Low Power Resistive Oxygen Sensor Based on Sonochemical SrTi0.6Fe0.4O2.8 (STFO40)

The current paper reports on a sonochemical synthesis method for manufacturing nanostructured (typical grain size of 50 nm) SrTi0.6Fe0.4O2.8 (Sono-STFO40) powder. This powder is characterized using X ray-diffraction (XRD), Mössbauer spectroscopy and Scanning Electron Microscopy (SEM), and results a...

Full description

Bibliographic Details
Main Authors: Alisa Stratulat, Bogdan-Catalin Serban, Andrea de Luca, Viorel Avramescu, Cornel Cobianu, Mihai Brezeanu, Octavian Buiu, Lucian Diamandescu, Marcel Feder, Syed Zeeshan Ali, Florin Udrea
Format: Article
Language:English
Published: MDPI AG 2015-07-01
Series:Sensors
Subjects:
Online Access:http://www.mdpi.com/1424-8220/15/7/17495
_version_ 1811185276623519744
author Alisa Stratulat
Bogdan-Catalin Serban
Andrea de Luca
Viorel Avramescu
Cornel Cobianu
Mihai Brezeanu
Octavian Buiu
Lucian Diamandescu
Marcel Feder
Syed Zeeshan Ali
Florin Udrea
author_facet Alisa Stratulat
Bogdan-Catalin Serban
Andrea de Luca
Viorel Avramescu
Cornel Cobianu
Mihai Brezeanu
Octavian Buiu
Lucian Diamandescu
Marcel Feder
Syed Zeeshan Ali
Florin Udrea
author_sort Alisa Stratulat
collection DOAJ
description The current paper reports on a sonochemical synthesis method for manufacturing nanostructured (typical grain size of 50 nm) SrTi0.6Fe0.4O2.8 (Sono-STFO40) powder. This powder is characterized using X ray-diffraction (XRD), Mössbauer spectroscopy and Scanning Electron Microscopy (SEM), and results are compared with commercially available SrTi0.4Fe0.6O2.8 (STFO60) powder. In order to manufacture resistive oxygen sensors, both Sono-STFO40 and STFO60 are deposited, by dip-pen nanolithography (DPN) method, on an SOI (Silicon-on-Insulator) micro-hotplate, employing a tungsten heater embedded within a dielectric membrane. Oxygen detection tests are performed in both dry (RH = 0%) and humid (RH = 60%) nitrogen atmosphere, varying oxygen concentrations between 1% and 16% (v/v), at a constant heater temperature of 650 °C. The oxygen sensor, based on the Sono-STFO40 sensing layer, shows good sensitivity, low power consumption (80 mW), and short response time (25 s). These performance are comparable to those exhibited by state-of-the-art O2 sensors based on STFO60, thus proving Sono-STFO40 to be a material suitable for oxygen detection in harsh environments.
first_indexed 2024-04-11T13:27:51Z
format Article
id doaj.art-7327b36e11e343a88da7ea3ee0ee1ebf
institution Directory Open Access Journal
issn 1424-8220
language English
last_indexed 2024-04-11T13:27:51Z
publishDate 2015-07-01
publisher MDPI AG
record_format Article
series Sensors
spelling doaj.art-7327b36e11e343a88da7ea3ee0ee1ebf2022-12-22T04:22:00ZengMDPI AGSensors1424-82202015-07-01157174951750610.3390/s150717495s150717495Low Power Resistive Oxygen Sensor Based on Sonochemical SrTi0.6Fe0.4O2.8 (STFO40)Alisa Stratulat0Bogdan-Catalin Serban1Andrea de Luca2Viorel Avramescu3Cornel Cobianu4Mihai Brezeanu5Octavian Buiu6Lucian Diamandescu7Marcel Feder8Syed Zeeshan Ali9Florin Udrea10Honeywell Romania SRL, Sensors and Wireless Laboratory Bucharest (SWLB), Bucharest 020339, RomaniaHoneywell Romania SRL, Sensors and Wireless Laboratory Bucharest (SWLB), Bucharest 020339, RomaniaCentre for Advanced Photonics and Electronics (CAPE), University of Cambridge, Cambridge CB3 0FA, UKHoneywell Romania SRL, Sensors and Wireless Laboratory Bucharest (SWLB), Bucharest 020339, RomaniaHoneywell Romania SRL, Sensors and Wireless Laboratory Bucharest (SWLB), Bucharest 020339, RomaniaHoneywell Romania SRL, Sensors and Wireless Laboratory Bucharest (SWLB), Bucharest 020339, RomaniaHoneywell Romania SRL, Sensors and Wireless Laboratory Bucharest (SWLB), Bucharest 020339, RomaniaNational Institute of Materials Physics, Bucharest-Magurele, P.O. Box. MG-7, Magurele 77125, RomaniaNational Institute of Materials Physics, Bucharest-Magurele, P.O. Box. MG-7, Magurele 77125, RomaniaCambridge CMOS Sensors Ltd., Cambridge CB4 0DL, UKCentre for Advanced Photonics and Electronics (CAPE), University of Cambridge, Cambridge CB3 0FA, UKThe current paper reports on a sonochemical synthesis method for manufacturing nanostructured (typical grain size of 50 nm) SrTi0.6Fe0.4O2.8 (Sono-STFO40) powder. This powder is characterized using X ray-diffraction (XRD), Mössbauer spectroscopy and Scanning Electron Microscopy (SEM), and results are compared with commercially available SrTi0.4Fe0.6O2.8 (STFO60) powder. In order to manufacture resistive oxygen sensors, both Sono-STFO40 and STFO60 are deposited, by dip-pen nanolithography (DPN) method, on an SOI (Silicon-on-Insulator) micro-hotplate, employing a tungsten heater embedded within a dielectric membrane. Oxygen detection tests are performed in both dry (RH = 0%) and humid (RH = 60%) nitrogen atmosphere, varying oxygen concentrations between 1% and 16% (v/v), at a constant heater temperature of 650 °C. The oxygen sensor, based on the Sono-STFO40 sensing layer, shows good sensitivity, low power consumption (80 mW), and short response time (25 s). These performance are comparable to those exhibited by state-of-the-art O2 sensors based on STFO60, thus proving Sono-STFO40 to be a material suitable for oxygen detection in harsh environments.http://www.mdpi.com/1424-8220/15/7/17495sonochemistrySTFOoxygen sensingsilicon-on-InsulatorCMOS-compatibledip-pen nanolithographyharsh environment
spellingShingle Alisa Stratulat
Bogdan-Catalin Serban
Andrea de Luca
Viorel Avramescu
Cornel Cobianu
Mihai Brezeanu
Octavian Buiu
Lucian Diamandescu
Marcel Feder
Syed Zeeshan Ali
Florin Udrea
Low Power Resistive Oxygen Sensor Based on Sonochemical SrTi0.6Fe0.4O2.8 (STFO40)
Sensors
sonochemistry
STFO
oxygen sensing
silicon-on-Insulator
CMOS-compatible
dip-pen nanolithography
harsh environment
title Low Power Resistive Oxygen Sensor Based on Sonochemical SrTi0.6Fe0.4O2.8 (STFO40)
title_full Low Power Resistive Oxygen Sensor Based on Sonochemical SrTi0.6Fe0.4O2.8 (STFO40)
title_fullStr Low Power Resistive Oxygen Sensor Based on Sonochemical SrTi0.6Fe0.4O2.8 (STFO40)
title_full_unstemmed Low Power Resistive Oxygen Sensor Based on Sonochemical SrTi0.6Fe0.4O2.8 (STFO40)
title_short Low Power Resistive Oxygen Sensor Based on Sonochemical SrTi0.6Fe0.4O2.8 (STFO40)
title_sort low power resistive oxygen sensor based on sonochemical srti0 6fe0 4o2 8 stfo40
topic sonochemistry
STFO
oxygen sensing
silicon-on-Insulator
CMOS-compatible
dip-pen nanolithography
harsh environment
url http://www.mdpi.com/1424-8220/15/7/17495
work_keys_str_mv AT alisastratulat lowpowerresistiveoxygensensorbasedonsonochemicalsrti06fe04o28stfo40
AT bogdancatalinserban lowpowerresistiveoxygensensorbasedonsonochemicalsrti06fe04o28stfo40
AT andreadeluca lowpowerresistiveoxygensensorbasedonsonochemicalsrti06fe04o28stfo40
AT viorelavramescu lowpowerresistiveoxygensensorbasedonsonochemicalsrti06fe04o28stfo40
AT cornelcobianu lowpowerresistiveoxygensensorbasedonsonochemicalsrti06fe04o28stfo40
AT mihaibrezeanu lowpowerresistiveoxygensensorbasedonsonochemicalsrti06fe04o28stfo40
AT octavianbuiu lowpowerresistiveoxygensensorbasedonsonochemicalsrti06fe04o28stfo40
AT luciandiamandescu lowpowerresistiveoxygensensorbasedonsonochemicalsrti06fe04o28stfo40
AT marcelfeder lowpowerresistiveoxygensensorbasedonsonochemicalsrti06fe04o28stfo40
AT syedzeeshanali lowpowerresistiveoxygensensorbasedonsonochemicalsrti06fe04o28stfo40
AT florinudrea lowpowerresistiveoxygensensorbasedonsonochemicalsrti06fe04o28stfo40