In-situ interstitial alloying during laser powder bed fusion of AISI 316 for superior corrosion resistance

The present work explores for the first time additive manufacturing of powder mixtures consisting of Chromium Nitride (Cr2N) and AISI 316L with laser powder bed fusion (L-PBF). The addition of 2.5 wt% Cr2N to an AISI 316L powder resulted in the successful dissolution of both chromium and nitrogen in...

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Main Authors: Emilie Hørdum Valente, Venkata Karthik Nadimpalli, Thomas L. Christiansen, David Bue Pedersen, Marcel A.J. Somers
Format: Article
Language:English
Published: Elsevier 2021-12-01
Series:Additive Manufacturing Letters
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2772369021000062
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author Emilie Hørdum Valente
Venkata Karthik Nadimpalli
Thomas L. Christiansen
David Bue Pedersen
Marcel A.J. Somers
author_facet Emilie Hørdum Valente
Venkata Karthik Nadimpalli
Thomas L. Christiansen
David Bue Pedersen
Marcel A.J. Somers
author_sort Emilie Hørdum Valente
collection DOAJ
description The present work explores for the first time additive manufacturing of powder mixtures consisting of Chromium Nitride (Cr2N) and AISI 316L with laser powder bed fusion (L-PBF). The addition of 2.5 wt% Cr2N to an AISI 316L powder resulted in the successful dissolution of both chromium and nitrogen into a fully austenitic stainless steel microstructure. The nitrogen content was augmented from 0.09 wt% in the as-delivered AISI 316L powder to 0.31 wt% in the L-PBF built part, causing a slight expansion of the austenite lattice. Elongated austenite grains with an internal cellular substructure were obtained in both the Cr2N modified 316L and the 316L specimens manufactured by L-PBF. The addition of nitrogen (and chromium) from Cr2N resulted in a Vickers hardness increase of about 40 HV0.1, mainly by interstitial solid solution strengthening. The modification of 316L by the addition of Cr2N significantly improved the corrosion resistance. The improved hardness and corrosion resistance while retaining the manufacturability and cellular microstructure illustrate the potential for modifying the composition and properties of L-PBF 316L with targeted dosing with Cr2N powders.
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spelling doaj.art-7ea0d6c69f014ec78ac96d424d6ed5982022-12-21T18:11:55ZengElsevierAdditive Manufacturing Letters2772-36902021-12-011100006In-situ interstitial alloying during laser powder bed fusion of AISI 316 for superior corrosion resistanceEmilie Hørdum Valente0Venkata Karthik Nadimpalli1Thomas L. Christiansen2David Bue Pedersen3Marcel A.J. Somers4Corresponding author.; Technical University of Denmark, Department of Mechanical Engineering, 2800 Kgs. Lyngby, DenmarkTechnical University of Denmark, Department of Mechanical Engineering, 2800 Kgs. Lyngby, DenmarkTechnical University of Denmark, Department of Mechanical Engineering, 2800 Kgs. Lyngby, DenmarkTechnical University of Denmark, Department of Mechanical Engineering, 2800 Kgs. Lyngby, DenmarkTechnical University of Denmark, Department of Mechanical Engineering, 2800 Kgs. Lyngby, DenmarkThe present work explores for the first time additive manufacturing of powder mixtures consisting of Chromium Nitride (Cr2N) and AISI 316L with laser powder bed fusion (L-PBF). The addition of 2.5 wt% Cr2N to an AISI 316L powder resulted in the successful dissolution of both chromium and nitrogen into a fully austenitic stainless steel microstructure. The nitrogen content was augmented from 0.09 wt% in the as-delivered AISI 316L powder to 0.31 wt% in the L-PBF built part, causing a slight expansion of the austenite lattice. Elongated austenite grains with an internal cellular substructure were obtained in both the Cr2N modified 316L and the 316L specimens manufactured by L-PBF. The addition of nitrogen (and chromium) from Cr2N resulted in a Vickers hardness increase of about 40 HV0.1, mainly by interstitial solid solution strengthening. The modification of 316L by the addition of Cr2N significantly improved the corrosion resistance. The improved hardness and corrosion resistance while retaining the manufacturability and cellular microstructure illustrate the potential for modifying the composition and properties of L-PBF 316L with targeted dosing with Cr2N powders.http://www.sciencedirect.com/science/article/pii/S2772369021000062Austenitic stainless steel316LChromium nitrideL-PBFCorrosion resistanceAdditive manufacturing
spellingShingle Emilie Hørdum Valente
Venkata Karthik Nadimpalli
Thomas L. Christiansen
David Bue Pedersen
Marcel A.J. Somers
In-situ interstitial alloying during laser powder bed fusion of AISI 316 for superior corrosion resistance
Additive Manufacturing Letters
Austenitic stainless steel
316L
Chromium nitride
L-PBF
Corrosion resistance
Additive manufacturing
title In-situ interstitial alloying during laser powder bed fusion of AISI 316 for superior corrosion resistance
title_full In-situ interstitial alloying during laser powder bed fusion of AISI 316 for superior corrosion resistance
title_fullStr In-situ interstitial alloying during laser powder bed fusion of AISI 316 for superior corrosion resistance
title_full_unstemmed In-situ interstitial alloying during laser powder bed fusion of AISI 316 for superior corrosion resistance
title_short In-situ interstitial alloying during laser powder bed fusion of AISI 316 for superior corrosion resistance
title_sort in situ interstitial alloying during laser powder bed fusion of aisi 316 for superior corrosion resistance
topic Austenitic stainless steel
316L
Chromium nitride
L-PBF
Corrosion resistance
Additive manufacturing
url http://www.sciencedirect.com/science/article/pii/S2772369021000062
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AT davidbuepedersen insituinterstitialalloyingduringlaserpowderbedfusionofaisi316forsuperiorcorrosionresistance
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