An Efficient One Pot Procedure for Preparation of Symmetrical N,N'-Disubstituted Urea from Aromatic and Aliphatic Amines and Urea under Microwave Irradiation
A phosgene-free synthesis of symmetrical N,N'-disubstituted urea by the reaction of aromatic and aliphatic primary amines and urea promoted by microwave irradiation in the presence of a suitable energy-transfer solvent such as N-N-dimethylacetamide is described.
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Format: | Article |
Language: | English |
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Iranian Institute of Research and Development in Chemical Industries (IRDCI)-ACECR
2000-06-01
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Series: | Iranian Journal of Chemistry & Chemical Engineering |
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Online Access: | http://www.ijcce.ac.ir/article_10203_4cdbfce8016c17706968d99a59c7dfc5.pdf |
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author | Mohammad S. Khajavi Mohammad Gl Dakamin Hassan Hazarkhani Mostafa Hajihadi Farzad Nikpour |
author_facet | Mohammad S. Khajavi Mohammad Gl Dakamin Hassan Hazarkhani Mostafa Hajihadi Farzad Nikpour |
author_sort | Mohammad S. Khajavi |
collection | DOAJ |
description | A phosgene-free synthesis of symmetrical N,N'-disubstituted urea by the reaction of aromatic and aliphatic primary amines and urea promoted by microwave irradiation in the presence of a suitable energy-transfer solvent such as N-N-dimethylacetamide is described. |
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format | Article |
id | doaj.art-801c24f905564636ac60e9295967f80c |
institution | Directory Open Access Journal |
issn | 1021-9986 1021-9986 |
language | English |
last_indexed | 2024-12-22T22:47:25Z |
publishDate | 2000-06-01 |
publisher | Iranian Institute of Research and Development in Chemical Industries (IRDCI)-ACECR |
record_format | Article |
series | Iranian Journal of Chemistry & Chemical Engineering |
spelling | doaj.art-801c24f905564636ac60e9295967f80c2022-12-21T18:10:02ZengIranian Institute of Research and Development in Chemical Industries (IRDCI)-ACECRIranian Journal of Chemistry & Chemical Engineering1021-99861021-99862000-06-01191242810203An Efficient One Pot Procedure for Preparation of Symmetrical N,N'-Disubstituted Urea from Aromatic and Aliphatic Amines and Urea under Microwave IrradiationMohammad S. Khajavi0Mohammad Gl Dakamin1Hassan Hazarkhani2Mostafa Hajihadi3Farzad Nikpour4Department of Chemistry, Faculty of Science, Shahid Beheshti University, Department of Chemistry, Faculty of Science, Shahid Beheshti University, Tehran, I.R. IRAN, I.R. IRANDepartment of Chemistry, Faculty of Science, Shahid Beheshti University, Tehran, I.R. IRANDepartment of Chemistry, Faculty of Science, Shahid Beheshti University, Tehran, I.R. IRANDepartment of Chemistry, Faculty of Science, Shahid Beheshti University, Tehran, I.R. IRANDepartment of Chemistry, Faculty of Science, Shahid Beheshti University, Tehran, I.R. IRANA phosgene-free synthesis of symmetrical N,N'-disubstituted urea by the reaction of aromatic and aliphatic primary amines and urea promoted by microwave irradiation in the presence of a suitable energy-transfer solvent such as N-N-dimethylacetamide is described.http://www.ijcce.ac.ir/article_10203_4cdbfce8016c17706968d99a59c7dfc5.pdfmicrowave irradiationaminesn'-disubstituted urean-dimethylacetamidesolvent free reactionurea |
spellingShingle | Mohammad S. Khajavi Mohammad Gl Dakamin Hassan Hazarkhani Mostafa Hajihadi Farzad Nikpour An Efficient One Pot Procedure for Preparation of Symmetrical N,N'-Disubstituted Urea from Aromatic and Aliphatic Amines and Urea under Microwave Irradiation Iranian Journal of Chemistry & Chemical Engineering microwave irradiation amines n'-disubstituted urea n-dimethylacetamide solvent free reaction urea |
title | An Efficient One Pot Procedure for Preparation of Symmetrical N,N'-Disubstituted Urea from Aromatic and Aliphatic Amines and Urea under Microwave Irradiation |
title_full | An Efficient One Pot Procedure for Preparation of Symmetrical N,N'-Disubstituted Urea from Aromatic and Aliphatic Amines and Urea under Microwave Irradiation |
title_fullStr | An Efficient One Pot Procedure for Preparation of Symmetrical N,N'-Disubstituted Urea from Aromatic and Aliphatic Amines and Urea under Microwave Irradiation |
title_full_unstemmed | An Efficient One Pot Procedure for Preparation of Symmetrical N,N'-Disubstituted Urea from Aromatic and Aliphatic Amines and Urea under Microwave Irradiation |
title_short | An Efficient One Pot Procedure for Preparation of Symmetrical N,N'-Disubstituted Urea from Aromatic and Aliphatic Amines and Urea under Microwave Irradiation |
title_sort | efficient one pot procedure for preparation of symmetrical n n disubstituted urea from aromatic and aliphatic amines and urea under microwave irradiation |
topic | microwave irradiation amines n'-disubstituted urea n-dimethylacetamide solvent free reaction urea |
url | http://www.ijcce.ac.ir/article_10203_4cdbfce8016c17706968d99a59c7dfc5.pdf |
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