Effect Of Severe Plastic Deformation On Microstructure Evolution Of Pure Aluminium

Processes of severe plastic deformation (SPD) are defined as a group of metalworking techniques in which a very large plastic strain is imposed on a bulk material in order to make an ultra-fine grained metal. The present study attempts to apply Equal-Channel Angular Pressing (ECAP), Hydrostatic Extr...

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Main Authors: Leszczyńska-Madej B., Richert M.W., Perek-Nowak M.
Format: Article
Language:English
Published: Polish Academy of Sciences 2015-06-01
Series:Archives of Metallurgy and Materials
Subjects:
Online Access:http://www.degruyter.com/view/j/amm.2015.60.issue-2/amm-2015-0148/amm-2015-0148.xml?format=INT
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author Leszczyńska-Madej B.
Richert M.W.
Perek-Nowak M.
author_facet Leszczyńska-Madej B.
Richert M.W.
Perek-Nowak M.
author_sort Leszczyńska-Madej B.
collection DOAJ
description Processes of severe plastic deformation (SPD) are defined as a group of metalworking techniques in which a very large plastic strain is imposed on a bulk material in order to make an ultra-fine grained metal. The present study attempts to apply Equal-Channel Angular Pressing (ECAP), Hydrostatic Extrusion (HE) and combination of ECAP and HE to 99.5% pure aluminium. ECAP process was realized at room temperature for 16 passes through route Bc using a die having an angle of 90°. Hydrostatic extrusion process was performed with cumulative strain of 2.68 to attain finally wire diameter of d = 3 mm. The microstructure of the samples was investigated by means of transmission and scanning electron microscopy. Additionally, the microhardness was measured and statistical analysis of the grains and subgrains was performed. Based on Kikuchi diffraction patterns misorientation was determined. The measured grain/subgrain size show, that regardless the mode of deformation process (ECAP, HE or combination of ECAP and HE processes), grain size is maintained at a similar level – equal to d = 0.55-0.59 μm. A combination of ECAP and HE has achieved better properties than either single process and show to be a promising procedure for manufacturing bulk UFG aluminium.
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spelling doaj.art-726c3f436c2d49d48d7f6193b70fe2e82022-12-22T01:26:15ZengPolish Academy of SciencesArchives of Metallurgy and Materials2300-19092015-06-016021437144010.1515/amm-2015-0148amm-2015-0148Effect Of Severe Plastic Deformation On Microstructure Evolution Of Pure AluminiumLeszczyńska-Madej B.0Richert M.W.1Perek-Nowak M.2 AGH UNIVERSITY OF SCIENCE AND TECHNOLOGY, FACULTY OF NON FERROUS METALS, DEPARTMENT OF MATERIALS SCIENCE AND NON – FERROUS METALS ENGINEERING, AL. A. MICKIEWICZA 30, 30-059 KRAKÓW, POLAND AGH UNIVERSITY OF SCIENCE AND TECHNOLOGY, FACULTY OF NON FERROUS METALS, DEPARTMENT OF MATERIALS SCIENCE AND NON – FERROUS METALS ENGINEERING, AL. A. MICKIEWICZA 30, 30-059 KRAKÓW, POLAND AGH UNIVERSITY OF SCIENCE AND TECHNOLOGY, FACULTY OF NON FERROUS METALS, DEPARTMENT OF MATERIALS SCIENCE AND NON – FERROUS METALS ENGINEERING, AL. A. MICKIEWICZA 30, 30-059 KRAKÓW, POLANDProcesses of severe plastic deformation (SPD) are defined as a group of metalworking techniques in which a very large plastic strain is imposed on a bulk material in order to make an ultra-fine grained metal. The present study attempts to apply Equal-Channel Angular Pressing (ECAP), Hydrostatic Extrusion (HE) and combination of ECAP and HE to 99.5% pure aluminium. ECAP process was realized at room temperature for 16 passes through route Bc using a die having an angle of 90°. Hydrostatic extrusion process was performed with cumulative strain of 2.68 to attain finally wire diameter of d = 3 mm. The microstructure of the samples was investigated by means of transmission and scanning electron microscopy. Additionally, the microhardness was measured and statistical analysis of the grains and subgrains was performed. Based on Kikuchi diffraction patterns misorientation was determined. The measured grain/subgrain size show, that regardless the mode of deformation process (ECAP, HE or combination of ECAP and HE processes), grain size is maintained at a similar level – equal to d = 0.55-0.59 μm. A combination of ECAP and HE has achieved better properties than either single process and show to be a promising procedure for manufacturing bulk UFG aluminium.http://www.degruyter.com/view/j/amm.2015.60.issue-2/amm-2015-0148/amm-2015-0148.xml?format=INTSevere Plastic Deformationultra-fine grained aluminiummicrostructure characterizationECAPhydrostatic extrusion
spellingShingle Leszczyńska-Madej B.
Richert M.W.
Perek-Nowak M.
Effect Of Severe Plastic Deformation On Microstructure Evolution Of Pure Aluminium
Archives of Metallurgy and Materials
Severe Plastic Deformation
ultra-fine grained aluminium
microstructure characterization
ECAP
hydrostatic extrusion
title Effect Of Severe Plastic Deformation On Microstructure Evolution Of Pure Aluminium
title_full Effect Of Severe Plastic Deformation On Microstructure Evolution Of Pure Aluminium
title_fullStr Effect Of Severe Plastic Deformation On Microstructure Evolution Of Pure Aluminium
title_full_unstemmed Effect Of Severe Plastic Deformation On Microstructure Evolution Of Pure Aluminium
title_short Effect Of Severe Plastic Deformation On Microstructure Evolution Of Pure Aluminium
title_sort effect of severe plastic deformation on microstructure evolution of pure aluminium
topic Severe Plastic Deformation
ultra-fine grained aluminium
microstructure characterization
ECAP
hydrostatic extrusion
url http://www.degruyter.com/view/j/amm.2015.60.issue-2/amm-2015-0148/amm-2015-0148.xml?format=INT
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