Microencapsulated Red Powders from Cornflower Extract—Spectral (FT-IR and FT-Raman) and Antioxidant Characteristics

Although the health benefits of cornflower extracts are known, their application in food production has not been widely investigated. This study assessed microencapsulated red powders (RP) prepared from the aqueous extract of blue cornflower petals. Microencapsulation was performed by freeze-drying...

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Main Authors: Renata Różyło, Monika Szymańska-Chargot, Artur Zdunek, Urszula Gawlik-Dziki, Dariusz Dziki
Format: Article
Language:English
Published: MDPI AG 2022-05-01
Series:Molecules
Subjects:
Online Access:https://www.mdpi.com/1420-3049/27/10/3094
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author Renata Różyło
Monika Szymańska-Chargot
Artur Zdunek
Urszula Gawlik-Dziki
Dariusz Dziki
author_facet Renata Różyło
Monika Szymańska-Chargot
Artur Zdunek
Urszula Gawlik-Dziki
Dariusz Dziki
author_sort Renata Różyło
collection DOAJ
description Although the health benefits of cornflower extracts are known, their application in food production has not been widely investigated. This study assessed microencapsulated red powders (RP) prepared from the aqueous extract of blue cornflower petals. Microencapsulation was performed by freeze-drying using various stabilizers, such as maltodextrin, guar gum, and lecithin. The microencapsulated RP were characterized by spectral (FT-IR and FT-Raman), mineral, structural, and antioxidant analyses. The FT-IR and FT-Raman band related to guar gum, lecithin, and maltodextrin dominated over the band characteristic of anthocyanins present in the cornflower petal powders. The main difference observed in the FT-Raman spectra was attributed to a shift of bands which is reflection of appearance of flavium cation forms of anthocyanins. The microencapsulated RP had total phenolic content of 21.6–23.4 mg GAE/g DW and total flavonoid content of 5.0–5.23 mg QE/g. The ABTS radical scavenging activity of the tested powders ranged from 13.8 to 20.2 EC<sub>50</sub> mg DW/mL. The reducing antioxidant power (RED) of the powders was estimated at between 31.0 and 38.7 EC<sub>50</sub> mg DW/mL, and OH<sup>•</sup> scavenging activity ranged from 1.9 to 2.6 EC<sub>50</sub> mg DW/mL. Microencapsulated cornflower RP can be valuable additives to food such as sweets, jellies, puddings, drinks, or dietary supplements.
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spelling doaj.art-7f445603d1a6445bb2bca9d42725737d2023-11-23T12:20:56ZengMDPI AGMolecules1420-30492022-05-012710309410.3390/molecules27103094Microencapsulated Red Powders from Cornflower Extract—Spectral (FT-IR and FT-Raman) and Antioxidant CharacteristicsRenata Różyło0Monika Szymańska-Chargot1Artur Zdunek2Urszula Gawlik-Dziki3Dariusz Dziki4Department of Food Engineering and Machines, University of Life Sciences in Lublin, Głęboka Street 28, 20-612 Lublin, PolandInstitute of Agrophysics, Polish Academy of Sciences, Doświadczalna Street 4, 20-290 Lublin, PolandInstitute of Agrophysics, Polish Academy of Sciences, Doświadczalna Street 4, 20-290 Lublin, PolandDepartment of Biochemistry and Food Chemistry, University of Life Sciences in Lublin, Skromna Street 8, 20-704 Lublin, PolandDepartment of Thermal Technology and Food Process Engineering, University of Life Sciences in Lublin, Głęboka Street 31, 20-612 Lublin, PolandAlthough the health benefits of cornflower extracts are known, their application in food production has not been widely investigated. This study assessed microencapsulated red powders (RP) prepared from the aqueous extract of blue cornflower petals. Microencapsulation was performed by freeze-drying using various stabilizers, such as maltodextrin, guar gum, and lecithin. The microencapsulated RP were characterized by spectral (FT-IR and FT-Raman), mineral, structural, and antioxidant analyses. The FT-IR and FT-Raman band related to guar gum, lecithin, and maltodextrin dominated over the band characteristic of anthocyanins present in the cornflower petal powders. The main difference observed in the FT-Raman spectra was attributed to a shift of bands which is reflection of appearance of flavium cation forms of anthocyanins. The microencapsulated RP had total phenolic content of 21.6–23.4 mg GAE/g DW and total flavonoid content of 5.0–5.23 mg QE/g. The ABTS radical scavenging activity of the tested powders ranged from 13.8 to 20.2 EC<sub>50</sub> mg DW/mL. The reducing antioxidant power (RED) of the powders was estimated at between 31.0 and 38.7 EC<sub>50</sub> mg DW/mL, and OH<sup>•</sup> scavenging activity ranged from 1.9 to 2.6 EC<sub>50</sub> mg DW/mL. Microencapsulated cornflower RP can be valuable additives to food such as sweets, jellies, puddings, drinks, or dietary supplements.https://www.mdpi.com/1420-3049/27/10/3094cornflower petalfood colorantmicroencapsulationfreeze-dryingspectralFT-IR
spellingShingle Renata Różyło
Monika Szymańska-Chargot
Artur Zdunek
Urszula Gawlik-Dziki
Dariusz Dziki
Microencapsulated Red Powders from Cornflower Extract—Spectral (FT-IR and FT-Raman) and Antioxidant Characteristics
Molecules
cornflower petal
food colorant
microencapsulation
freeze-drying
spectral
FT-IR
title Microencapsulated Red Powders from Cornflower Extract—Spectral (FT-IR and FT-Raman) and Antioxidant Characteristics
title_full Microencapsulated Red Powders from Cornflower Extract—Spectral (FT-IR and FT-Raman) and Antioxidant Characteristics
title_fullStr Microencapsulated Red Powders from Cornflower Extract—Spectral (FT-IR and FT-Raman) and Antioxidant Characteristics
title_full_unstemmed Microencapsulated Red Powders from Cornflower Extract—Spectral (FT-IR and FT-Raman) and Antioxidant Characteristics
title_short Microencapsulated Red Powders from Cornflower Extract—Spectral (FT-IR and FT-Raman) and Antioxidant Characteristics
title_sort microencapsulated red powders from cornflower extract spectral ft ir and ft raman and antioxidant characteristics
topic cornflower petal
food colorant
microencapsulation
freeze-drying
spectral
FT-IR
url https://www.mdpi.com/1420-3049/27/10/3094
work_keys_str_mv AT renatarozyło microencapsulatedredpowdersfromcornflowerextractspectralftirandftramanandantioxidantcharacteristics
AT monikaszymanskachargot microencapsulatedredpowdersfromcornflowerextractspectralftirandftramanandantioxidantcharacteristics
AT arturzdunek microencapsulatedredpowdersfromcornflowerextractspectralftirandftramanandantioxidantcharacteristics
AT urszulagawlikdziki microencapsulatedredpowdersfromcornflowerextractspectralftirandftramanandantioxidantcharacteristics
AT dariuszdziki microencapsulatedredpowdersfromcornflowerextractspectralftirandftramanandantioxidantcharacteristics