Solvent recovery from solvent-fine coal slurries by filtration and steam stripping

Dewatering of fine coal is a significant industrial challenge with economic and environmental implications. Due to the lack of suitable dewatering technologies, fine coal particles are often discarded to waste impoundments, leading to substantial loss of valuable natural resources while creating env...

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Main Authors: Michael Huylo, Kaiwu Huang, Aaron Noble, Roe-Hoan Yoon, Rui Qiao
Format: Article
Language:English
Published: Frontiers Media S.A. 2023-08-01
Series:Frontiers in Thermal Engineering
Subjects:
Online Access:https://www.frontiersin.org/articles/10.3389/fther.2023.1239800/full
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author Michael Huylo
Kaiwu Huang
Aaron Noble
Roe-Hoan Yoon
Rui Qiao
author_facet Michael Huylo
Kaiwu Huang
Aaron Noble
Roe-Hoan Yoon
Rui Qiao
author_sort Michael Huylo
collection DOAJ
description Dewatering of fine coal is a significant industrial challenge with economic and environmental implications. Due to the lack of suitable dewatering technologies, fine coal particles are often discarded to waste impoundments, leading to substantial loss of valuable natural resources while creating environmental problems. The hydrophobic-hydrophilic separation (HHS) process is a unique solution to this problem. In this process, a recyclable solvent is used to simultaneously remove inorganic impurities (ash) and water from a run-of-mine fine coal slurry. A small amount of recyclable oil (or solvent) is added to a fine coal slurry so that the solvent can spontaneously displace the water from the surface of coal particles. The spent solvent is subsequently recovered and recycled in a closed loop. Here, we report the results obtained using two different solvents, i.e., pentane and hexane, to de-ash and dewater ultrafine coal and recover the spent solvent by filtration, followed by steam stripping. Most of the spent solvent can be recovered during the filtration step at 20 psig N₂ and at a 60 s filtration time. The residual solvent left in the cake was then recovered using steam under different conditions. The results showed that the residual solvent concentration could be reduced to <1,400 ppm after 10 s of steam stripping at 150°C and 15 psig.
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spelling doaj.art-81a972c7d32d4158bf6e4c65db22a7d52023-08-22T07:38:34ZengFrontiers Media S.A.Frontiers in Thermal Engineering2813-04562023-08-01310.3389/fther.2023.12398001239800Solvent recovery from solvent-fine coal slurries by filtration and steam strippingMichael Huylo0Kaiwu Huang1Aaron Noble2Roe-Hoan Yoon3Rui Qiao4Department of Mechanical Engineering, Virginia Tech, Blacksburg, VA, United StatesDepartment of Mining and Minerals Engineering, Virginia Tech, Blacksburg, VA, United StatesDepartment of Mining and Minerals Engineering, Virginia Tech, Blacksburg, VA, United StatesDepartment of Mining and Minerals Engineering, Virginia Tech, Blacksburg, VA, United StatesDepartment of Mechanical Engineering, Virginia Tech, Blacksburg, VA, United StatesDewatering of fine coal is a significant industrial challenge with economic and environmental implications. Due to the lack of suitable dewatering technologies, fine coal particles are often discarded to waste impoundments, leading to substantial loss of valuable natural resources while creating environmental problems. The hydrophobic-hydrophilic separation (HHS) process is a unique solution to this problem. In this process, a recyclable solvent is used to simultaneously remove inorganic impurities (ash) and water from a run-of-mine fine coal slurry. A small amount of recyclable oil (or solvent) is added to a fine coal slurry so that the solvent can spontaneously displace the water from the surface of coal particles. The spent solvent is subsequently recovered and recycled in a closed loop. Here, we report the results obtained using two different solvents, i.e., pentane and hexane, to de-ash and dewater ultrafine coal and recover the spent solvent by filtration, followed by steam stripping. Most of the spent solvent can be recovered during the filtration step at 20 psig N₂ and at a 60 s filtration time. The residual solvent left in the cake was then recovered using steam under different conditions. The results showed that the residual solvent concentration could be reduced to <1,400 ppm after 10 s of steam stripping at 150°C and 15 psig.https://www.frontiersin.org/articles/10.3389/fther.2023.1239800/fullcoal finesdewateringsteam strippingfiltration cakesdrying
spellingShingle Michael Huylo
Kaiwu Huang
Aaron Noble
Roe-Hoan Yoon
Rui Qiao
Solvent recovery from solvent-fine coal slurries by filtration and steam stripping
Frontiers in Thermal Engineering
coal fines
dewatering
steam stripping
filtration cakes
drying
title Solvent recovery from solvent-fine coal slurries by filtration and steam stripping
title_full Solvent recovery from solvent-fine coal slurries by filtration and steam stripping
title_fullStr Solvent recovery from solvent-fine coal slurries by filtration and steam stripping
title_full_unstemmed Solvent recovery from solvent-fine coal slurries by filtration and steam stripping
title_short Solvent recovery from solvent-fine coal slurries by filtration and steam stripping
title_sort solvent recovery from solvent fine coal slurries by filtration and steam stripping
topic coal fines
dewatering
steam stripping
filtration cakes
drying
url https://www.frontiersin.org/articles/10.3389/fther.2023.1239800/full
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AT kaiwuhuang solventrecoveryfromsolventfinecoalslurriesbyfiltrationandsteamstripping
AT aaronnoble solventrecoveryfromsolventfinecoalslurriesbyfiltrationandsteamstripping
AT roehoanyoon solventrecoveryfromsolventfinecoalslurriesbyfiltrationandsteamstripping
AT ruiqiao solventrecoveryfromsolventfinecoalslurriesbyfiltrationandsteamstripping