Optimising dynamic mechanical analysis experiments on soft rubbers for use in time temperature superposition
Rubbers are ubiquitous in engineering applications where they are often subjected to loading leading to high strain rate deformation. The strong rate and temperature dependence of rubbers and their composites motivates research into understanding their mechanical response under a wide range of condi...
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Fformat: | Erthygl |
Iaith: | English |
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Elsevier
2022-01-01
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Cyfres: | MethodsX |
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Mynediad Ar-lein: | http://www.sciencedirect.com/science/article/pii/S2215016122002114 |
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author | Akash R. Trivedi Nicholas Hawkins Clive R. Siviour |
author_facet | Akash R. Trivedi Nicholas Hawkins Clive R. Siviour |
author_sort | Akash R. Trivedi |
collection | DOAJ |
description | Rubbers are ubiquitous in engineering applications where they are often subjected to loading leading to high strain rate deformation. The strong rate and temperature dependence of rubbers and their composites motivates research into understanding their mechanical response under a wide range of conditions. However, experimental characterisation of the rate-temperature dependence of soft rubbers is challenging. In this methods paper, an improved methodology is proposed for conducting Dynamic Mechanical Analysis (DMA) experiments on rubbers. The higher quality data produced can be used in time-temperature superposition (TTS) applications to derive a more accurate definition of the rubber’s rate-temperature dependence. Overall, the improvements obtained can be summarised as follows: • Reducing clamping artefacts due to volume expansion • Ensuring high quality temperature stability • Improving the contact area between the specimen and the clamps |
first_indexed | 2024-04-12T02:18:58Z |
format | Article |
id | doaj.art-7265e901b128473fa93cccc1ab5e44d8 |
institution | Directory Open Access Journal |
issn | 2215-0161 |
language | English |
last_indexed | 2024-04-12T02:18:58Z |
publishDate | 2022-01-01 |
publisher | Elsevier |
record_format | Article |
series | MethodsX |
spelling | doaj.art-7265e901b128473fa93cccc1ab5e44d82022-12-22T03:52:10ZengElsevierMethodsX2215-01612022-01-019101831Optimising dynamic mechanical analysis experiments on soft rubbers for use in time temperature superpositionAkash R. Trivedi0Nicholas Hawkins1Clive R. Siviour2Corresponding author.; Department of Engineering Science, University of Oxford, Parks Road, OX1 3PJ, UKDepartment of Engineering Science, University of Oxford, Parks Road, OX1 3PJ, UKDepartment of Engineering Science, University of Oxford, Parks Road, OX1 3PJ, UKRubbers are ubiquitous in engineering applications where they are often subjected to loading leading to high strain rate deformation. The strong rate and temperature dependence of rubbers and their composites motivates research into understanding their mechanical response under a wide range of conditions. However, experimental characterisation of the rate-temperature dependence of soft rubbers is challenging. In this methods paper, an improved methodology is proposed for conducting Dynamic Mechanical Analysis (DMA) experiments on rubbers. The higher quality data produced can be used in time-temperature superposition (TTS) applications to derive a more accurate definition of the rubber’s rate-temperature dependence. Overall, the improvements obtained can be summarised as follows: • Reducing clamping artefacts due to volume expansion • Ensuring high quality temperature stability • Improving the contact area between the specimen and the clampshttp://www.sciencedirect.com/science/article/pii/S2215016122002114ViscoelasticityHigh strain rateThermomechanical characterisationRate and temperature dependence |
spellingShingle | Akash R. Trivedi Nicholas Hawkins Clive R. Siviour Optimising dynamic mechanical analysis experiments on soft rubbers for use in time temperature superposition MethodsX Viscoelasticity High strain rate Thermomechanical characterisation Rate and temperature dependence |
title | Optimising dynamic mechanical analysis experiments on soft rubbers for use in time temperature superposition |
title_full | Optimising dynamic mechanical analysis experiments on soft rubbers for use in time temperature superposition |
title_fullStr | Optimising dynamic mechanical analysis experiments on soft rubbers for use in time temperature superposition |
title_full_unstemmed | Optimising dynamic mechanical analysis experiments on soft rubbers for use in time temperature superposition |
title_short | Optimising dynamic mechanical analysis experiments on soft rubbers for use in time temperature superposition |
title_sort | optimising dynamic mechanical analysis experiments on soft rubbers for use in time temperature superposition |
topic | Viscoelasticity High strain rate Thermomechanical characterisation Rate and temperature dependence |
url | http://www.sciencedirect.com/science/article/pii/S2215016122002114 |
work_keys_str_mv | AT akashrtrivedi optimisingdynamicmechanicalanalysisexperimentsonsoftrubbersforuseintimetemperaturesuperposition AT nicholashawkins optimisingdynamicmechanicalanalysisexperimentsonsoftrubbersforuseintimetemperaturesuperposition AT cliversiviour optimisingdynamicmechanicalanalysisexperimentsonsoftrubbersforuseintimetemperaturesuperposition |