Rapid method to obtain virgin olive oil for acidity determination.

A rapid and simple method to obtain, from olive samples, enough quantity of oil to determine acidity grade is proposed. From paste samples of milled olives, different fraction are separated to be centrifugated during 5 minutes at 4500 r.p.m. Oil acidity results obtained from sodium sulfate anhidrous...

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Main Authors: F. Martínez, Mª J. Moyano, J. Alba, Mª A. Ruiz, F. Hidalgo, F. J. Heredia
Format: Article
Language:English
Published: Consejo Superior de Investigaciones Científicas 1999-04-01
Series:Grasas y Aceites
Subjects:
Online Access:http://grasasyaceites.revistas.csic.es/index.php/grasasyaceites/article/view/646
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author F. Martínez
Mª J. Moyano
J. Alba
Mª A. Ruiz
F. Hidalgo
F. J. Heredia
author_facet F. Martínez
Mª J. Moyano
J. Alba
Mª A. Ruiz
F. Hidalgo
F. J. Heredia
author_sort F. Martínez
collection DOAJ
description A rapid and simple method to obtain, from olive samples, enough quantity of oil to determine acidity grade is proposed. From paste samples of milled olives, different fraction are separated to be centrifugated during 5 minutes at 4500 r.p.m. Oil acidity results obtained from sodium sulfate anhidrous and natural microtalc added samples are compared with blank samples, and with those obtained by the Abencor extraction procedure. The correlation between the acidity of oil samples obtained by the Abencor method is also analyzed against other samples obtained by the normalized method in Spain, norm UNE 55070, Soxhlet system. Results show that in all the centrifugated samples enough amount of oil is obtained to determin the acidity grade, it also show that treatment with sodium sulfate anhidrous obtains a bigger recovery percentage, and that in all 3 cases, the acidity shows a good correlation with that of the Abencor system, doubling the number of samples analysed by the Abencor system. It also shows that the acidity grade obtained by using the UNE 55070 norm is aproximately 0,3 grades above that obtained by the Abencor system.
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spelling doaj.art-77f06532886f4af5ba9feccc27576d472022-12-21T18:52:14ZengConsejo Superior de Investigaciones CientíficasGrasas y Aceites0017-34951988-42141999-04-0150212212610.3989/gya.1999.v50.i2.646636Rapid method to obtain virgin olive oil for acidity determination.F. Martínez0Mª J. Moyano1J. Alba2Mª A. Ruiz3F. Hidalgo4F. J. Heredia5Almazara Experimental. Instituto de la Grasa (GSIC)Almazara Experimental. Instituto de la Grasa (GSIC)Almazara Experimental. Instituto de la Grasa (GSIC)Almazara Experimental. Instituto de la Grasa (GSIC)Almazara Experimental. Instituto de la Grasa (GSIC)Area de Nutrición y Bromatología. Facultad de Farmacia. Universidad de Sevilla.A rapid and simple method to obtain, from olive samples, enough quantity of oil to determine acidity grade is proposed. From paste samples of milled olives, different fraction are separated to be centrifugated during 5 minutes at 4500 r.p.m. Oil acidity results obtained from sodium sulfate anhidrous and natural microtalc added samples are compared with blank samples, and with those obtained by the Abencor extraction procedure. The correlation between the acidity of oil samples obtained by the Abencor method is also analyzed against other samples obtained by the normalized method in Spain, norm UNE 55070, Soxhlet system. Results show that in all the centrifugated samples enough amount of oil is obtained to determin the acidity grade, it also show that treatment with sodium sulfate anhidrous obtains a bigger recovery percentage, and that in all 3 cases, the acidity shows a good correlation with that of the Abencor system, doubling the number of samples analysed by the Abencor system. It also shows that the acidity grade obtained by using the UNE 55070 norm is aproximately 0,3 grades above that obtained by the Abencor system.http://grasasyaceites.revistas.csic.es/index.php/grasasyaceites/article/view/646acidityanalysiscentrifugationqualityvirgin olive oil.
spellingShingle F. Martínez
Mª J. Moyano
J. Alba
Mª A. Ruiz
F. Hidalgo
F. J. Heredia
Rapid method to obtain virgin olive oil for acidity determination.
Grasas y Aceites
acidity
analysis
centrifugation
quality
virgin olive oil.
title Rapid method to obtain virgin olive oil for acidity determination.
title_full Rapid method to obtain virgin olive oil for acidity determination.
title_fullStr Rapid method to obtain virgin olive oil for acidity determination.
title_full_unstemmed Rapid method to obtain virgin olive oil for acidity determination.
title_short Rapid method to obtain virgin olive oil for acidity determination.
title_sort rapid method to obtain virgin olive oil for acidity determination
topic acidity
analysis
centrifugation
quality
virgin olive oil.
url http://grasasyaceites.revistas.csic.es/index.php/grasasyaceites/article/view/646
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