Measurement of Effects of Different Substrates on the Mechanical Properties of Submicron Titanium Nickel Shape Memory Alloy Thin Film Using the Bulge Test

This study investigated the effects of different substrates on the mechanical properties of Ti-60at%Ni shape memory alloys (SMA). Two types of samples were prepared for this experiment: (1) a Ti-60at%Ni deposited on SiNx, and (2) a Ti-60at%Ni deposited on SiNx/Cr; both had a 600 nm thick film of Ti-...

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Main Authors: Nhat Minh Dang, Zhao-Ying Wang, Ti-Yuan Wu, Tra Anh Khoa Nguyen, Ming-Tzer Lin
Format: Article
Language:English
Published: MDPI AG 2021-01-01
Series:Micromachines
Subjects:
Online Access:https://www.mdpi.com/2072-666X/12/1/85
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author Nhat Minh Dang
Zhao-Ying Wang
Ti-Yuan Wu
Tra Anh Khoa Nguyen
Ming-Tzer Lin
author_facet Nhat Minh Dang
Zhao-Ying Wang
Ti-Yuan Wu
Tra Anh Khoa Nguyen
Ming-Tzer Lin
author_sort Nhat Minh Dang
collection DOAJ
description This study investigated the effects of different substrates on the mechanical properties of Ti-60at%Ni shape memory alloys (SMA). Two types of samples were prepared for this experiment: (1) a Ti-60at%Ni deposited on SiNx, and (2) a Ti-60at%Ni deposited on SiNx/Cr; both had a 600 nm thick film of Ti-60at%Ni. Deposition was done using the physical vapor deposition (PVD) process, and the microstructural changes and crystallization phase changes were observed through scanning electron microscopy (SEM) and X-ray diffraction (XRD). The results showed that the TiNi thin film with a Cr adhesion layer had better mechanical properties. The bulge test showed that TiNi thin film with a Cr adhesion had a higher Young’s modulus and lower residual stress. From the thermal cycling experiment, it was found that the Cr adhesion layer buffered the mismatch between TiNi and SiNx. Additionally, the thermal cycling test was also used to measure the thermal expansion coefficient of the films, and the fatigue test showed that the Cr layer significantly improved the fatigue resistance of the TiNi film.
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spelling doaj.art-7de3e2ca03ae4d36aed234594465a9c72023-12-03T13:27:00ZengMDPI AGMicromachines2072-666X2021-01-011218510.3390/mi12010085Measurement of Effects of Different Substrates on the Mechanical Properties of Submicron Titanium Nickel Shape Memory Alloy Thin Film Using the Bulge TestNhat Minh Dang0Zhao-Ying Wang1Ti-Yuan Wu2Tra Anh Khoa Nguyen3Ming-Tzer Lin4Graduate Institute of Precision Engineering, National Chung Hsing University Taichung, Taichung 40749, TaiwanGraduate Institute of Precision Engineering, National Chung Hsing University Taichung, Taichung 40749, TaiwanGraduate Institute of Precision Engineering, National Chung Hsing University Taichung, Taichung 40749, TaiwanGraduate Institute of Precision Engineering, National Chung Hsing University Taichung, Taichung 40749, TaiwanGraduate Institute of Precision Engineering, National Chung Hsing University Taichung, Taichung 40749, TaiwanThis study investigated the effects of different substrates on the mechanical properties of Ti-60at%Ni shape memory alloys (SMA). Two types of samples were prepared for this experiment: (1) a Ti-60at%Ni deposited on SiNx, and (2) a Ti-60at%Ni deposited on SiNx/Cr; both had a 600 nm thick film of Ti-60at%Ni. Deposition was done using the physical vapor deposition (PVD) process, and the microstructural changes and crystallization phase changes were observed through scanning electron microscopy (SEM) and X-ray diffraction (XRD). The results showed that the TiNi thin film with a Cr adhesion layer had better mechanical properties. The bulge test showed that TiNi thin film with a Cr adhesion had a higher Young’s modulus and lower residual stress. From the thermal cycling experiment, it was found that the Cr adhesion layer buffered the mismatch between TiNi and SiNx. Additionally, the thermal cycling test was also used to measure the thermal expansion coefficient of the films, and the fatigue test showed that the Cr layer significantly improved the fatigue resistance of the TiNi film.https://www.mdpi.com/2072-666X/12/1/85shape memory alloysbulge testCr adhesion layerresidual stress
spellingShingle Nhat Minh Dang
Zhao-Ying Wang
Ti-Yuan Wu
Tra Anh Khoa Nguyen
Ming-Tzer Lin
Measurement of Effects of Different Substrates on the Mechanical Properties of Submicron Titanium Nickel Shape Memory Alloy Thin Film Using the Bulge Test
Micromachines
shape memory alloys
bulge test
Cr adhesion layer
residual stress
title Measurement of Effects of Different Substrates on the Mechanical Properties of Submicron Titanium Nickel Shape Memory Alloy Thin Film Using the Bulge Test
title_full Measurement of Effects of Different Substrates on the Mechanical Properties of Submicron Titanium Nickel Shape Memory Alloy Thin Film Using the Bulge Test
title_fullStr Measurement of Effects of Different Substrates on the Mechanical Properties of Submicron Titanium Nickel Shape Memory Alloy Thin Film Using the Bulge Test
title_full_unstemmed Measurement of Effects of Different Substrates on the Mechanical Properties of Submicron Titanium Nickel Shape Memory Alloy Thin Film Using the Bulge Test
title_short Measurement of Effects of Different Substrates on the Mechanical Properties of Submicron Titanium Nickel Shape Memory Alloy Thin Film Using the Bulge Test
title_sort measurement of effects of different substrates on the mechanical properties of submicron titanium nickel shape memory alloy thin film using the bulge test
topic shape memory alloys
bulge test
Cr adhesion layer
residual stress
url https://www.mdpi.com/2072-666X/12/1/85
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