Evolution of the Microstructure of a CuCr1Zr Alloy during Direct Heating by Electric Current

Round tensile test specimens of an age-hardened CuCr1Zr alloy were subjected to direct electrical current heating in a Gleeble thermal–mechanical simulator at 800 °C. The mechanical properties were monitored by the Vickers hardness test, and the changes in the grain structure were examined by light...

Full description

Bibliographic Details
Main Authors: Miroslav Karlík, Petr Haušild, Philippe Pilvin, Denis Carron
Format: Article
Language:English
Published: MDPI AG 2021-07-01
Series:Metals
Subjects:
Online Access:https://www.mdpi.com/2075-4701/11/7/1074
_version_ 1827687370565091328
author Miroslav Karlík
Petr Haušild
Philippe Pilvin
Denis Carron
author_facet Miroslav Karlík
Petr Haušild
Philippe Pilvin
Denis Carron
author_sort Miroslav Karlík
collection DOAJ
description Round tensile test specimens of an age-hardened CuCr1Zr alloy were subjected to direct electrical current heating in a Gleeble thermal–mechanical simulator at 800 °C. The mechanical properties were monitored by the Vickers hardness test, and the changes in the grain structure were examined by light metallography. A quantitative analysis of the size and distribution of fine precipitates during annealing was carried out using transmission electron microscopy (TEM). The grain structure showed a gradient corresponding to the gradient of the temperature on the test piece. Annealing for 60 s at 800 °C resulted in a partially (~50%) recrystallized structure with new grains about 45 μm in diameter. In the as-delivered condition, TEM documented tiny (1 to 4 nm) coherent chromium precipitates inducing strain fields in the matrix. During overaging, the particles lost their coherence and gradually coarsened up to a mean diameter of 40 nm after 300 s at 800 °C. The coarsening kinetics obeys Lifshitz, Sloyzov, and Wagner’s theory.
first_indexed 2024-03-10T09:32:30Z
format Article
id doaj.art-81a5ffb76fcb4a4cac27bd7047f2c6fe
institution Directory Open Access Journal
issn 2075-4701
language English
last_indexed 2024-03-10T09:32:30Z
publishDate 2021-07-01
publisher MDPI AG
record_format Article
series Metals
spelling doaj.art-81a5ffb76fcb4a4cac27bd7047f2c6fe2023-11-22T04:23:21ZengMDPI AGMetals2075-47012021-07-01117107410.3390/met11071074Evolution of the Microstructure of a CuCr1Zr Alloy during Direct Heating by Electric CurrentMiroslav Karlík0Petr Haušild1Philippe Pilvin2Denis Carron3Department of Materials, Faculty of Nuclear Sciences and Physical Engineering, Czech Technical University in Prague, Trojanova 13, 120 00 Praha 2, Czech RepublicDepartment of Materials, Faculty of Nuclear Sciences and Physical Engineering, Czech Technical University in Prague, Trojanova 13, 120 00 Praha 2, Czech RepublicUMR CNRS 6027, IRDL, Centre de Recherche C. Huygens, Université Bretagne Sud, Rue de Saint-Maudé, 56321 Lorient, FranceUMR CNRS 6027, IRDL, Centre de Recherche C. Huygens, Université Bretagne Sud, Rue de Saint-Maudé, 56321 Lorient, FranceRound tensile test specimens of an age-hardened CuCr1Zr alloy were subjected to direct electrical current heating in a Gleeble thermal–mechanical simulator at 800 °C. The mechanical properties were monitored by the Vickers hardness test, and the changes in the grain structure were examined by light metallography. A quantitative analysis of the size and distribution of fine precipitates during annealing was carried out using transmission electron microscopy (TEM). The grain structure showed a gradient corresponding to the gradient of the temperature on the test piece. Annealing for 60 s at 800 °C resulted in a partially (~50%) recrystallized structure with new grains about 45 μm in diameter. In the as-delivered condition, TEM documented tiny (1 to 4 nm) coherent chromium precipitates inducing strain fields in the matrix. During overaging, the particles lost their coherence and gradually coarsened up to a mean diameter of 40 nm after 300 s at 800 °C. The coarsening kinetics obeys Lifshitz, Sloyzov, and Wagner’s theory.https://www.mdpi.com/2075-4701/11/7/1074CuCr1Zr alloyrecrystallizationprecipitationelectron microscopymechanical properties
spellingShingle Miroslav Karlík
Petr Haušild
Philippe Pilvin
Denis Carron
Evolution of the Microstructure of a CuCr1Zr Alloy during Direct Heating by Electric Current
Metals
CuCr1Zr alloy
recrystallization
precipitation
electron microscopy
mechanical properties
title Evolution of the Microstructure of a CuCr1Zr Alloy during Direct Heating by Electric Current
title_full Evolution of the Microstructure of a CuCr1Zr Alloy during Direct Heating by Electric Current
title_fullStr Evolution of the Microstructure of a CuCr1Zr Alloy during Direct Heating by Electric Current
title_full_unstemmed Evolution of the Microstructure of a CuCr1Zr Alloy during Direct Heating by Electric Current
title_short Evolution of the Microstructure of a CuCr1Zr Alloy during Direct Heating by Electric Current
title_sort evolution of the microstructure of a cucr1zr alloy during direct heating by electric current
topic CuCr1Zr alloy
recrystallization
precipitation
electron microscopy
mechanical properties
url https://www.mdpi.com/2075-4701/11/7/1074
work_keys_str_mv AT miroslavkarlik evolutionofthemicrostructureofacucr1zralloyduringdirectheatingbyelectriccurrent
AT petrhausild evolutionofthemicrostructureofacucr1zralloyduringdirectheatingbyelectriccurrent
AT philippepilvin evolutionofthemicrostructureofacucr1zralloyduringdirectheatingbyelectriccurrent
AT deniscarron evolutionofthemicrostructureofacucr1zralloyduringdirectheatingbyelectriccurrent