Infiuence of Hydrogen on the Properties of Nanostructured C-Pd Films for Sensing Applications
In this paper we present the results of the investigations of nanostructured C-Pd films for hydrogen sensing applications. These C-Pd films were prepared by physical vapor deposition and then annealed in an argon flow at the temperature of 500°C. The structure and morphology of the prepared C-Pd fil...
| Main Authors: | , , , , |
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| Format: | Article |
| Language: | English |
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Sciendo
2014-06-01
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| Series: | Polish Journal of Chemical Technology |
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| Online Access: | https://doi.org/10.2478/pjct-2014-0034 |
| _version_ | 1818718778145374208 |
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| author | Kamińska Anna Diduszko Ryszard Krawczyk Sławomir Czerwosz Elżbieta Sobczak Kamil |
| author_facet | Kamińska Anna Diduszko Ryszard Krawczyk Sławomir Czerwosz Elżbieta Sobczak Kamil |
| author_sort | Kamińska Anna |
| collection | DOAJ |
| description | In this paper we present the results of the investigations of nanostructured C-Pd films for hydrogen sensing applications. These C-Pd films were prepared by physical vapor deposition and then annealed in an argon flow at the temperature of 500°C. The structure and morphology of the prepared C-Pd films were investigated using transmission electron microscopy and energy dispersive X-ray spectroscopy. We studied the infiuence of hydrogen on the electrical properties and crystal structure of C-Pd films. It was shown that film resistance changes depended on hydrogen concentration. At lower hydrogen concentration (up to 2 vol.%), the films response increased proportionally to [H2], while above 2 vol.% H2, it was almost constant. This is connected with the formation of a solid solution of hydrogen in palladium at lower H2 concentration and the creation of palladium hydride at higher H2 concentration. X-ray diffraction was used to confirm the formation of Pd-H solid solution and palladium hydride. |
| first_indexed | 2024-12-17T19:56:27Z |
| format | Article |
| id | doaj.art-765ca46480e341ee80af1ee6fcea0624 |
| institution | Directory Open Access Journal |
| issn | 1899-4741 |
| language | English |
| last_indexed | 2024-12-17T19:56:27Z |
| publishDate | 2014-06-01 |
| publisher | Sciendo |
| record_format | Article |
| series | Polish Journal of Chemical Technology |
| spelling | doaj.art-765ca46480e341ee80af1ee6fcea06242022-12-21T21:34:35ZengSciendoPolish Journal of Chemical Technology1899-47412014-06-01162778110.2478/pjct-2014-0034pjct-2014-0034Infiuence of Hydrogen on the Properties of Nanostructured C-Pd Films for Sensing ApplicationsKamińska Anna0Diduszko Ryszard1Krawczyk Sławomir2Czerwosz Elżbieta3Sobczak Kamil4Tele and Radio Research Institute, Ratuszowa 11, 03-450 Warsaw, PolandTele and Radio Research Institute, Ratuszowa 11, 03-450 Warsaw, PolandTele and Radio Research Institute, Ratuszowa 11, 03-450 Warsaw, PolandTele and Radio Research Institute, Ratuszowa 11, 03-450 Warsaw, PolandInstitute of Physics, PAS, al. Lotnikow 32/46, 02-668 Warsaw, PolandIn this paper we present the results of the investigations of nanostructured C-Pd films for hydrogen sensing applications. These C-Pd films were prepared by physical vapor deposition and then annealed in an argon flow at the temperature of 500°C. The structure and morphology of the prepared C-Pd films were investigated using transmission electron microscopy and energy dispersive X-ray spectroscopy. We studied the infiuence of hydrogen on the electrical properties and crystal structure of C-Pd films. It was shown that film resistance changes depended on hydrogen concentration. At lower hydrogen concentration (up to 2 vol.%), the films response increased proportionally to [H2], while above 2 vol.% H2, it was almost constant. This is connected with the formation of a solid solution of hydrogen in palladium at lower H2 concentration and the creation of palladium hydride at higher H2 concentration. X-ray diffraction was used to confirm the formation of Pd-H solid solution and palladium hydride.https://doi.org/10.2478/pjct-2014-0034c-pd filmshydrogen sensorgixd measurementsresistance changes |
| spellingShingle | Kamińska Anna Diduszko Ryszard Krawczyk Sławomir Czerwosz Elżbieta Sobczak Kamil Infiuence of Hydrogen on the Properties of Nanostructured C-Pd Films for Sensing Applications Polish Journal of Chemical Technology c-pd films hydrogen sensor gixd measurements resistance changes |
| title | Infiuence of Hydrogen on the Properties of Nanostructured C-Pd Films for Sensing Applications |
| title_full | Infiuence of Hydrogen on the Properties of Nanostructured C-Pd Films for Sensing Applications |
| title_fullStr | Infiuence of Hydrogen on the Properties of Nanostructured C-Pd Films for Sensing Applications |
| title_full_unstemmed | Infiuence of Hydrogen on the Properties of Nanostructured C-Pd Films for Sensing Applications |
| title_short | Infiuence of Hydrogen on the Properties of Nanostructured C-Pd Films for Sensing Applications |
| title_sort | infiuence of hydrogen on the properties of nanostructured c pd films for sensing applications |
| topic | c-pd films hydrogen sensor gixd measurements resistance changes |
| url | https://doi.org/10.2478/pjct-2014-0034 |
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