In Situ Testing of Polymers Immersed in Aging Fluids at Elevated Temperature and Pressure

A novel elevated-temperature and high-pressure in situ punch-shear-test cell was developed to qualify materials for reliable service in harsh environments representative of those typically encountered in oil and gas operations. The proposed modular and compact test device is an extension of the ASTM...

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Main Authors: Bo Xu, Mark Redmond, Ahmed Hammami, Pierre Mertiny
Format: Article
Language:English
Published: MDPI AG 2022-04-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/15/7/2690
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author Bo Xu
Mark Redmond
Ahmed Hammami
Pierre Mertiny
author_facet Bo Xu
Mark Redmond
Ahmed Hammami
Pierre Mertiny
author_sort Bo Xu
collection DOAJ
description A novel elevated-temperature and high-pressure in situ punch-shear-test cell was developed to qualify materials for reliable service in harsh environments representative of those typically encountered in oil and gas operations. The proposed modular and compact test device is an extension of the ASTM D 732 punch-shear method. Conventionally, materials are first exposed to harsh environments, then removed from the aging environment for mechanical testing. This practice can lead to the generation of unrealistic (often optimistic) mechanical properties. This is especially true in the case of materials for which fluid ingress is reversible. The present contribution elaborates on the developed in situ punch-shear device that has been successfully used to realistically assess the tensile yield strength and modulus properties of in-service polymer materials based on experimentally established correlations between shear and tensile tests.
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spelling doaj.art-7c210776eb1c4fa49e7fa94d2031f69c2023-11-30T23:35:37ZengMDPI AGMaterials1996-19442022-04-01157269010.3390/ma15072690In Situ Testing of Polymers Immersed in Aging Fluids at Elevated Temperature and PressureBo Xu0Mark Redmond1Ahmed Hammami2Pierre Mertiny3CAEVIS Technology Ltd., 31 Kingslake Rd., Toronto, ON M2J 3E2, CanadaShawcor Ltd., Corporate Research & Development, 25 Bethridge Rd., Toronto, ON M9W 1M7, CanadaShawcor Ltd., Composite Systems, 3501 54 Ave SE, Calgary, AB T2C 0A9, CanadaDepartment of Mechanical Engineering, University of Alberta, 9211-116 St., Edmonton, AB T6G 1H9, CanadaA novel elevated-temperature and high-pressure in situ punch-shear-test cell was developed to qualify materials for reliable service in harsh environments representative of those typically encountered in oil and gas operations. The proposed modular and compact test device is an extension of the ASTM D 732 punch-shear method. Conventionally, materials are first exposed to harsh environments, then removed from the aging environment for mechanical testing. This practice can lead to the generation of unrealistic (often optimistic) mechanical properties. This is especially true in the case of materials for which fluid ingress is reversible. The present contribution elaborates on the developed in situ punch-shear device that has been successfully used to realistically assess the tensile yield strength and modulus properties of in-service polymer materials based on experimentally established correlations between shear and tensile tests.https://www.mdpi.com/1996-1944/15/7/2690in situ material testingpolymerspunch-shear testmaterial aging and degradation
spellingShingle Bo Xu
Mark Redmond
Ahmed Hammami
Pierre Mertiny
In Situ Testing of Polymers Immersed in Aging Fluids at Elevated Temperature and Pressure
Materials
in situ material testing
polymers
punch-shear test
material aging and degradation
title In Situ Testing of Polymers Immersed in Aging Fluids at Elevated Temperature and Pressure
title_full In Situ Testing of Polymers Immersed in Aging Fluids at Elevated Temperature and Pressure
title_fullStr In Situ Testing of Polymers Immersed in Aging Fluids at Elevated Temperature and Pressure
title_full_unstemmed In Situ Testing of Polymers Immersed in Aging Fluids at Elevated Temperature and Pressure
title_short In Situ Testing of Polymers Immersed in Aging Fluids at Elevated Temperature and Pressure
title_sort in situ testing of polymers immersed in aging fluids at elevated temperature and pressure
topic in situ material testing
polymers
punch-shear test
material aging and degradation
url https://www.mdpi.com/1996-1944/15/7/2690
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