Production of Surface Layer with Gradient Microstructure and Microhardess on Copper by High Pressure Surface Rolling

Pure copper was subjected to high-pressure surface rolling (HPSR) to obtain a surface gradient layer. Effects of HPSR parameters on the surface microstructure and microhardness of Cu were investigated by using optical microscopy, transmission electronic microscopy, X-ray diffraction, and the microha...

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Main Authors: Juying Li, Qingsong Mei, Yana Li, Beihai Wang
Format: Article
Language:English
Published: MDPI AG 2020-01-01
Series:Metals
Subjects:
Online Access:https://www.mdpi.com/2075-4701/10/1/73
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author Juying Li
Qingsong Mei
Yana Li
Beihai Wang
author_facet Juying Li
Qingsong Mei
Yana Li
Beihai Wang
author_sort Juying Li
collection DOAJ
description Pure copper was subjected to high-pressure surface rolling (HPSR) to obtain a surface gradient layer. Effects of HPSR parameters on the surface microstructure and microhardness of Cu were investigated by using optical microscopy, transmission electronic microscopy, X-ray diffraction, and the microhardness test. The HPSR surface layer has a gradient microstructure consisting of increasingly refined grains with decreasing depth from the treated surface (DFS). The thicknesses of the refined surface layer can be up to ~1.8 mm, and the grain size of the topmost surface is down to ~88 nm, depending on the HPSR parameters including pressure, time, and temperature. Microhardness of HPSR samples increases with decreasing DFS, with a maximum of ~2.4 times that of the undeformed matrix. The present results indicated that HPSR could be an effective method for the production of a mm-thick surface layer on Cu with gradient microstructure and property.
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spelling doaj.art-7952bd5e923f4049b4ad9d55d6e6d2fe2022-12-22T01:32:45ZengMDPI AGMetals2075-47012020-01-011017310.3390/met10010073met10010073Production of Surface Layer with Gradient Microstructure and Microhardess on Copper by High Pressure Surface RollingJuying Li0Qingsong Mei1Yana Li2Beihai Wang3School of Mechanical Engineering, Wuhan Polytechnic University, Wuhan 430023, ChinaSchool of Power and Mechanical Engineering, Wuhan University, Wuhan 430072, ChinaSchool of Mechanical Engineering, Wuhan Polytechnic University, Wuhan 430023, ChinaSchool of Mechanical Engineering, Wuhan Polytechnic University, Wuhan 430023, ChinaPure copper was subjected to high-pressure surface rolling (HPSR) to obtain a surface gradient layer. Effects of HPSR parameters on the surface microstructure and microhardness of Cu were investigated by using optical microscopy, transmission electronic microscopy, X-ray diffraction, and the microhardness test. The HPSR surface layer has a gradient microstructure consisting of increasingly refined grains with decreasing depth from the treated surface (DFS). The thicknesses of the refined surface layer can be up to ~1.8 mm, and the grain size of the topmost surface is down to ~88 nm, depending on the HPSR parameters including pressure, time, and temperature. Microhardness of HPSR samples increases with decreasing DFS, with a maximum of ~2.4 times that of the undeformed matrix. The present results indicated that HPSR could be an effective method for the production of a mm-thick surface layer on Cu with gradient microstructure and property.https://www.mdpi.com/2075-4701/10/1/73high-pressure surface rollingcoppergrain refinementmicrohardness
spellingShingle Juying Li
Qingsong Mei
Yana Li
Beihai Wang
Production of Surface Layer with Gradient Microstructure and Microhardess on Copper by High Pressure Surface Rolling
Metals
high-pressure surface rolling
copper
grain refinement
microhardness
title Production of Surface Layer with Gradient Microstructure and Microhardess on Copper by High Pressure Surface Rolling
title_full Production of Surface Layer with Gradient Microstructure and Microhardess on Copper by High Pressure Surface Rolling
title_fullStr Production of Surface Layer with Gradient Microstructure and Microhardess on Copper by High Pressure Surface Rolling
title_full_unstemmed Production of Surface Layer with Gradient Microstructure and Microhardess on Copper by High Pressure Surface Rolling
title_short Production of Surface Layer with Gradient Microstructure and Microhardess on Copper by High Pressure Surface Rolling
title_sort production of surface layer with gradient microstructure and microhardess on copper by high pressure surface rolling
topic high-pressure surface rolling
copper
grain refinement
microhardness
url https://www.mdpi.com/2075-4701/10/1/73
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AT yanali productionofsurfacelayerwithgradientmicrostructureandmicrohardessoncopperbyhighpressuresurfacerolling
AT beihaiwang productionofsurfacelayerwithgradientmicrostructureandmicrohardessoncopperbyhighpressuresurfacerolling