Dynamic Wet Etching of Silicon through Isopropanol Alcohol Evaporation

In this paper, Isopropanol (IPA) availability during the anisotropic etching of silicon in Potassium Hydroxide (KOH) solutions was investigated. Squares of 8 to 40 µm were patterned to (100) oriented silicon wafers through DWL (Direct Writing Laser) photolithography. The wet etching process was perf...

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Main Authors: Tiago S. Monteiro, Pamakštys Kastytis, Luís M. Gonçalves, Graça Minas, Susana Cardoso
Format: Article
Language:English
Published: MDPI AG 2015-10-01
Series:Micromachines
Subjects:
Online Access:http://www.mdpi.com/2072-666X/6/10/1437
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author Tiago S. Monteiro
Pamakštys Kastytis
Luís M. Gonçalves
Graça Minas
Susana Cardoso
author_facet Tiago S. Monteiro
Pamakštys Kastytis
Luís M. Gonçalves
Graça Minas
Susana Cardoso
author_sort Tiago S. Monteiro
collection DOAJ
description In this paper, Isopropanol (IPA) availability during the anisotropic etching of silicon in Potassium Hydroxide (KOH) solutions was investigated. Squares of 8 to 40 µm were patterned to (100) oriented silicon wafers through DWL (Direct Writing Laser) photolithography. The wet etching process was performed inside an open HDPE (High Density Polyethylene) flask with ultrasonic agitation. IPA volume and evaporation was studied in a dynamic etching process, and subsequent influence on the silicon etching was inspected. For the tested conditions, evaporation rates for water vapor and IPA were determined as approximately 0.0417 mL/min and 0.175 mL/min, respectively. Results demonstrate that IPA availability, and not concentration, plays an important role in the definition of the final structure. Transversal SEM (Scanning Electron Microscopy) analysis demonstrates a correlation between microloading effects (as a consequence of structure spacing) and the angle formed towards the (100) plane.
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spelling doaj.art-7971fcfb70ac4bc2980b9082178bdbfe2022-12-22T00:31:17ZengMDPI AGMicromachines2072-666X2015-10-016101534154510.3390/mi6101437mi6101437Dynamic Wet Etching of Silicon through Isopropanol Alcohol EvaporationTiago S. Monteiro0Pamakštys Kastytis1Luís M. Gonçalves2Graça Minas3Susana Cardoso4Instituto de Engenharia de Sistemas de Computadores–Microsystems and Nanotechnology (INESC–MN), Rua Alves Redol, Lisboa 1000-029, PortugalInstituto de Engenharia de Sistemas de Computadores–Microsystems and Nanotechnology (INESC–MN), Rua Alves Redol, Lisboa 1000-029, PortugalMicroelectromechanical Systems Research Unit (CMEMS-UMinho), Universidade do Minho, Campus de Azurem, Guimarães 4800-058, PortugalMicroelectromechanical Systems Research Unit (CMEMS-UMinho), Universidade do Minho, Campus de Azurem, Guimarães 4800-058, PortugalInstituto de Engenharia de Sistemas de Computadores–Microsystems and Nanotechnology (INESC–MN), Rua Alves Redol, Lisboa 1000-029, PortugalIn this paper, Isopropanol (IPA) availability during the anisotropic etching of silicon in Potassium Hydroxide (KOH) solutions was investigated. Squares of 8 to 40 µm were patterned to (100) oriented silicon wafers through DWL (Direct Writing Laser) photolithography. The wet etching process was performed inside an open HDPE (High Density Polyethylene) flask with ultrasonic agitation. IPA volume and evaporation was studied in a dynamic etching process, and subsequent influence on the silicon etching was inspected. For the tested conditions, evaporation rates for water vapor and IPA were determined as approximately 0.0417 mL/min and 0.175 mL/min, respectively. Results demonstrate that IPA availability, and not concentration, plays an important role in the definition of the final structure. Transversal SEM (Scanning Electron Microscopy) analysis demonstrates a correlation between microloading effects (as a consequence of structure spacing) and the angle formed towards the (100) plane.http://www.mdpi.com/2072-666X/6/10/1437isopropanol evaporationisopropanol availabilitysilicon wet etchingmicroloading effect
spellingShingle Tiago S. Monteiro
Pamakštys Kastytis
Luís M. Gonçalves
Graça Minas
Susana Cardoso
Dynamic Wet Etching of Silicon through Isopropanol Alcohol Evaporation
Micromachines
isopropanol evaporation
isopropanol availability
silicon wet etching
microloading effect
title Dynamic Wet Etching of Silicon through Isopropanol Alcohol Evaporation
title_full Dynamic Wet Etching of Silicon through Isopropanol Alcohol Evaporation
title_fullStr Dynamic Wet Etching of Silicon through Isopropanol Alcohol Evaporation
title_full_unstemmed Dynamic Wet Etching of Silicon through Isopropanol Alcohol Evaporation
title_short Dynamic Wet Etching of Silicon through Isopropanol Alcohol Evaporation
title_sort dynamic wet etching of silicon through isopropanol alcohol evaporation
topic isopropanol evaporation
isopropanol availability
silicon wet etching
microloading effect
url http://www.mdpi.com/2072-666X/6/10/1437
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AT pamakstyskastytis dynamicwetetchingofsiliconthroughisopropanolalcoholevaporation
AT luismgoncalves dynamicwetetchingofsiliconthroughisopropanolalcoholevaporation
AT gracaminas dynamicwetetchingofsiliconthroughisopropanolalcoholevaporation
AT susanacardoso dynamicwetetchingofsiliconthroughisopropanolalcoholevaporation