Sustainable synthesis of benzopyran derivatives catalyzed by MgO nanoparticles: Spectral, DFT and TEM analysis
In current work, a magnesium oxide nanocatalyst was synthesized via greener route using aloe-vera plant leaf extracts as a reducing and stabilizing agent to construct MgO nanoparticle. The synthesized nanocatalyst has been characterized by UV–visible spectroscopy, FT-IR spectroscopy, TEM, and SAED....
| Main Authors: | , , , , |
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| Format: | Article |
| Language: | English |
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Elsevier
2023-01-01
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| Series: | Results in Chemistry |
| Subjects: | |
| Online Access: | http://www.sciencedirect.com/science/article/pii/S2211715623001236 |
| _version_ | 1797799015270580224 |
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| author | Har Lal Singh Mamta Chahar Sangeeta Saloni Sahal Sarita Khaturia |
| author_facet | Har Lal Singh Mamta Chahar Sangeeta Saloni Sahal Sarita Khaturia |
| author_sort | Har Lal Singh |
| collection | DOAJ |
| description | In current work, a magnesium oxide nanocatalyst was synthesized via greener route using aloe-vera plant leaf extracts as a reducing and stabilizing agent to construct MgO nanoparticle. The synthesized nanocatalyst has been characterized by UV–visible spectroscopy, FT-IR spectroscopy, TEM, and SAED. Further, magnesium oxide nanoparticles used as a catalyst for the efficient and facile green synthesis of various benzopyran derivatives (4a-i) in good to outstanding yields (89–94%) under microwave irradiation. This catalyst has showed good characteristics in terms of amount, recoverability, activity and reusability without noticeably degrading performance. |
| first_indexed | 2024-03-13T04:13:36Z |
| format | Article |
| id | doaj.art-801b068a495e4c86b80c1a2b5ff42105 |
| institution | Directory Open Access Journal |
| issn | 2211-7156 |
| language | English |
| last_indexed | 2024-03-13T04:13:36Z |
| publishDate | 2023-01-01 |
| publisher | Elsevier |
| record_format | Article |
| series | Results in Chemistry |
| spelling | doaj.art-801b068a495e4c86b80c1a2b5ff421052023-06-21T06:52:25ZengElsevierResults in Chemistry2211-71562023-01-015100884Sustainable synthesis of benzopyran derivatives catalyzed by MgO nanoparticles: Spectral, DFT and TEM analysisHar Lal Singh0Mamta Chahar1 Sangeeta2Saloni Sahal3Sarita Khaturia4Department of Chemistry, Mody University of Science and Technology, Lakshmangarh-332311, Sikar, Rajasthan, IndiaSchool of Sciences, P. P. Savani University, Surat 394125, IndiaDepartment of Chemistry, Mody University of Science and Technology, Lakshmangarh-332311, Sikar, Rajasthan, IndiaDepartment of Chemistry, Mody University of Science and Technology, Lakshmangarh-332311, Sikar, Rajasthan, IndiaDepartment of Chemistry, Mody University of Science and Technology, Lakshmangarh-332311, Sikar, Rajasthan, India; Corresponding author.In current work, a magnesium oxide nanocatalyst was synthesized via greener route using aloe-vera plant leaf extracts as a reducing and stabilizing agent to construct MgO nanoparticle. The synthesized nanocatalyst has been characterized by UV–visible spectroscopy, FT-IR spectroscopy, TEM, and SAED. Further, magnesium oxide nanoparticles used as a catalyst for the efficient and facile green synthesis of various benzopyran derivatives (4a-i) in good to outstanding yields (89–94%) under microwave irradiation. This catalyst has showed good characteristics in terms of amount, recoverability, activity and reusability without noticeably degrading performance.http://www.sciencedirect.com/science/article/pii/S2211715623001236MgO NPsAloe-veraCatalysisHeterocyclesGreen synthesisBenzopyrans |
| spellingShingle | Har Lal Singh Mamta Chahar Sangeeta Saloni Sahal Sarita Khaturia Sustainable synthesis of benzopyran derivatives catalyzed by MgO nanoparticles: Spectral, DFT and TEM analysis Results in Chemistry MgO NPs Aloe-vera Catalysis Heterocycles Green synthesis Benzopyrans |
| title | Sustainable synthesis of benzopyran derivatives catalyzed by MgO nanoparticles: Spectral, DFT and TEM analysis |
| title_full | Sustainable synthesis of benzopyran derivatives catalyzed by MgO nanoparticles: Spectral, DFT and TEM analysis |
| title_fullStr | Sustainable synthesis of benzopyran derivatives catalyzed by MgO nanoparticles: Spectral, DFT and TEM analysis |
| title_full_unstemmed | Sustainable synthesis of benzopyran derivatives catalyzed by MgO nanoparticles: Spectral, DFT and TEM analysis |
| title_short | Sustainable synthesis of benzopyran derivatives catalyzed by MgO nanoparticles: Spectral, DFT and TEM analysis |
| title_sort | sustainable synthesis of benzopyran derivatives catalyzed by mgo nanoparticles spectral dft and tem analysis |
| topic | MgO NPs Aloe-vera Catalysis Heterocycles Green synthesis Benzopyrans |
| url | http://www.sciencedirect.com/science/article/pii/S2211715623001236 |
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