Syntheses of 1,5-Benzothiazepines. Part 20. Syntheses of 8-Substituted-2,5-dihydro-2-(4-N-dimethylaminophenyl)-4-(4-methoxyphenyl)-1,5-benzothiazepines
8-Substituted-2,5-dihydro-2-(4-N-dimethylaminophenyl)-4-(4-methoxyphenyl)-1,5-benzothiazepines (5a-e) have been synthesized by reacting 5-substituted-2-aminobenzene-thiols (1a-e) with 4-Ndimethylaminobenzal-4-methoxy acetophenone (2) in dry ethanol saturated with hydrogen chloride gas. The products...
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| Format: | Article |
| Language: | English |
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MDPI AG
1998-05-01
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| Series: | Molecules |
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| Online Access: | http://www.mdpi.com/1420-3049/3/6/159/ |
| _version_ | 1818481504597049344 |
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| author | Umesh C. Pant Mani Upreti Babita Singhal Seema Pant |
| author_facet | Umesh C. Pant Mani Upreti Babita Singhal Seema Pant |
| author_sort | Umesh C. Pant |
| collection | DOAJ |
| description | 8-Substituted-2,5-dihydro-2-(4-N-dimethylaminophenyl)-4-(4-methoxyphenyl)-1,5-benzothiazepines (5a-e) have been synthesized by reacting 5-substituted-2-aminobenzene-thiols (1a-e) with 4-Ndimethylaminobenzal-4-methoxy acetophenone (2) in dry ethanol saturated with hydrogen chloride gas. The products were tested for purity by tlc and characterized by elemental analysis for carbon, hydrogen and nitrogen and IR, 1H NMR and mass spectral studies. |
| first_indexed | 2024-12-10T11:35:48Z |
| format | Article |
| id | doaj.art-81896d31335a401da7e243e813d563bd |
| institution | Directory Open Access Journal |
| issn | 1420-3049 |
| language | English |
| last_indexed | 2024-12-10T11:35:48Z |
| publishDate | 1998-05-01 |
| publisher | MDPI AG |
| record_format | Article |
| series | Molecules |
| spelling | doaj.art-81896d31335a401da7e243e813d563bd2022-12-22T01:50:27ZengMDPI AGMolecules1420-30491998-05-013615916310.3390/30600159Syntheses of 1,5-Benzothiazepines. Part 20. Syntheses of 8-Substituted-2,5-dihydro-2-(4-N-dimethylaminophenyl)-4-(4-methoxyphenyl)-1,5-benzothiazepinesUmesh C. PantMani UpretiBabita SinghalSeema Pant8-Substituted-2,5-dihydro-2-(4-N-dimethylaminophenyl)-4-(4-methoxyphenyl)-1,5-benzothiazepines (5a-e) have been synthesized by reacting 5-substituted-2-aminobenzene-thiols (1a-e) with 4-Ndimethylaminobenzal-4-methoxy acetophenone (2) in dry ethanol saturated with hydrogen chloride gas. The products were tested for purity by tlc and characterized by elemental analysis for carbon, hydrogen and nitrogen and IR, 1H NMR and mass spectral studies.http://www.mdpi.com/1420-3049/3/6/159/15-Benzothiazepinehydrogen chloride gas |
| spellingShingle | Umesh C. Pant Mani Upreti Babita Singhal Seema Pant Syntheses of 1,5-Benzothiazepines. Part 20. Syntheses of 8-Substituted-2,5-dihydro-2-(4-N-dimethylaminophenyl)-4-(4-methoxyphenyl)-1,5-benzothiazepines Molecules 1 5-Benzothiazepine hydrogen chloride gas |
| title | Syntheses of 1,5-Benzothiazepines. Part 20. Syntheses of 8-Substituted-2,5-dihydro-2-(4-N-dimethylaminophenyl)-4-(4-methoxyphenyl)-1,5-benzothiazepines |
| title_full | Syntheses of 1,5-Benzothiazepines. Part 20. Syntheses of 8-Substituted-2,5-dihydro-2-(4-N-dimethylaminophenyl)-4-(4-methoxyphenyl)-1,5-benzothiazepines |
| title_fullStr | Syntheses of 1,5-Benzothiazepines. Part 20. Syntheses of 8-Substituted-2,5-dihydro-2-(4-N-dimethylaminophenyl)-4-(4-methoxyphenyl)-1,5-benzothiazepines |
| title_full_unstemmed | Syntheses of 1,5-Benzothiazepines. Part 20. Syntheses of 8-Substituted-2,5-dihydro-2-(4-N-dimethylaminophenyl)-4-(4-methoxyphenyl)-1,5-benzothiazepines |
| title_short | Syntheses of 1,5-Benzothiazepines. Part 20. Syntheses of 8-Substituted-2,5-dihydro-2-(4-N-dimethylaminophenyl)-4-(4-methoxyphenyl)-1,5-benzothiazepines |
| title_sort | syntheses of 1 5 benzothiazepines part 20 syntheses of 8 substituted 2 5 dihydro 2 4 n dimethylaminophenyl 4 4 methoxyphenyl 1 5 benzothiazepines |
| topic | 1 5-Benzothiazepine hydrogen chloride gas |
| url | http://www.mdpi.com/1420-3049/3/6/159/ |
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