Preparation and Application of Nickel Electroplating on Copper (Ni/EC) Electrode for Glucose Detection

An electrode of the nickel electroplating on copper (Ni/EC) has been prepared for a simple and low cost glucose sensor in human urine detection. The electrode was prepared by using pure copper (99.9%) with electroplating method in NiSO4 solution. The electrochemical oxidation of Ni/EC electrode was...

Full description

Bibliographic Details
Main Authors: Muh. Supwatul Hakim, Haryoko Pangestu, Riyanto
Format: Article
Language:English
Published: Magister Program of Material Sciences, Graduate School of Universitas Sriwijaya 2022-04-01
Series:Science and Technology Indonesia
Subjects:
Online Access:https://sciencetechindonesia.com/index.php/jsti/article/view/416
_version_ 1797285805066027008
author Muh. Supwatul Hakim
Haryoko Pangestu
Riyanto
author_facet Muh. Supwatul Hakim
Haryoko Pangestu
Riyanto
author_sort Muh. Supwatul Hakim
collection DOAJ
description An electrode of the nickel electroplating on copper (Ni/EC) has been prepared for a simple and low cost glucose sensor in human urine detection. The electrode was prepared by using pure copper (99.9%) with electroplating method in NiSO4 solution. The electrochemical oxidation of Ni/EC electrode was investigated bys using cyclic voltammetry method. Material Ni/EC identification of morphology used Scanning Electron Magnetic (SEM) and Energy Dispersive X-Ray (EDX). The electrochemical reaction of glucose was analyzed by the cyclic voltammetry method in some electrolyte solutions. Calibration curved was constructed and a linear response for glucose concentration at range 0-0.004 M with R2 = 0.992, LOD and LOQ was determined 4.85x10−4 M, 1.6x10−3 respectively. The proposed electrode might open up a new possibility for the determination of glucose concentration in human urine. Its advantages are simple to prepare, low cost analyzing, and excellent results.
first_indexed 2024-03-07T18:08:41Z
format Article
id doaj.art-7d8f1164e19648dab2ad7345ffa53cdd
institution Directory Open Access Journal
issn 2580-4405
2580-4391
language English
last_indexed 2024-03-07T18:08:41Z
publishDate 2022-04-01
publisher Magister Program of Material Sciences, Graduate School of Universitas Sriwijaya
record_format Article
series Science and Technology Indonesia
spelling doaj.art-7d8f1164e19648dab2ad7345ffa53cdd2024-03-02T08:06:14ZengMagister Program of Material Sciences, Graduate School of Universitas SriwijayaScience and Technology Indonesia2580-44052580-43912022-04-017220821210.26554/sti.2022.7.2.208-212Preparation and Application of Nickel Electroplating on Copper (Ni/EC) Electrode for Glucose DetectionMuh. Supwatul Hakim 0Haryoko Pangestu 1Riyanto 2Department of Chemistry, Faculty of Mathematics and Natural Sciences, Islamic University of Indonesia, Yogyakarta, 55584, IndonesiaDepartment of Chemistry, Faculty of Mathematics and Natural Sciences, Islamic University of Indonesia, Yogyakarta, 55584, IndonesiaDepartment of Chemistry, Faculty of Mathematics and Natural Sciences, Islamic University of Indonesia, Yogyakarta, 55584, IndonesiaAn electrode of the nickel electroplating on copper (Ni/EC) has been prepared for a simple and low cost glucose sensor in human urine detection. The electrode was prepared by using pure copper (99.9%) with electroplating method in NiSO4 solution. The electrochemical oxidation of Ni/EC electrode was investigated bys using cyclic voltammetry method. Material Ni/EC identification of morphology used Scanning Electron Magnetic (SEM) and Energy Dispersive X-Ray (EDX). The electrochemical reaction of glucose was analyzed by the cyclic voltammetry method in some electrolyte solutions. Calibration curved was constructed and a linear response for glucose concentration at range 0-0.004 M with R2 = 0.992, LOD and LOQ was determined 4.85x10−4 M, 1.6x10−3 respectively. The proposed electrode might open up a new possibility for the determination of glucose concentration in human urine. Its advantages are simple to prepare, low cost analyzing, and excellent results.https://sciencetechindonesia.com/index.php/jsti/article/view/416glucoseelectroplatinghuman urine
spellingShingle Muh. Supwatul Hakim
Haryoko Pangestu
Riyanto
Preparation and Application of Nickel Electroplating on Copper (Ni/EC) Electrode for Glucose Detection
Science and Technology Indonesia
glucose
electroplating
human urine
title Preparation and Application of Nickel Electroplating on Copper (Ni/EC) Electrode for Glucose Detection
title_full Preparation and Application of Nickel Electroplating on Copper (Ni/EC) Electrode for Glucose Detection
title_fullStr Preparation and Application of Nickel Electroplating on Copper (Ni/EC) Electrode for Glucose Detection
title_full_unstemmed Preparation and Application of Nickel Electroplating on Copper (Ni/EC) Electrode for Glucose Detection
title_short Preparation and Application of Nickel Electroplating on Copper (Ni/EC) Electrode for Glucose Detection
title_sort preparation and application of nickel electroplating on copper ni ec electrode for glucose detection
topic glucose
electroplating
human urine
url https://sciencetechindonesia.com/index.php/jsti/article/view/416
work_keys_str_mv AT muhsupwatulhakim preparationandapplicationofnickelelectroplatingoncopperniecelectrodeforglucosedetection
AT haryokopangestu preparationandapplicationofnickelelectroplatingoncopperniecelectrodeforglucosedetection
AT riyanto preparationandapplicationofnickelelectroplatingoncopperniecelectrodeforglucosedetection