Synthesis, Crystal Structure, and Some Transformations of 9,12-Dichloro-<i>ortho</i>-Carborane

Synthesis, Crystal Structure, and Some Transformations of 9,12-Dichloro-<i>ortho</i>-Carborane

Reaction of <i>ortho</i>-carborane with anhydrous AlCl<sub>3</sub> in chloroform results in a mixture of 9-chloro, 9,12-dichloro, and 8,9,12-trichloro derivatives with 9,12-dichloro-<i>ortho</i>-carborane being the main product. Molecular crystal structure of 9,12...

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Bibliographic Details
Main Authors: Sergey A. Anufriev, Sergey V. Timofeev, Olga B. Zhidkova, Kyrill Yu. Suponitsky, Igor B. Sivaev
Format: Article
Language:English
Published: MDPI AG 2022-09-01
Series:Crystals
Subjects:
carborane
chloro derivatives
synthesis
NMR spectra
single crystal X-ray diffraction
Online Access:https://www.mdpi.com/2073-4352/12/9/1251

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https://www.mdpi.com/2073-4352/12/9/1251

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