N′-(2-Methoxybenzylidene)nicotinohydrazide

The title compound, C14H13N3O2, was prepared by the reaction of 2-methoxybenzyaldehyde with nicotinic acid hydrazide in methanol. The dihedral angle between the benzene and pyridine rings is 5.9 (3)°. In the crystal structure, molecules are linked by intermolecular N&a...

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Main Authors: Yong-Qing Su, Cong Li, Ping Wang
Format: Article
Language:English
Published: International Union of Crystallography 2010-03-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536810003831
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author Yong-Qing Su
Cong Li
Ping Wang
author_facet Yong-Qing Su
Cong Li
Ping Wang
author_sort Yong-Qing Su
collection DOAJ
description The title compound, C14H13N3O2, was prepared by the reaction of 2-methoxybenzyaldehyde with nicotinic acid hydrazide in methanol. The dihedral angle between the benzene and pyridine rings is 5.9 (3)°. In the crystal structure, molecules are linked by intermolecular N—H...O hydrogen bonds, leading to the formation of chains along the c axis; adjacent chains are linked via C—H...O and C—H...N hydrogen bonds.
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spelling doaj.art-81f37f232e694cc29bfd8bc4dcdc127a2022-12-21T17:24:00ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682010-03-01663o542o54210.1107/S1600536810003831N′-(2-Methoxybenzylidene)nicotinohydrazideYong-Qing SuCong LiPing WangThe title compound, C14H13N3O2, was prepared by the reaction of 2-methoxybenzyaldehyde with nicotinic acid hydrazide in methanol. The dihedral angle between the benzene and pyridine rings is 5.9 (3)°. In the crystal structure, molecules are linked by intermolecular N—H...O hydrogen bonds, leading to the formation of chains along the c axis; adjacent chains are linked via C—H...O and C—H...N hydrogen bonds.http://scripts.iucr.org/cgi-bin/paper?S1600536810003831
spellingShingle Yong-Qing Su
Cong Li
Ping Wang
N′-(2-Methoxybenzylidene)nicotinohydrazide
Acta Crystallographica Section E
title N′-(2-Methoxybenzylidene)nicotinohydrazide
title_full N′-(2-Methoxybenzylidene)nicotinohydrazide
title_fullStr N′-(2-Methoxybenzylidene)nicotinohydrazide
title_full_unstemmed N′-(2-Methoxybenzylidene)nicotinohydrazide
title_short N′-(2-Methoxybenzylidene)nicotinohydrazide
title_sort n amp 8242 2 methoxybenzylidene nicotinohydrazide
url http://scripts.iucr.org/cgi-bin/paper?S1600536810003831
work_keys_str_mv AT yongqingsu namp82422methoxybenzylidenenicotinohydrazide
AT congli namp82422methoxybenzylidenenicotinohydrazide
AT pingwang namp82422methoxybenzylidenenicotinohydrazide