Isolation and Characterization of Cellulose Obtained from Bagasse Pith by Oxygen-Containing Agents
The environmentally-friendly procedure of oxygen treatment (O) and peroxide treatment with oxygen and anthraquinone as a catalyst (Po-AQ) was studied for isolation of cellulose from bagasse pith (BP) mainly consisting of parenchyma cells. The optimal conditions were: 20% alkali dosages with 12% BP c...
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Language: | English |
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North Carolina State University
2014-05-01
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Series: | BioResources |
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Online Access: | http://ojs.cnr.ncsu.edu/index.php/BioRes/article/view/BioRes_09_3_4094_Gao_Cellulose_Bagasse_Pith |
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author | Xin Gao Ke-Li Chen Heng Zhang Lin-Cai Peng Qi-Xing Liu |
author_facet | Xin Gao Ke-Li Chen Heng Zhang Lin-Cai Peng Qi-Xing Liu |
author_sort | Xin Gao |
collection | DOAJ |
description | The environmentally-friendly procedure of oxygen treatment (O) and peroxide treatment with oxygen and anthraquinone as a catalyst (Po-AQ) was studied for isolation of cellulose from bagasse pith (BP) mainly consisting of parenchyma cells. The optimal conditions were: 20% alkali dosages with 12% BP consistency at 120 °C for 3 h under 0.6 MPa initial oxygen pressure for the O step; then 8% H2O2, 20% NaOH, and 0.3% AQ charges with 8% BP consistency at 120 °C for 6 h under the same oxygen pressure for the Po-AQ step. And the optimum process was: BP pretreated by cool-water extraction was firstly O-treated, and after finishing O treatment, intermediate pulp which was manually separated from effluent, was continuously processed by Po-AQ treatment. Based on the conditions above, this process can yield 37.1% of cellulose sample, containing 7.01% hemicelluloses and 0.57% lignin. The representative samples were characterized by gas chromatography (GC), Fourier transform infrared spectrometry (FT-IR), X-ray diffraction (XRD), and scanning electron microscopy (SEM). |
first_indexed | 2024-12-11T12:43:40Z |
format | Article |
id | doaj.art-7fcc4fff3b134c4098dc8ba254bd500a |
institution | Directory Open Access Journal |
issn | 1930-2126 1930-2126 |
language | English |
last_indexed | 2024-12-11T12:43:40Z |
publishDate | 2014-05-01 |
publisher | North Carolina State University |
record_format | Article |
series | BioResources |
spelling | doaj.art-7fcc4fff3b134c4098dc8ba254bd500a2022-12-22T01:06:53ZengNorth Carolina State UniversityBioResources1930-21261930-21262014-05-01934094410710.15376/biores.9.3.4094-4107Isolation and Characterization of Cellulose Obtained from Bagasse Pith by Oxygen-Containing AgentsXin Gao0Ke-Li Chen1Heng Zhang2Lin-Cai Peng3Qi-Xing Liu4Kunming University of Science and TechnologyKunming University of Science and TechnologyKunming University of Science and TechnologyKunming University of Science and TechnologyKunming University of Science and TechnologyThe environmentally-friendly procedure of oxygen treatment (O) and peroxide treatment with oxygen and anthraquinone as a catalyst (Po-AQ) was studied for isolation of cellulose from bagasse pith (BP) mainly consisting of parenchyma cells. The optimal conditions were: 20% alkali dosages with 12% BP consistency at 120 °C for 3 h under 0.6 MPa initial oxygen pressure for the O step; then 8% H2O2, 20% NaOH, and 0.3% AQ charges with 8% BP consistency at 120 °C for 6 h under the same oxygen pressure for the Po-AQ step. And the optimum process was: BP pretreated by cool-water extraction was firstly O-treated, and after finishing O treatment, intermediate pulp which was manually separated from effluent, was continuously processed by Po-AQ treatment. Based on the conditions above, this process can yield 37.1% of cellulose sample, containing 7.01% hemicelluloses and 0.57% lignin. The representative samples were characterized by gas chromatography (GC), Fourier transform infrared spectrometry (FT-IR), X-ray diffraction (XRD), and scanning electron microscopy (SEM).http://ojs.cnr.ncsu.edu/index.php/BioRes/article/view/BioRes_09_3_4094_Gao_Cellulose_Bagasse_PithBagasse pithParenchyma cellCellulose isolationOxygen-containing treatment |
spellingShingle | Xin Gao Ke-Li Chen Heng Zhang Lin-Cai Peng Qi-Xing Liu Isolation and Characterization of Cellulose Obtained from Bagasse Pith by Oxygen-Containing Agents BioResources Bagasse pith Parenchyma cell Cellulose isolation Oxygen-containing treatment |
title | Isolation and Characterization of Cellulose Obtained from Bagasse Pith by Oxygen-Containing Agents |
title_full | Isolation and Characterization of Cellulose Obtained from Bagasse Pith by Oxygen-Containing Agents |
title_fullStr | Isolation and Characterization of Cellulose Obtained from Bagasse Pith by Oxygen-Containing Agents |
title_full_unstemmed | Isolation and Characterization of Cellulose Obtained from Bagasse Pith by Oxygen-Containing Agents |
title_short | Isolation and Characterization of Cellulose Obtained from Bagasse Pith by Oxygen-Containing Agents |
title_sort | isolation and characterization of cellulose obtained from bagasse pith by oxygen containing agents |
topic | Bagasse pith Parenchyma cell Cellulose isolation Oxygen-containing treatment |
url | http://ojs.cnr.ncsu.edu/index.php/BioRes/article/view/BioRes_09_3_4094_Gao_Cellulose_Bagasse_Pith |
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