Surface Modification of Electroosmotic Silicon Microchannel Using Thermal Dry Oxidation

A simple fabrication method for the surface modification of an electroosmotic silicon microchannel using thermal dry oxidation is presented. The surface modification is done by coating the silicon surface with a silicon dioxide (SiO2) layer using a thermal oxidation process. The process aims not onl...

Full description

Bibliographic Details
Main Authors: Tuan Norjihan Tuan Yaakub, Jumril Yunas, Rhonira Latif, Azrul Azlan Hamzah, Mohd Farhanulhakim Mohd Razip Wee, Burhanuddin Yeop Majlis
Format: Article
Language:English
Published: MDPI AG 2018-05-01
Series:Micromachines
Subjects:
Online Access:http://www.mdpi.com/2072-666X/9/5/222
_version_ 1818034653558210560
author Tuan Norjihan Tuan Yaakub
Jumril Yunas
Rhonira Latif
Azrul Azlan Hamzah
Mohd Farhanulhakim Mohd Razip Wee
Burhanuddin Yeop Majlis
author_facet Tuan Norjihan Tuan Yaakub
Jumril Yunas
Rhonira Latif
Azrul Azlan Hamzah
Mohd Farhanulhakim Mohd Razip Wee
Burhanuddin Yeop Majlis
author_sort Tuan Norjihan Tuan Yaakub
collection DOAJ
description A simple fabrication method for the surface modification of an electroosmotic silicon microchannel using thermal dry oxidation is presented. The surface modification is done by coating the silicon surface with a silicon dioxide (SiO2) layer using a thermal oxidation process. The process aims not only to improve the surface quality of the channel to be suitable for electroosmotic fluid transport but also to reduce the channel width using a simple technique. Initially, the parallel microchannel array with dimensions of 0.5 mm length and a width ranging from 1.8 µm to 2 µm are created using plasma etching on the 2 cm × 2 cm silicon substrate <100>. The oxidation of the silicon channel in a thermal chamber is then conducted to create the SiO2 layer. The layer properties and the quality of the surface are analyzed using scanning electron microscopy (SEM) and a surface profiler, respectively. The results show that the maximum oxidation growth rate occurs in the first 4 h of oxidation time and the rate decreases over time as the oxide layer becomes thicker. It is also found that the surface roughness is reduced with the increase of the process temperature and the oxide thickness. The scallop effect on the vertical wall due to the plasma etching process also improved with the presence of the oxide layer. After oxidation, the channel width is reduced by ~40%. The demonstrated method is suggested for the fabrication of a uniform channel cross section with high aspect ratio in sub-micro and nanometer scale that will be useful for the electroosmotic (EO) ion manipulation of the biomedical fluid sample.
first_indexed 2024-12-10T06:42:35Z
format Article
id doaj.art-7335647660bb43af970e4be72e6a9dbe
institution Directory Open Access Journal
issn 2072-666X
language English
last_indexed 2024-12-10T06:42:35Z
publishDate 2018-05-01
publisher MDPI AG
record_format Article
series Micromachines
spelling doaj.art-7335647660bb43af970e4be72e6a9dbe2022-12-22T01:58:45ZengMDPI AGMicromachines2072-666X2018-05-019522210.3390/mi9050222mi9050222Surface Modification of Electroosmotic Silicon Microchannel Using Thermal Dry OxidationTuan Norjihan Tuan Yaakub0Jumril Yunas1Rhonira Latif2Azrul Azlan Hamzah3Mohd Farhanulhakim Mohd Razip Wee4Burhanuddin Yeop Majlis5Institute of Microengineering and Nanoelectronics (IMEN), Universiti Kebangsaan Malaysia (UKM), 43600 UKM Bangi, Selangor, MalaysiaInstitute of Microengineering and Nanoelectronics (IMEN), Universiti Kebangsaan Malaysia (UKM), 43600 UKM Bangi, Selangor, MalaysiaInstitute of Microengineering and Nanoelectronics (IMEN), Universiti Kebangsaan Malaysia (UKM), 43600 UKM Bangi, Selangor, MalaysiaInstitute of Microengineering and Nanoelectronics (IMEN), Universiti Kebangsaan Malaysia (UKM), 43600 UKM Bangi, Selangor, MalaysiaInstitute of Microengineering and Nanoelectronics (IMEN), Universiti Kebangsaan Malaysia (UKM), 43600 UKM Bangi, Selangor, MalaysiaInstitute of Microengineering and Nanoelectronics (IMEN), Universiti Kebangsaan Malaysia (UKM), 43600 UKM Bangi, Selangor, MalaysiaA simple fabrication method for the surface modification of an electroosmotic silicon microchannel using thermal dry oxidation is presented. The surface modification is done by coating the silicon surface with a silicon dioxide (SiO2) layer using a thermal oxidation process. The process aims not only to improve the surface quality of the channel to be suitable for electroosmotic fluid transport but also to reduce the channel width using a simple technique. Initially, the parallel microchannel array with dimensions of 0.5 mm length and a width ranging from 1.8 µm to 2 µm are created using plasma etching on the 2 cm × 2 cm silicon substrate <100>. The oxidation of the silicon channel in a thermal chamber is then conducted to create the SiO2 layer. The layer properties and the quality of the surface are analyzed using scanning electron microscopy (SEM) and a surface profiler, respectively. The results show that the maximum oxidation growth rate occurs in the first 4 h of oxidation time and the rate decreases over time as the oxide layer becomes thicker. It is also found that the surface roughness is reduced with the increase of the process temperature and the oxide thickness. The scallop effect on the vertical wall due to the plasma etching process also improved with the presence of the oxide layer. After oxidation, the channel width is reduced by ~40%. The demonstrated method is suggested for the fabrication of a uniform channel cross section with high aspect ratio in sub-micro and nanometer scale that will be useful for the electroosmotic (EO) ion manipulation of the biomedical fluid sample.http://www.mdpi.com/2072-666X/9/5/222surface modificationelectroosmotic flowmicrofluidicsilicon nanochannelthermal oxidation
spellingShingle Tuan Norjihan Tuan Yaakub
Jumril Yunas
Rhonira Latif
Azrul Azlan Hamzah
Mohd Farhanulhakim Mohd Razip Wee
Burhanuddin Yeop Majlis
Surface Modification of Electroosmotic Silicon Microchannel Using Thermal Dry Oxidation
Micromachines
surface modification
electroosmotic flow
microfluidic
silicon nanochannel
thermal oxidation
title Surface Modification of Electroosmotic Silicon Microchannel Using Thermal Dry Oxidation
title_full Surface Modification of Electroosmotic Silicon Microchannel Using Thermal Dry Oxidation
title_fullStr Surface Modification of Electroosmotic Silicon Microchannel Using Thermal Dry Oxidation
title_full_unstemmed Surface Modification of Electroosmotic Silicon Microchannel Using Thermal Dry Oxidation
title_short Surface Modification of Electroosmotic Silicon Microchannel Using Thermal Dry Oxidation
title_sort surface modification of electroosmotic silicon microchannel using thermal dry oxidation
topic surface modification
electroosmotic flow
microfluidic
silicon nanochannel
thermal oxidation
url http://www.mdpi.com/2072-666X/9/5/222
work_keys_str_mv AT tuannorjihantuanyaakub surfacemodificationofelectroosmoticsiliconmicrochannelusingthermaldryoxidation
AT jumrilyunas surfacemodificationofelectroosmoticsiliconmicrochannelusingthermaldryoxidation
AT rhoniralatif surfacemodificationofelectroosmoticsiliconmicrochannelusingthermaldryoxidation
AT azrulazlanhamzah surfacemodificationofelectroosmoticsiliconmicrochannelusingthermaldryoxidation
AT mohdfarhanulhakimmohdrazipwee surfacemodificationofelectroosmoticsiliconmicrochannelusingthermaldryoxidation
AT burhanuddinyeopmajlis surfacemodificationofelectroosmoticsiliconmicrochannelusingthermaldryoxidation