Comparison of Gas Sensing Properties of Reduced Graphene Oxide Obtained by Two Different Methods

In this study, the sensitivity of reduced graphene oxide structures (rGO) to the action of selected gases (especially hydrogen, but also nitrogen dioxide and ammonia) was examined. Two sensing structures, based on rGO structures, obtained by different methods of oxidation (the modified Hummers, and...

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Main Authors: Sabina Drewniak, Marcin Procek, Roksana Muzyka, Tadeusz Pustelny
Format: Article
Language:English
Published: MDPI AG 2020-06-01
Series:Sensors
Subjects:
Online Access:https://www.mdpi.com/1424-8220/20/11/3175
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author Sabina Drewniak
Marcin Procek
Roksana Muzyka
Tadeusz Pustelny
author_facet Sabina Drewniak
Marcin Procek
Roksana Muzyka
Tadeusz Pustelny
author_sort Sabina Drewniak
collection DOAJ
description In this study, the sensitivity of reduced graphene oxide structures (rGO) to the action of selected gases (especially hydrogen, but also nitrogen dioxide and ammonia) was examined. Two sensing structures, based on rGO structures, obtained by different methods of oxidation (the modified Hummers, and the modified Tour’s method respectively), were investigated. We show here that the method used for the oxidation of rGO influences the sensitivity of the sensing structure during contact with various gaseous atmospheres. We performed our experiments in the atmosphere, containing hydrogen in a concentration range from 0 to 4% in nitrogen or synthetic air, both in dry and wet conditions. The temperature range was from 50 °C to 190 °C. Finally, we checked how the resistance of the samples changes when the other gases (NO<sub>2</sub>, NH<sub>3</sub>) appear in tested gas mixtures. The gas investigations were supplemented by the characterization of rGOs materials using scanning electron microscopy (SEM), X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS) and N<sub>2</sub> sorption method.
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spelling doaj.art-783933f9794f4e76b8df6c1b08d4a1c72023-11-20T02:43:36ZengMDPI AGSensors1424-82202020-06-012011317510.3390/s20113175Comparison of Gas Sensing Properties of Reduced Graphene Oxide Obtained by Two Different MethodsSabina Drewniak0Marcin Procek1Roksana Muzyka2Tadeusz Pustelny3Department of Optoelectronics, Silesian University of Technology, 2 Krzywoustego St., 44-100 Gliwice, PolandDepartment of Optoelectronics, Silesian University of Technology, 2 Krzywoustego St., 44-100 Gliwice, PolandInstitute for Chemical Processing of Coal, 1 Zamkowa St., 41-803 Zabrze, PolandDepartment of Optoelectronics, Silesian University of Technology, 2 Krzywoustego St., 44-100 Gliwice, PolandIn this study, the sensitivity of reduced graphene oxide structures (rGO) to the action of selected gases (especially hydrogen, but also nitrogen dioxide and ammonia) was examined. Two sensing structures, based on rGO structures, obtained by different methods of oxidation (the modified Hummers, and the modified Tour’s method respectively), were investigated. We show here that the method used for the oxidation of rGO influences the sensitivity of the sensing structure during contact with various gaseous atmospheres. We performed our experiments in the atmosphere, containing hydrogen in a concentration range from 0 to 4% in nitrogen or synthetic air, both in dry and wet conditions. The temperature range was from 50 °C to 190 °C. Finally, we checked how the resistance of the samples changes when the other gases (NO<sub>2</sub>, NH<sub>3</sub>) appear in tested gas mixtures. The gas investigations were supplemented by the characterization of rGOs materials using scanning electron microscopy (SEM), X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS) and N<sub>2</sub> sorption method.https://www.mdpi.com/1424-8220/20/11/3175reduced graphene oxidegas sensorsensing structurehydrogen
spellingShingle Sabina Drewniak
Marcin Procek
Roksana Muzyka
Tadeusz Pustelny
Comparison of Gas Sensing Properties of Reduced Graphene Oxide Obtained by Two Different Methods
Sensors
reduced graphene oxide
gas sensor
sensing structure
hydrogen
title Comparison of Gas Sensing Properties of Reduced Graphene Oxide Obtained by Two Different Methods
title_full Comparison of Gas Sensing Properties of Reduced Graphene Oxide Obtained by Two Different Methods
title_fullStr Comparison of Gas Sensing Properties of Reduced Graphene Oxide Obtained by Two Different Methods
title_full_unstemmed Comparison of Gas Sensing Properties of Reduced Graphene Oxide Obtained by Two Different Methods
title_short Comparison of Gas Sensing Properties of Reduced Graphene Oxide Obtained by Two Different Methods
title_sort comparison of gas sensing properties of reduced graphene oxide obtained by two different methods
topic reduced graphene oxide
gas sensor
sensing structure
hydrogen
url https://www.mdpi.com/1424-8220/20/11/3175
work_keys_str_mv AT sabinadrewniak comparisonofgassensingpropertiesofreducedgrapheneoxideobtainedbytwodifferentmethods
AT marcinprocek comparisonofgassensingpropertiesofreducedgrapheneoxideobtainedbytwodifferentmethods
AT roksanamuzyka comparisonofgassensingpropertiesofreducedgrapheneoxideobtainedbytwodifferentmethods
AT tadeuszpustelny comparisonofgassensingpropertiesofreducedgrapheneoxideobtainedbytwodifferentmethods