Rapid Solidification of Invar Alloy

The Invar alloy has excellent properties, such as a low coefficient of thermal expansion, but there are few reports about the rapid solidification of this alloy. In this study, Invar alloy solidification at different undercooling (Δ<i>T</i>) was investigated via glass melt-flux technique...

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Main Authors: Hanxin He, Zhirui Yao, Xuyang Li, Junfeng Xu
Format: Article
Language:English
Published: MDPI AG 2023-12-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/17/1/231
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author Hanxin He
Zhirui Yao
Xuyang Li
Junfeng Xu
author_facet Hanxin He
Zhirui Yao
Xuyang Li
Junfeng Xu
author_sort Hanxin He
collection DOAJ
description The Invar alloy has excellent properties, such as a low coefficient of thermal expansion, but there are few reports about the rapid solidification of this alloy. In this study, Invar alloy solidification at different undercooling (Δ<i>T</i>) was investigated via glass melt-flux techniques. The sample with the highest undercooling of Δ<i>T</i> = 231 K (recalescence height 140 K) was obtained. The thermal history curve, microstructure, hardness, grain number, and sample density of the alloy were analyzed. The results show that with the increase in solidification undercooling, the XRD peak of the sample shifted to the left, indicating that the lattice constant increased and the solid solubility increased. As the solidification of undercooling increases, the microstructure changes from large dendrites to small columnar grains and then to fine equiaxed grains. At the same time, the number of grains also increases with the increase in the undercooling. The hardness of the sample increases with increasing undercooling. If Δ<i>T</i> ≥ 181 K (128 K), the grain number and the hardness do not increase with undercooling.
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spelling doaj.art-809861334c2745dbb895f2f888c3ccd62024-01-10T15:03:03ZengMDPI AGMaterials1996-19442023-12-0117123110.3390/ma17010231Rapid Solidification of Invar AlloyHanxin He0Zhirui Yao1Xuyang Li2Junfeng Xu3School of Civil Engineering, Xi’an University of Architecture and Technology, No. 13 Yanta Road, Xi’an 710055, ChinaSchool of Materials and Chemical Engineering, Xi’an Technological University, Xi’an 710021, ChinaXi’an Institute of Optics and Precision Mechanics, Xi’an 710119, ChinaSchool of Materials and Chemical Engineering, Xi’an Technological University, Xi’an 710021, ChinaThe Invar alloy has excellent properties, such as a low coefficient of thermal expansion, but there are few reports about the rapid solidification of this alloy. In this study, Invar alloy solidification at different undercooling (Δ<i>T</i>) was investigated via glass melt-flux techniques. The sample with the highest undercooling of Δ<i>T</i> = 231 K (recalescence height 140 K) was obtained. The thermal history curve, microstructure, hardness, grain number, and sample density of the alloy were analyzed. The results show that with the increase in solidification undercooling, the XRD peak of the sample shifted to the left, indicating that the lattice constant increased and the solid solubility increased. As the solidification of undercooling increases, the microstructure changes from large dendrites to small columnar grains and then to fine equiaxed grains. At the same time, the number of grains also increases with the increase in the undercooling. The hardness of the sample increases with increasing undercooling. If Δ<i>T</i> ≥ 181 K (128 K), the grain number and the hardness do not increase with undercooling.https://www.mdpi.com/1996-1944/17/1/231Invar alloysolidificationundercoolinghardness
spellingShingle Hanxin He
Zhirui Yao
Xuyang Li
Junfeng Xu
Rapid Solidification of Invar Alloy
Materials
Invar alloy
solidification
undercooling
hardness
title Rapid Solidification of Invar Alloy
title_full Rapid Solidification of Invar Alloy
title_fullStr Rapid Solidification of Invar Alloy
title_full_unstemmed Rapid Solidification of Invar Alloy
title_short Rapid Solidification of Invar Alloy
title_sort rapid solidification of invar alloy
topic Invar alloy
solidification
undercooling
hardness
url https://www.mdpi.com/1996-1944/17/1/231
work_keys_str_mv AT hanxinhe rapidsolidificationofinvaralloy
AT zhiruiyao rapidsolidificationofinvaralloy
AT xuyangli rapidsolidificationofinvaralloy
AT junfengxu rapidsolidificationofinvaralloy