Microstructure and Micromechanical Behaviors of Bulk Amorphous Alloy Prepared by Spark Plasma Sintering
This study aimed to prepare Zr55Cu30Al10Ni5 bulk amorphous alloys by spark plasma sintering of raw amorphous alloy powders and investigate their microstructure and micromechanical behaviors. When the sintering temperature ( Ts) was 675K, which was lower than the glass transition temperature ( Tg) of...
Main Authors: | , , , |
---|---|
Format: | Article |
Language: | English |
Published: |
Polish Academy of Sciences
2023-03-01
|
Series: | Archives of Metallurgy and Materials |
Subjects: | |
Online Access: | https://journals.pan.pl/Content/126220/PDF/AMM-2023-1-04-Yaqiong%20Ge.pdf |
_version_ | 1827988790628581376 |
---|---|
author | Yaqiong Ge Zexin Chang Wenxian Wang Qingling Hou |
author_facet | Yaqiong Ge Zexin Chang Wenxian Wang Qingling Hou |
author_sort | Yaqiong Ge |
collection | DOAJ |
description | This study aimed to prepare Zr55Cu30Al10Ni5 bulk amorphous alloys by spark plasma sintering of raw amorphous alloy powders and investigate their microstructure and micromechanical behaviors. When the sintering temperature ( Ts) was 675K, which was lower than the glass transition temperature ( Tg) of the material, the sintered sample was almost fully amorphous but the density was lower. However, when Ts was 705K, which was higher than Tg, partial crystallization occurred, but the density was higher. The hardness of the bonding zone of the sintered sample at 675K was 5.291 GPa due to the lower density, which was lower than that at 705K, and the hardness at 705K was 8.836 GPa. The generation of thermodynamically stable intermetallic phases, the hardness, and the elastic modulus of the samples sintered above Tg were higher due to the higher density. |
first_indexed | 2024-04-10T00:08:57Z |
format | Article |
id | doaj.art-7c8df946e4c54b87aac7338cd3da2a19 |
institution | Directory Open Access Journal |
issn | 2300-1909 |
language | English |
last_indexed | 2024-04-10T00:08:57Z |
publishDate | 2023-03-01 |
publisher | Polish Academy of Sciences |
record_format | Article |
series | Archives of Metallurgy and Materials |
spelling | doaj.art-7c8df946e4c54b87aac7338cd3da2a192023-03-16T15:02:45ZengPolish Academy of SciencesArchives of Metallurgy and Materials2300-19092023-03-01vol. 68No 13136https://doi.org/10.24425/amm.2023.141468Microstructure and Micromechanical Behaviors of Bulk Amorphous Alloy Prepared by Spark Plasma SinteringYaqiong Ge0Zexin Chang1Wenxian Wang2Qingling Hou3Taiyuan University of Science and Technology, College of Materials Science and Engineering, Taiyuan 030024, ChinaTaiyuan University of Science and Technology, College of Materials Science and Engineering, Taiyuan 030024, ChinaTaiyuan University of Science and Technology, College of Materials Science and Engineering, Taiyuan 030024, ChinaTaiyuan University of Science and Technology, College of Materials Science and Engineering, Taiyuan 030024, ChinaThis study aimed to prepare Zr55Cu30Al10Ni5 bulk amorphous alloys by spark plasma sintering of raw amorphous alloy powders and investigate their microstructure and micromechanical behaviors. When the sintering temperature ( Ts) was 675K, which was lower than the glass transition temperature ( Tg) of the material, the sintered sample was almost fully amorphous but the density was lower. However, when Ts was 705K, which was higher than Tg, partial crystallization occurred, but the density was higher. The hardness of the bonding zone of the sintered sample at 675K was 5.291 GPa due to the lower density, which was lower than that at 705K, and the hardness at 705K was 8.836 GPa. The generation of thermodynamically stable intermetallic phases, the hardness, and the elastic modulus of the samples sintered above Tg were higher due to the higher density.https://journals.pan.pl/Content/126220/PDF/AMM-2023-1-04-Yaqiong%20Ge.pdfbulk amorphous alloyspark plasma sintering (sps)microstructuremicromechanical behaviors |
spellingShingle | Yaqiong Ge Zexin Chang Wenxian Wang Qingling Hou Microstructure and Micromechanical Behaviors of Bulk Amorphous Alloy Prepared by Spark Plasma Sintering Archives of Metallurgy and Materials bulk amorphous alloy spark plasma sintering (sps) microstructure micromechanical behaviors |
title | Microstructure and Micromechanical Behaviors of Bulk Amorphous Alloy Prepared by Spark Plasma Sintering |
title_full | Microstructure and Micromechanical Behaviors of Bulk Amorphous Alloy Prepared by Spark Plasma Sintering |
title_fullStr | Microstructure and Micromechanical Behaviors of Bulk Amorphous Alloy Prepared by Spark Plasma Sintering |
title_full_unstemmed | Microstructure and Micromechanical Behaviors of Bulk Amorphous Alloy Prepared by Spark Plasma Sintering |
title_short | Microstructure and Micromechanical Behaviors of Bulk Amorphous Alloy Prepared by Spark Plasma Sintering |
title_sort | microstructure and micromechanical behaviors of bulk amorphous alloy prepared by spark plasma sintering |
topic | bulk amorphous alloy spark plasma sintering (sps) microstructure micromechanical behaviors |
url | https://journals.pan.pl/Content/126220/PDF/AMM-2023-1-04-Yaqiong%20Ge.pdf |
work_keys_str_mv | AT yaqiongge microstructureandmicromechanicalbehaviorsofbulkamorphousalloypreparedbysparkplasmasintering AT zexinchang microstructureandmicromechanicalbehaviorsofbulkamorphousalloypreparedbysparkplasmasintering AT wenxianwang microstructureandmicromechanicalbehaviorsofbulkamorphousalloypreparedbysparkplasmasintering AT qinglinghou microstructureandmicromechanicalbehaviorsofbulkamorphousalloypreparedbysparkplasmasintering |