftrubbersforuseintimetemperaturesuperposition
AT nicholashawkins optimisingdynamicmechanicalanalysisexperimentsonsoftrubbersforuseintimetemperaturesuperposition
AT cliversiviour optimisingdynamicmechanicalanalysisexperimentsonsoftrubbersforuseintimetemperaturesuperposition