A simple co-precipitation sorbent-based preconcentration method for the analysis of fungicides in water and juice samples by high-performance liquid chromatography coupled with photodiode array detection
Abstract A magnesium hydroxide co-precipitation sorbent-based method in the presence of an anionic surfactant (e.g., sodium dodecylbenzenesulfonate) and high-performance liquid chromatography were used to preconcentrate and analyze fungicides in water and apple juice samples. The preconcentration pr...
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| Format: | Article |
| Language: | English |
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SpringerOpen
2022-12-01
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| Series: | Journal of Analytical Science and Technology |
| Subjects: | |
| Online Access: | https://doi.org/10.1186/s40543-022-00356-z |
| _version_ | 1797977410739634176 |
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| author | Yanawath Santaladchaiyakit Anuchit Sirijan Methaporn Wongchalee Chayakom Phurimsak Areebhorn Baoulan Jirasak Gamonchuang Tittaya Boontongto Jitlada Vichapong Rodjana Burakham Supalax Srijaranai |
| author_facet | Yanawath Santaladchaiyakit Anuchit Sirijan Methaporn Wongchalee Chayakom Phurimsak Areebhorn Baoulan Jirasak Gamonchuang Tittaya Boontongto Jitlada Vichapong Rodjana Burakham Supalax Srijaranai |
| author_sort | Yanawath Santaladchaiyakit |
| collection | DOAJ |
| description | Abstract A magnesium hydroxide co-precipitation sorbent-based method in the presence of an anionic surfactant (e.g., sodium dodecylbenzenesulfonate) and high-performance liquid chromatography were used to preconcentrate and analyze fungicides in water and apple juice samples. The preconcentration procedure can be accomplished in a single step based on the co-precipitation of target fungicides and magnesium chloride in the presence of surfactant in a sodium hydroxide solution (pH 11) and a white precipitate gel was simply obtained after centrifugation. The property of precipitate phase was subsequently characterized using Fourier-transform infrared spectroscopy, scanning electron microscopy, and X-ray diffractometry. Under the optimum conditions, the developed method exhibited good sensitivity, with an enrichment factor of 11–18 and limits of detection of approximately 1–5 μg/L for water samples and 7–10 μg/L for apple juices. High reproducibility was achieved with a relative standard deviation of less than 11%, and a good recovery range of 72% to 120% was also obtained. The proposed method was shown to be a simple preconcentration procedure for concentrating fungicides in the samples investigated. |
| first_indexed | 2024-04-11T05:06:28Z |
| format | Article |
| id | doaj.art-7714b3d43e6b45fcba010df74e804ea1 |
| institution | Directory Open Access Journal |
| issn | 2093-3371 |
| language | English |
| last_indexed | 2024-04-11T05:06:28Z |
| publishDate | 2022-12-01 |
| publisher | SpringerOpen |
| record_format | Article |
| series | Journal of Analytical Science and Technology |
| spelling | doaj.art-7714b3d43e6b45fcba010df74e804ea12022-12-25T12:19:19ZengSpringerOpenJournal of Analytical Science and Technology2093-33712022-12-0113111310.1186/s40543-022-00356-zA simple co-precipitation sorbent-based preconcentration method for the analysis of fungicides in water and juice samples by high-performance liquid chromatography coupled with photodiode array detectionYanawath Santaladchaiyakit0Anuchit Sirijan1Methaporn Wongchalee2Chayakom Phurimsak3Areebhorn Baoulan4Jirasak Gamonchuang5Tittaya Boontongto6Jitlada Vichapong7Rodjana Burakham8Supalax Srijaranai9Department of Chemistry, Faculty of Engineering, Rajamangala University of Technology IsanDepartment of Chemistry, Faculty of Engineering, Rajamangala University of Technology IsanDepartment of Chemistry, Faculty of Engineering, Rajamangala University of Technology IsanDepartment of Chemistry, Faculty of Engineering, Rajamangala University of Technology IsanDepartment of Chemistry, Faculty of Engineering, Rajamangala University of Technology IsanMaterials Chemistry Research Center, Department of Chemistry and Center of Excellence for Innovation in Chemistry, Faculty of Science, Khon Kaen UniversityMaterials Chemistry Research Center, Department of Chemistry and Center of Excellence for Innovation in Chemistry, Faculty of Science, Khon Kaen UniversityCreative Chemistry and Innovation Research Unit, Department of Chemistry and Center of Excellence for Innovation in Chemistry, Faculty of Science, Mahasarakham UniversityMaterials Chemistry Research Center, Department of Chemistry and Center of Excellence for Innovation in Chemistry, Faculty of Science, Khon Kaen UniversityMaterials Chemistry Research Center, Department of Chemistry and Center of Excellence for Innovation in Chemistry, Faculty of Science, Khon Kaen UniversityAbstract A magnesium hydroxide co-precipitation sorbent-based method in the presence of an anionic surfactant (e.g., sodium dodecylbenzenesulfonate) and high-performance liquid chromatography were used to preconcentrate and analyze fungicides in water and apple juice samples. The preconcentration procedure can be accomplished in a single step based on the co-precipitation of target fungicides and magnesium chloride in the presence of surfactant in a sodium hydroxide solution (pH 11) and a white precipitate gel was simply obtained after centrifugation. The property of precipitate phase was subsequently characterized using Fourier-transform infrared spectroscopy, scanning electron microscopy, and X-ray diffractometry. Under the optimum conditions, the developed method exhibited good sensitivity, with an enrichment factor of 11–18 and limits of detection of approximately 1–5 μg/L for water samples and 7–10 μg/L for apple juices. High reproducibility was achieved with a relative standard deviation of less than 11%, and a good recovery range of 72% to 120% was also obtained. The proposed method was shown to be a simple preconcentration procedure for concentrating fungicides in the samples investigated.https://doi.org/10.1186/s40543-022-00356-zCarbendazimThiabendazoleFuberidazoleSodium dodecylbenzenesulfonateMetal hydroxideHPLC |
| spellingShingle | Yanawath Santaladchaiyakit Anuchit Sirijan Methaporn Wongchalee Chayakom Phurimsak Areebhorn Baoulan Jirasak Gamonchuang Tittaya Boontongto Jitlada Vichapong Rodjana Burakham Supalax Srijaranai A simple co-precipitation sorbent-based preconcentration method for the analysis of fungicides in water and juice samples by high-performance liquid chromatography coupled with photodiode array detection Journal of Analytical Science and Technology Carbendazim Thiabendazole Fuberidazole Sodium dodecylbenzenesulfonate Metal hydroxide HPLC |
| title | A simple co-precipitation sorbent-based preconcentration method for the analysis of fungicides in water and juice samples by high-performance liquid chromatography coupled with photodiode array detection |
| title_full | A simple co-precipitation sorbent-based preconcentration method for the analysis of fungicides in water and juice samples by high-performance liquid chromatography coupled with photodiode array detection |
| title_fullStr | A simple co-precipitation sorbent-based preconcentration method for the analysis of fungicides in water and juice samples by high-performance liquid chromatography coupled with photodiode array detection |
| title_full_unstemmed | A simple co-precipitation sorbent-based preconcentration method for the analysis of fungicides in water and juice samples by high-performance liquid chromatography coupled with photodiode array detection |
| title_short | A simple co-precipitation sorbent-based preconcentration method for the analysis of fungicides in water and juice samples by high-performance liquid chromatography coupled with photodiode array detection |
| title_sort | simple co precipitation sorbent based preconcentration method for the analysis of fungicides in water and juice samples by high performance liquid chromatography coupled with photodiode array detection |
| topic | Carbendazim Thiabendazole Fuberidazole Sodium dodecylbenzenesulfonate Metal hydroxide HPLC |
| url | https://doi.org/10.1186/s40543-022-00356-z |
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