Influence of banded ε-martensite and deformation twin on cryogenic toughness of Fe–Mn–xAl–C steel

Fe–Mn–xAl–C steel ingots have been fabricated by vacuum melting with Al compositions varied from x = 0 to 3 and 5 wt.%, respectively. After properly hot-forging and hot-rolling as well as solution heat treatments, impact toughness tests were carried out at 77 K using a standard full-size of Charpy i...

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Main Authors: Leilei Li, Gang Niu, Na Gong, Hongfei Liu, Xuelin Wang, Chengjia Shang, Yong Wang, Huibin Wu
Format: Article
Language:English
Published: Elsevier 2023-11-01
Series:Journal of Materials Research and Technology
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2238785423023815
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author Leilei Li
Gang Niu
Na Gong
Hongfei Liu
Xuelin Wang
Chengjia Shang
Yong Wang
Huibin Wu
author_facet Leilei Li
Gang Niu
Na Gong
Hongfei Liu
Xuelin Wang
Chengjia Shang
Yong Wang
Huibin Wu
author_sort Leilei Li
collection DOAJ
description Fe–Mn–xAl–C steel ingots have been fabricated by vacuum melting with Al compositions varied from x = 0 to 3 and 5 wt.%, respectively. After properly hot-forging and hot-rolling as well as solution heat treatments, impact toughness tests were carried out at 77 K using a standard full-size of Charpy impact V-notch configuration. It was found that the addition of Al element is more conducive to enhance the cryogenic toughness. The relationship between the cryogenic toughness and the Al composition has been revealed through detailed microstructural studies by electron back scatter diffraction and transmission-electron microscopy. The stack fault energy (SFE) increases with the increase of Al content at various temperature. The plastic deformation is dominated by deformation bands which are dominated by deformation twins (DTs) and ε-martensite at x = 0 and DTs at x = 3 and 5%, respectively. The DTs near fracture the notch-tip area increased in the order of the 0Al, 3Al, and 5Al steel. The DTs with high density, together with their contented dislocations, significantly contributed to the high cryogenic toughness of the studied high manganese steel with higher Al content. Banded ε-martensite will deterioration cryogenic toughness due to its large size compared to DTs at 0Al steel.
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spelling doaj.art-7ed7f88b80c24ce2b5bd21206df386b12024-02-21T05:25:14ZengElsevierJournal of Materials Research and Technology2238-78542023-11-0127262271Influence of banded ε-martensite and deformation twin on cryogenic toughness of Fe–Mn–xAl–C steelLeilei Li0Gang Niu1Na Gong2Hongfei Liu3Xuelin Wang4Chengjia Shang5Yong Wang6Huibin Wu7Collaborative Innovation Center of Steel Technology, University of Science and Technology Beijing 100083, ChinaCollaborative Innovation Center of Steel Technology, University of Science and Technology Beijing 100083, China; Yangjiang Branch, Guangdong Laboratory for Materials Science and Technology (Yangjiang Advanced Alloys Laboratory), Yangjiang, Guangdong 529500, China; Corresponding author. Yangjiang Branch, Guangdong Laboratory for Materials Science and Technology (Yangjiang Advanced Alloys Laboratory), Yangjiang, Guangdong 529500, China.Institute of Materials Research and Engineering (IMRE), A∗STAR (Agency for Science, Technology and Research), Singapore 138634, SingaporeInstitute of Materials Research and Engineering (IMRE), A∗STAR (Agency for Science, Technology and Research), Singapore 138634, SingaporeCollaborative Innovation Center of Steel Technology, University of Science and Technology Beijing 100083, China; Yangjiang Branch, Guangdong Laboratory for Materials Science and Technology (Yangjiang Advanced Alloys Laboratory), Yangjiang, Guangdong 529500, ChinaCollaborative Innovation Center of Steel Technology, University of Science and Technology Beijing 100083, China; Yangjiang Branch, Guangdong Laboratory for Materials Science and Technology (Yangjiang Advanced Alloys Laboratory), Yangjiang, Guangdong 529500, ChinaSchool of Materials Science and Engineering, Nanyang Technological University, Singapore 639798, SingaporeCollaborative Innovation Center of Steel Technology, University of Science and Technology Beijing 100083, China; Yangjiang Branch, Guangdong Laboratory for Materials Science and Technology (Yangjiang Advanced Alloys Laboratory), Yangjiang, Guangdong 529500, China; Corresponding author. Collaborative Innovation Center of Steel Technology, University of Science and Technology Beijing 100083, China.Fe–Mn–xAl–C steel ingots have been fabricated by vacuum melting with Al compositions varied from x = 0 to 3 and 5 wt.%, respectively. After properly hot-forging and hot-rolling as well as solution heat treatments, impact toughness tests were carried out at 77 K using a standard full-size of Charpy impact V-notch configuration. It was found that the addition of Al element is more conducive to enhance the cryogenic toughness. The relationship between the cryogenic toughness and the Al composition has been revealed through detailed microstructural studies by electron back scatter diffraction and transmission-electron microscopy. The stack fault energy (SFE) increases with the increase of Al content at various temperature. The plastic deformation is dominated by deformation bands which are dominated by deformation twins (DTs) and ε-martensite at x = 0 and DTs at x = 3 and 5%, respectively. The DTs near fracture the notch-tip area increased in the order of the 0Al, 3Al, and 5Al steel. The DTs with high density, together with their contented dislocations, significantly contributed to the high cryogenic toughness of the studied high manganese steel with higher Al content. Banded ε-martensite will deterioration cryogenic toughness due to its large size compared to DTs at 0Al steel.http://www.sciencedirect.com/science/article/pii/S2238785423023815Fe–Mn–Al–C steelε-martensiteCryogenic toughnessDeformation twin
spellingShingle Leilei Li
Gang Niu
Na Gong
Hongfei Liu
Xuelin Wang
Chengjia Shang
Yong Wang
Huibin Wu
Influence of banded ε-martensite and deformation twin on cryogenic toughness of Fe–Mn–xAl–C steel
Journal of Materials Research and Technology
Fe–Mn–Al–C steel
ε-martensite
Cryogenic toughness
Deformation twin
title Influence of banded ε-martensite and deformation twin on cryogenic toughness of Fe–Mn–xAl–C steel
title_full Influence of banded ε-martensite and deformation twin on cryogenic toughness of Fe–Mn–xAl–C steel
title_fullStr Influence of banded ε-martensite and deformation twin on cryogenic toughness of Fe–Mn–xAl–C steel
title_full_unstemmed Influence of banded ε-martensite and deformation twin on cryogenic toughness of Fe–Mn–xAl–C steel
title_short Influence of banded ε-martensite and deformation twin on cryogenic toughness of Fe–Mn–xAl–C steel
title_sort influence of banded ε martensite and deformation twin on cryogenic toughness of fe mn xal c steel
topic Fe–Mn–Al–C steel
ε-martensite
Cryogenic toughness
Deformation twin
url http://www.sciencedirect.com/science/article/pii/S2238785423023815
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