Revealing microstructures evolution and dynamic recrystallization mechanisms of Mg–Sn–Mn alloy during compressive deformation at elevated temperature

The flow behavior of as-extruded Mg–3Sn-1.5Mn (wt.%) alloy was systematically researched via isothermal compression tests. The compressive temperatures (T) were from 250 °C to 400 °C, the strain rates were from 0.001 s−1 to 1s−1 and the true strain reached 0.69. Based on compression curves, flow str...

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Main Authors: Yunduo Feng, Jinhui Wang, Shiyu Luan, Shuai Yuan, Xiaoyu Liu, Xiaowei Li, Li Han, Qi Wei
Format: Article
Language:English
Published: Elsevier 2023-12-01
Series:Results in Materials
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2590048X23001115
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author Yunduo Feng
Jinhui Wang
Shiyu Luan
Shuai Yuan
Xiaoyu Liu
Xiaowei Li
Li Han
Qi Wei
author_facet Yunduo Feng
Jinhui Wang
Shiyu Luan
Shuai Yuan
Xiaoyu Liu
Xiaowei Li
Li Han
Qi Wei
author_sort Yunduo Feng
collection DOAJ
description The flow behavior of as-extruded Mg–3Sn-1.5Mn (wt.%) alloy was systematically researched via isothermal compression tests. The compressive temperatures (T) were from 250 °C to 400 °C, the strain rates were from 0.001 s−1 to 1s−1 and the true strain reached 0.69. Based on compression curves, flow stress apparently rose with increasing strain rate and/or decreasing temperature. Combined with the analysis of microstructure and processing map, the optimum working parameter was determined in the range of 350–400 °C, 0.01–1 s−1. According to electron backscatter diffraction (EBSD) analysis results, texture intensity significantly decreased and the basal (0001)//ED texture had transformed to basal <0001>//CD texture after compressive deformation obviously. Furthermore, the typical discontinue dynamic recrystallization (DDRX) and continue dynamic recrystallization (CDRX) were largely believed to be the major DRX mechanisms in Mg–3Sn-1.5Mn alloy. Both increasing temperature and decreasing strain rate had obvious influence on the degree of DRX. The activated slip systems in deformed grains were determined by the analysis of the in-grain misorientation axis (IGMA). As deformation temperature elevated, pyramidal <c+a> slip greatly activated and dominated compressive deformation.
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spelling doaj.art-80185a20fbc1460f8c4cdbd2e5f453692023-12-10T06:17:19ZengElsevierResults in Materials2590-048X2023-12-0120100473Revealing microstructures evolution and dynamic recrystallization mechanisms of Mg–Sn–Mn alloy during compressive deformation at elevated temperatureYunduo Feng0Jinhui Wang1Shiyu Luan2Shuai Yuan3Xiaoyu Liu4Xiaowei Li5Li Han6Qi Wei7Qinghai Provincial Key Laboratory of New Light Alloys, Qinghai Provincial Engineering Research Center of High-Performance Light Metal Alloys and Forming, Qinghai University, Xining, 810016, ChinaQinghai Provincial Key Laboratory of New Light Alloys, Qinghai Provincial Engineering Research Center of High-Performance Light Metal Alloys and Forming, Qinghai University, Xining, 810016, ChinaQinghai Provincial Key Laboratory of New Light Alloys, Qinghai Provincial Engineering Research Center of High-Performance Light Metal Alloys and Forming, Qinghai University, Xining, 810016, ChinaQinghai Provincial Key Laboratory of New Light Alloys, Qinghai Provincial Engineering Research Center of High-Performance Light Metal Alloys and Forming, Qinghai University, Xining, 810016, ChinaQinghai Provincial Key Laboratory of New Light Alloys, Qinghai Provincial Engineering Research Center of High-Performance Light Metal Alloys and Forming, Qinghai University, Xining, 810016, ChinaQinghai Provincial Key Laboratory of New Light Alloys, Qinghai Provincial Engineering Research Center of High-Performance Light Metal Alloys and Forming, Qinghai University, Xining, 810016, ChinaKey Laboratory of Comprehensive and Highly Efficient Utilization of Salt Lake Resources, Qinghai Institute of Salt Lakes, Chinese Academy of Sciences, 18 Xinning Road, Xining, 810008, China; Corresponding author.Qinghai Provincial Key Laboratory of New Light Alloys, Qinghai Provincial Engineering Research Center of High-Performance Light Metal Alloys and Forming, Qinghai University, Xining, 810016, China; Corresponding author.The flow behavior of as-extruded Mg–3Sn-1.5Mn (wt.%) alloy was systematically researched via isothermal compression tests. The compressive temperatures (T) were from 250 °C to 400 °C, the strain rates were from 0.001 s−1 to 1s−1 and the true strain reached 0.69. Based on compression curves, flow stress apparently rose with increasing strain rate and/or decreasing temperature. Combined with the analysis of microstructure and processing map, the optimum working parameter was determined in the range of 350–400 °C, 0.01–1 s−1. According to electron backscatter diffraction (EBSD) analysis results, texture intensity significantly decreased and the basal (0001)//ED texture had transformed to basal <0001>//CD texture after compressive deformation obviously. Furthermore, the typical discontinue dynamic recrystallization (DDRX) and continue dynamic recrystallization (CDRX) were largely believed to be the major DRX mechanisms in Mg–3Sn-1.5Mn alloy. Both increasing temperature and decreasing strain rate had obvious influence on the degree of DRX. The activated slip systems in deformed grains were determined by the analysis of the in-grain misorientation axis (IGMA). As deformation temperature elevated, pyramidal <c+a> slip greatly activated and dominated compressive deformation.http://www.sciencedirect.com/science/article/pii/S2590048X23001115Magnesium alloyHot compressive deformationDynamic recrystallizationMicrostructure evolution
spellingShingle Yunduo Feng
Jinhui Wang
Shiyu Luan
Shuai Yuan
Xiaoyu Liu
Xiaowei Li
Li Han
Qi Wei
Revealing microstructures evolution and dynamic recrystallization mechanisms of Mg–Sn–Mn alloy during compressive deformation at elevated temperature
Results in Materials
Magnesium alloy
Hot compressive deformation
Dynamic recrystallization
Microstructure evolution
title Revealing microstructures evolution and dynamic recrystallization mechanisms of Mg–Sn–Mn alloy during compressive deformation at elevated temperature
title_full Revealing microstructures evolution and dynamic recrystallization mechanisms of Mg–Sn–Mn alloy during compressive deformation at elevated temperature
title_fullStr Revealing microstructures evolution and dynamic recrystallization mechanisms of Mg–Sn–Mn alloy during compressive deformation at elevated temperature
title_full_unstemmed Revealing microstructures evolution and dynamic recrystallization mechanisms of Mg–Sn–Mn alloy during compressive deformation at elevated temperature
title_short Revealing microstructures evolution and dynamic recrystallization mechanisms of Mg–Sn–Mn alloy during compressive deformation at elevated temperature
title_sort revealing microstructures evolution and dynamic recrystallization mechanisms of mg sn mn alloy during compressive deformation at elevated temperature
topic Magnesium alloy
Hot compressive deformation
Dynamic recrystallization
Microstructure evolution
url http://www.sciencedirect.com/science/article/pii/S2590048X23001115
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