Simulation-Assisted Process Design and Experimental Verification of Laterally Confined Oxide Areas Generated with Continuous Electrolytic Free Jet on EN AW-7075 Aluminum Alloy

Local anodization with a free electrolyte jet is a suitable solution for locally confined surface functionalization without additionally required preparation of the parts. However, the geometrical formation of the anodic oxide layer in jet-based anodization is not yet sufficiently understood. In thi...

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Main Authors: Susanne Quitzke, Igor Danilov, André Martin, Roy Morgenstern, Thomas Lampke, Andreas Schubert
Format: Article
Language:English
Published: MDPI AG 2023-01-01
Series:Micromachines
Subjects:
Online Access:https://www.mdpi.com/2072-666X/14/2/293
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author Susanne Quitzke
Igor Danilov
André Martin
Roy Morgenstern
Thomas Lampke
Andreas Schubert
author_facet Susanne Quitzke
Igor Danilov
André Martin
Roy Morgenstern
Thomas Lampke
Andreas Schubert
author_sort Susanne Quitzke
collection DOAJ
description Local anodization with a free electrolyte jet is a suitable solution for locally confined surface functionalization without additionally required preparation of the parts. However, the geometrical formation of the anodic oxide layer in jet-based anodization is not yet sufficiently understood. In this study, numerical calculations based on physical descriptions are used to describe the lateral and vertical oxide formation on aluminum alloy EN AW-7075. The required electrical resistance and capacitance were determined by immersion-based anodization and implemented into the numerical simulation model to evaluate the electrical conductivity of the porous layer. The simulation results showed an electrical conductivity of 2.6 × 10<sup>−6</sup> S/m for the porous layer. Subsequently, a model for jet-based anodization was developed and the previous results were implemented to calculate the oxide formation. The simulation results showed decreasing oxide layer thickness at increasing radial distance from the center of the jet, which corresponds to experimental results. The simulation model was validated by varying the current efficiency from 5% to 90%, where similar developments of the anodic oxide layer thickness compared with experimental results were determined at 5%.
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spelling doaj.art-7de1dcfe9ec34a8b966b98d1f5ad1a7b2023-11-16T22:10:12ZengMDPI AGMicromachines2072-666X2023-01-0114229310.3390/mi14020293Simulation-Assisted Process Design and Experimental Verification of Laterally Confined Oxide Areas Generated with Continuous Electrolytic Free Jet on EN AW-7075 Aluminum AlloySusanne Quitzke0Igor Danilov1André Martin2Roy Morgenstern3Thomas Lampke4Andreas Schubert5Professorship Micromanufacturing Technology, Faculty of Mechanical Engineering, Chemnitz University of Technology, 09107 Chemnitz, GermanyProfessorship Micromanufacturing Technology, Faculty of Mechanical Engineering, Chemnitz University of Technology, 09107 Chemnitz, GermanyProfessorship Micromanufacturing Technology, Faculty of Mechanical Engineering, Chemnitz University of Technology, 09107 Chemnitz, GermanyMaterials and Surface Engineering, Faculty of Mechanical Engineering, Chemnitz University of Technology, 09107 Chemnitz, GermanyMaterials and Surface Engineering, Faculty of Mechanical Engineering, Chemnitz University of Technology, 09107 Chemnitz, GermanyProfessorship Micromanufacturing Technology, Faculty of Mechanical Engineering, Chemnitz University of Technology, 09107 Chemnitz, GermanyLocal anodization with a free electrolyte jet is a suitable solution for locally confined surface functionalization without additionally required preparation of the parts. However, the geometrical formation of the anodic oxide layer in jet-based anodization is not yet sufficiently understood. In this study, numerical calculations based on physical descriptions are used to describe the lateral and vertical oxide formation on aluminum alloy EN AW-7075. The required electrical resistance and capacitance were determined by immersion-based anodization and implemented into the numerical simulation model to evaluate the electrical conductivity of the porous layer. The simulation results showed an electrical conductivity of 2.6 × 10<sup>−6</sup> S/m for the porous layer. Subsequently, a model for jet-based anodization was developed and the previous results were implemented to calculate the oxide formation. The simulation results showed decreasing oxide layer thickness at increasing radial distance from the center of the jet, which corresponds to experimental results. The simulation model was validated by varying the current efficiency from 5% to 90%, where similar developments of the anodic oxide layer thickness compared with experimental results were determined at 5%.https://www.mdpi.com/2072-666X/14/2/293localized mask-less anodizationlocal functionalizationoxide layer formationfree electrolyte jetelectrodynamic simulation
spellingShingle Susanne Quitzke
Igor Danilov
André Martin
Roy Morgenstern
Thomas Lampke
Andreas Schubert
Simulation-Assisted Process Design and Experimental Verification of Laterally Confined Oxide Areas Generated with Continuous Electrolytic Free Jet on EN AW-7075 Aluminum Alloy
Micromachines
localized mask-less anodization
local functionalization
oxide layer formation
free electrolyte jet
electrodynamic simulation
title Simulation-Assisted Process Design and Experimental Verification of Laterally Confined Oxide Areas Generated with Continuous Electrolytic Free Jet on EN AW-7075 Aluminum Alloy
title_full Simulation-Assisted Process Design and Experimental Verification of Laterally Confined Oxide Areas Generated with Continuous Electrolytic Free Jet on EN AW-7075 Aluminum Alloy
title_fullStr Simulation-Assisted Process Design and Experimental Verification of Laterally Confined Oxide Areas Generated with Continuous Electrolytic Free Jet on EN AW-7075 Aluminum Alloy
title_full_unstemmed Simulation-Assisted Process Design and Experimental Verification of Laterally Confined Oxide Areas Generated with Continuous Electrolytic Free Jet on EN AW-7075 Aluminum Alloy
title_short Simulation-Assisted Process Design and Experimental Verification of Laterally Confined Oxide Areas Generated with Continuous Electrolytic Free Jet on EN AW-7075 Aluminum Alloy
title_sort simulation assisted process design and experimental verification of laterally confined oxide areas generated with continuous electrolytic free jet on en aw 7075 aluminum alloy
topic localized mask-less anodization
local functionalization
oxide layer formation
free electrolyte jet
electrodynamic simulation
url https://www.mdpi.com/2072-666X/14/2/293
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