Preparation of nanodimensional CdS by chemical dipping technique and their characterization
A simple and cost effective chemical technique has been utilized to grow cadmium sulphide (CdS) nanoparticles at room temperature. The sample is characterized with XRD (X-ray diffractometer), SEM (Scanning electron microscope), TEM (Transmission electron microscope) and UV-VIS spectrophotometer. The...
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Format: | Article |
Language: | English |
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Associação Brasileira de Metalurgia e Materiais (ABM); Associação Brasileira de Cerâmica (ABC); Associação Brasileira de Polímeros (ABPol)
2011-03-01
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Series: | Materials Research |
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Online Access: | http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392011000100005 |
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author | Soumitra Patra Partha Mitra Swapan Kumar Pradhan |
author_facet | Soumitra Patra Partha Mitra Swapan Kumar Pradhan |
author_sort | Soumitra Patra |
collection | DOAJ |
description | A simple and cost effective chemical technique has been utilized to grow cadmium sulphide (CdS) nanoparticles at room temperature. The sample is characterized with XRD (X-ray diffractometer), SEM (Scanning electron microscope), TEM (Transmission electron microscope) and UV-VIS spectrophotometer. The particle size estimated using X-ray line broadening method is approximately 5 nm. Instrumental broadening was taken into account while particle size estimation. The lattice strain was evaluated using Williamson-Hall equation. SEM illustrates formation of sub-micron size crystallites and TEM image gives particle size approximately between 4-5 nm. Optical absorption study exhibits a band gap energy value of about 2.6 eV. |
first_indexed | 2024-12-20T04:31:15Z |
format | Article |
id | doaj.art-7af9bc716eba4c50a6843e81219e949f |
institution | Directory Open Access Journal |
issn | 1516-1439 |
language | English |
last_indexed | 2024-12-20T04:31:15Z |
publishDate | 2011-03-01 |
publisher | Associação Brasileira de Metalurgia e Materiais (ABM); Associação Brasileira de Cerâmica (ABC); Associação Brasileira de Polímeros (ABPol) |
record_format | Article |
series | Materials Research |
spelling | doaj.art-7af9bc716eba4c50a6843e81219e949f2022-12-21T19:53:23ZengAssociação Brasileira de Metalurgia e Materiais (ABM); Associação Brasileira de Cerâmica (ABC); Associação Brasileira de Polímeros (ABPol)Materials Research1516-14392011-03-011411720Preparation of nanodimensional CdS by chemical dipping technique and their characterizationSoumitra PatraPartha MitraSwapan Kumar PradhanA simple and cost effective chemical technique has been utilized to grow cadmium sulphide (CdS) nanoparticles at room temperature. The sample is characterized with XRD (X-ray diffractometer), SEM (Scanning electron microscope), TEM (Transmission electron microscope) and UV-VIS spectrophotometer. The particle size estimated using X-ray line broadening method is approximately 5 nm. Instrumental broadening was taken into account while particle size estimation. The lattice strain was evaluated using Williamson-Hall equation. SEM illustrates formation of sub-micron size crystallites and TEM image gives particle size approximately between 4-5 nm. Optical absorption study exhibits a band gap energy value of about 2.6 eV.http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392011000100005CdS thin filmchemical dippingparticle sizeoptical band gap |
spellingShingle | Soumitra Patra Partha Mitra Swapan Kumar Pradhan Preparation of nanodimensional CdS by chemical dipping technique and their characterization Materials Research CdS thin film chemical dipping particle size optical band gap |
title | Preparation of nanodimensional CdS by chemical dipping technique and their characterization |
title_full | Preparation of nanodimensional CdS by chemical dipping technique and their characterization |
title_fullStr | Preparation of nanodimensional CdS by chemical dipping technique and their characterization |
title_full_unstemmed | Preparation of nanodimensional CdS by chemical dipping technique and their characterization |
title_short | Preparation of nanodimensional CdS by chemical dipping technique and their characterization |
title_sort | preparation of nanodimensional cds by chemical dipping technique and their characterization |
topic | CdS thin film chemical dipping particle size optical band gap |
url | http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392011000100005 |
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