3-Methyl-1-phenyl-4-thioacetylpyrazol-5-one
The novel compound 3-methyl-1-phenyl-4-thioacetylpyrazol-5-one is obtained in excellent yield via a thionation of the corresponding oxygen analogue. The product is isolated in pure form using column chromatography and is characterised using 1D and 2D NMR experiments, ATR IR and HRMS spectra, and sin...
| Main Authors: | , , , |
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| Format: | Article |
| Language: | English |
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MDPI AG
2023-02-01
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| Series: | Molbank |
| Subjects: | |
| Online Access: | https://www.mdpi.com/1422-8599/2023/1/M1588 |
| _version_ | 1797609924766728192 |
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| author | Zhanina Petkova Rusi Rusew Boris Shivachev Vanya Kurteva |
| author_facet | Zhanina Petkova Rusi Rusew Boris Shivachev Vanya Kurteva |
| author_sort | Zhanina Petkova |
| collection | DOAJ |
| description | The novel compound 3-methyl-1-phenyl-4-thioacetylpyrazol-5-one is obtained in excellent yield via a thionation of the corresponding oxygen analogue. The product is isolated in pure form using column chromatography and is characterised using 1D and 2D NMR experiments, ATR IR and HRMS spectra, and single-crystal XRD. |
| first_indexed | 2024-03-11T06:08:23Z |
| format | Article |
| id | doaj.art-7dc0e0b8fe684d0ca7699a87998282e2 |
| institution | Directory Open Access Journal |
| issn | 1422-8599 |
| language | English |
| last_indexed | 2024-03-11T06:08:23Z |
| publishDate | 2023-02-01 |
| publisher | MDPI AG |
| record_format | Article |
| series | Molbank |
| spelling | doaj.art-7dc0e0b8fe684d0ca7699a87998282e22023-11-17T12:49:49ZengMDPI AGMolbank1422-85992023-02-0120231M158810.3390/M15883-Methyl-1-phenyl-4-thioacetylpyrazol-5-oneZhanina Petkova0Rusi Rusew1Boris Shivachev2Vanya Kurteva3Institute of Organic Chemistry with Centre of Phytochemistry, Bulgarian Academy of Sciences, Acad. G. Bonchev Street, bl. 9, 1113 Sofia, BulgariaInstitute of Mineralogy and Crystallography “Acad. Ivan Kostov”, Bulgarian Academy of Sciences, Acad. G. Bonchev Street, bl. 107, 1113 Sofia, BulgariaInstitute of Mineralogy and Crystallography “Acad. Ivan Kostov”, Bulgarian Academy of Sciences, Acad. G. Bonchev Street, bl. 107, 1113 Sofia, BulgariaInstitute of Organic Chemistry with Centre of Phytochemistry, Bulgarian Academy of Sciences, Acad. G. Bonchev Street, bl. 9, 1113 Sofia, BulgariaThe novel compound 3-methyl-1-phenyl-4-thioacetylpyrazol-5-one is obtained in excellent yield via a thionation of the corresponding oxygen analogue. The product is isolated in pure form using column chromatography and is characterised using 1D and 2D NMR experiments, ATR IR and HRMS spectra, and single-crystal XRD.https://www.mdpi.com/1422-8599/2023/1/M15883-methyl-1-phenyl-4-thioacetylpyrazol-5-oneacylpyrazoloneNMRsingle-crystal XRD |
| spellingShingle | Zhanina Petkova Rusi Rusew Boris Shivachev Vanya Kurteva 3-Methyl-1-phenyl-4-thioacetylpyrazol-5-one Molbank 3-methyl-1-phenyl-4-thioacetylpyrazol-5-one acylpyrazolone NMR single-crystal XRD |
| title | 3-Methyl-1-phenyl-4-thioacetylpyrazol-5-one |
| title_full | 3-Methyl-1-phenyl-4-thioacetylpyrazol-5-one |
| title_fullStr | 3-Methyl-1-phenyl-4-thioacetylpyrazol-5-one |
| title_full_unstemmed | 3-Methyl-1-phenyl-4-thioacetylpyrazol-5-one |
| title_short | 3-Methyl-1-phenyl-4-thioacetylpyrazol-5-one |
| title_sort | 3 methyl 1 phenyl 4 thioacetylpyrazol 5 one |
| topic | 3-methyl-1-phenyl-4-thioacetylpyrazol-5-one acylpyrazolone NMR single-crystal XRD |
| url | https://www.mdpi.com/1422-8599/2023/1/M1588 |
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