Dependence of Creep Performance and Microstructure Evolution on Solution Cooling Rate in a Polycrystalline Superalloy

It is well known that the solution cooling rate has a great effect on the creep life of superalloys. In this research, three typical cooling rates were applied to generate different distributions of γ’ precipitates for creep tests. Ingots used to make specimens were manufactured by hot extrusion, an...

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Main Authors: Chao Xu, Feng Liu, Lan Huang, Liang Jiang
Format: Article
Language:English
Published: MDPI AG 2017-12-01
Series:Metals
Subjects:
Online Access:https://www.mdpi.com/2075-4701/8/1/4
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author Chao Xu
Feng Liu
Lan Huang
Liang Jiang
author_facet Chao Xu
Feng Liu
Lan Huang
Liang Jiang
author_sort Chao Xu
collection DOAJ
description It is well known that the solution cooling rate has a great effect on the creep life of superalloys. In this research, three typical cooling rates were applied to generate different distributions of γ’ precipitates for creep tests. Ingots used to make specimens were manufactured by hot extrusion, and the master alloy had the composition of an FGH4096 power metallurgy superalloy. SEM and SESD were used to observe the microstructure’s evolution. The experimental results show that the fastest cooling rate corresponds to the highest creep life as well as the smallest rupture strain, and vice versa. The microscopic observations disclose that with an increasing cooling rate, the size and area fraction of γ’ precipitates decrease, and the rupture mechanism changes from transgranular to intergranular. Moreover, some γ’ precipitates changed to cuboid after the creep test. The results will provide new technological processes to design more creep-resistant, nickel-base superalloys.
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spelling doaj.art-768f52daca684315b383545c645e34c92022-12-21T23:02:03ZengMDPI AGMetals2075-47012017-12-0181410.3390/met8010004met8010004Dependence of Creep Performance and Microstructure Evolution on Solution Cooling Rate in a Polycrystalline SuperalloyChao Xu0Feng Liu1Lan Huang2Liang Jiang3State Key Laboratory of Powder Metallurgy, Central South University, Changsha 410083, ChinaState Key Laboratory of Powder Metallurgy, Central South University, Changsha 410083, ChinaState Key Laboratory of Powder Metallurgy, Central South University, Changsha 410083, ChinaState Key Laboratory of Powder Metallurgy, Central South University, Changsha 410083, ChinaIt is well known that the solution cooling rate has a great effect on the creep life of superalloys. In this research, three typical cooling rates were applied to generate different distributions of γ’ precipitates for creep tests. Ingots used to make specimens were manufactured by hot extrusion, and the master alloy had the composition of an FGH4096 power metallurgy superalloy. SEM and SESD were used to observe the microstructure’s evolution. The experimental results show that the fastest cooling rate corresponds to the highest creep life as well as the smallest rupture strain, and vice versa. The microscopic observations disclose that with an increasing cooling rate, the size and area fraction of γ’ precipitates decrease, and the rupture mechanism changes from transgranular to intergranular. Moreover, some γ’ precipitates changed to cuboid after the creep test. The results will provide new technological processes to design more creep-resistant, nickel-base superalloys.https://www.mdpi.com/2075-4701/8/1/4polycrystalline superalloycreepruptureγ’ precipitate
spellingShingle Chao Xu
Feng Liu
Lan Huang
Liang Jiang
Dependence of Creep Performance and Microstructure Evolution on Solution Cooling Rate in a Polycrystalline Superalloy
Metals
polycrystalline superalloy
creep
rupture
γ’ precipitate
title Dependence of Creep Performance and Microstructure Evolution on Solution Cooling Rate in a Polycrystalline Superalloy
title_full Dependence of Creep Performance and Microstructure Evolution on Solution Cooling Rate in a Polycrystalline Superalloy
title_fullStr Dependence of Creep Performance and Microstructure Evolution on Solution Cooling Rate in a Polycrystalline Superalloy
title_full_unstemmed Dependence of Creep Performance and Microstructure Evolution on Solution Cooling Rate in a Polycrystalline Superalloy
title_short Dependence of Creep Performance and Microstructure Evolution on Solution Cooling Rate in a Polycrystalline Superalloy
title_sort dependence of creep performance and microstructure evolution on solution cooling rate in a polycrystalline superalloy
topic polycrystalline superalloy
creep
rupture
γ’ precipitate
url https://www.mdpi.com/2075-4701/8/1/4
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AT lanhuang dependenceofcreepperformanceandmicrostructureevolutiononsolutioncoolingrateinapolycrystallinesuperalloy
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