Effect of Internal Hydrogen on the Fatigue Crack Growth Rate in the Coarse-Grain Heat-Affected Zone of a CrMo Steel

The effect of internal hydrogen in the fatigue crack growth rate of the coarse grain region of a 2.25Cr1Mo steel welded joint was analyzed in this work. The microstructure of the coarse grain region was simulated by means of a heat treatment able to provide the same microstructure with a similar pri...

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Main Authors: Guillermo Álvarez, Alfredo Zafra, Francisco Javier Belzunce, Cristina Rodríguez
Format: Article
Language:English
Published: MDPI AG 2022-04-01
Series:Metals
Subjects:
Online Access:https://www.mdpi.com/2075-4701/12/4/673
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author Guillermo Álvarez
Alfredo Zafra
Francisco Javier Belzunce
Cristina Rodríguez
author_facet Guillermo Álvarez
Alfredo Zafra
Francisco Javier Belzunce
Cristina Rodríguez
author_sort Guillermo Álvarez
collection DOAJ
description The effect of internal hydrogen in the fatigue crack growth rate of the coarse grain region of a 2.25Cr1Mo steel welded joint was analyzed in this work. The microstructure of the coarse grain region was simulated by means of a heat treatment able to provide the same microstructure with a similar prior austenite grain size and hardness to the one in a real welded joint. The fatigue crack growth rate was measured under standard laboratory conditions using compact tensile (CT) specimens that were (i) uncharged and hydrogen pre-charged in a hydrogen pressure reactor (under 19.5 MPa and 450 °C for 21 h). The influence of fatigue frequency was assessed using frequencies of 10 Hz, 0.1 Hz, and 0.05 Hz. Additionally, two load ratios (<i>R</i> = 0.1 and <i>R</i> = 0.5) were applied to analyze their influence in the <i>da/dN</i> vs. ∆<i>K</i> curves and therefore in the fatigue crack growth rate. The embrittlement produced by the presence of internal hydrogen was clearly noticed at the beginning of the fatigue crack growth rate test (Δ<i>K</i> = 30 MP<inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><mrow><msqrt><mi>m</mi></msqrt></mrow></semantics></math></inline-formula>), obtaining significant higher values than without hydrogen. This effect became more notorious as the test frequency decreased and the load ratio increased. At the same time, the failure mechanism changed from ductile (striations) to brittle (hydrogen decohesion) with intergranular fracture (IG) becoming the predominant failure mechanism under the highest loads (<i>R</i> = 0.5).
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spelling doaj.art-7a6ded6cefa34b3e8b12d66d04a61c672023-12-01T21:14:12ZengMDPI AGMetals2075-47012022-04-0112467310.3390/met12040673Effect of Internal Hydrogen on the Fatigue Crack Growth Rate in the Coarse-Grain Heat-Affected Zone of a CrMo SteelGuillermo Álvarez0Alfredo Zafra1Francisco Javier Belzunce2Cristina Rodríguez3SIMUMECAMAT Research Group, University of Oviedo, Campus Universitario, 33203 Gijón, SpainSIMUMECAMAT Research Group, University of Oviedo, Campus Universitario, 33203 Gijón, SpainSIMUMECAMAT Research Group, University of Oviedo, Campus Universitario, 33203 Gijón, SpainSIMUMECAMAT Research Group, University of Oviedo, Campus Universitario, 33203 Gijón, SpainThe effect of internal hydrogen in the fatigue crack growth rate of the coarse grain region of a 2.25Cr1Mo steel welded joint was analyzed in this work. The microstructure of the coarse grain region was simulated by means of a heat treatment able to provide the same microstructure with a similar prior austenite grain size and hardness to the one in a real welded joint. The fatigue crack growth rate was measured under standard laboratory conditions using compact tensile (CT) specimens that were (i) uncharged and hydrogen pre-charged in a hydrogen pressure reactor (under 19.5 MPa and 450 °C for 21 h). The influence of fatigue frequency was assessed using frequencies of 10 Hz, 0.1 Hz, and 0.05 Hz. Additionally, two load ratios (<i>R</i> = 0.1 and <i>R</i> = 0.5) were applied to analyze their influence in the <i>da/dN</i> vs. ∆<i>K</i> curves and therefore in the fatigue crack growth rate. The embrittlement produced by the presence of internal hydrogen was clearly noticed at the beginning of the fatigue crack growth rate test (Δ<i>K</i> = 30 MP<inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><mrow><msqrt><mi>m</mi></msqrt></mrow></semantics></math></inline-formula>), obtaining significant higher values than without hydrogen. This effect became more notorious as the test frequency decreased and the load ratio increased. At the same time, the failure mechanism changed from ductile (striations) to brittle (hydrogen decohesion) with intergranular fracture (IG) becoming the predominant failure mechanism under the highest loads (<i>R</i> = 0.5).https://www.mdpi.com/2075-4701/12/4/673hydrogen embrittlementfatigue crack growth ratepre-charged specimenscoarse grain heat affected zone
spellingShingle Guillermo Álvarez
Alfredo Zafra
Francisco Javier Belzunce
Cristina Rodríguez
Effect of Internal Hydrogen on the Fatigue Crack Growth Rate in the Coarse-Grain Heat-Affected Zone of a CrMo Steel
Metals
hydrogen embrittlement
fatigue crack growth rate
pre-charged specimens
coarse grain heat affected zone
title Effect of Internal Hydrogen on the Fatigue Crack Growth Rate in the Coarse-Grain Heat-Affected Zone of a CrMo Steel
title_full Effect of Internal Hydrogen on the Fatigue Crack Growth Rate in the Coarse-Grain Heat-Affected Zone of a CrMo Steel
title_fullStr Effect of Internal Hydrogen on the Fatigue Crack Growth Rate in the Coarse-Grain Heat-Affected Zone of a CrMo Steel
title_full_unstemmed Effect of Internal Hydrogen on the Fatigue Crack Growth Rate in the Coarse-Grain Heat-Affected Zone of a CrMo Steel
title_short Effect of Internal Hydrogen on the Fatigue Crack Growth Rate in the Coarse-Grain Heat-Affected Zone of a CrMo Steel
title_sort effect of internal hydrogen on the fatigue crack growth rate in the coarse grain heat affected zone of a crmo steel
topic hydrogen embrittlement
fatigue crack growth rate
pre-charged specimens
coarse grain heat affected zone
url https://www.mdpi.com/2075-4701/12/4/673
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