Additively Manufactured Detection Module with Integrated Tuning Fork for Enhanced Photo-Acoustic Spectroscopy

Starting from Quartz-Enhanced Photo-Acoustic Spectroscopy (QEPAS), we have explored the potential of a tightly linked method of gas/vapor sensing, from now on referred to as Tuning-Fork-Enhanced Photo-Acoustic Spectroscopy (TFEPAS). TFEPAS utilizes a non-piezoelectric metal or dielectric tuning fork...

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Main Authors: Roberto Viola, Nicola Liberatore, Sandro Mengali
Format: Article
Language:English
Published: MDPI AG 2022-09-01
Series:Sensors
Subjects:
Online Access:https://www.mdpi.com/1424-8220/22/19/7193
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author Roberto Viola
Nicola Liberatore
Sandro Mengali
author_facet Roberto Viola
Nicola Liberatore
Sandro Mengali
author_sort Roberto Viola
collection DOAJ
description Starting from Quartz-Enhanced Photo-Acoustic Spectroscopy (QEPAS), we have explored the potential of a tightly linked method of gas/vapor sensing, from now on referred to as Tuning-Fork-Enhanced Photo-Acoustic Spectroscopy (TFEPAS). TFEPAS utilizes a non-piezoelectric metal or dielectric tuning fork to transduce the photoacoustic excitation and an optical interferometric readout to measure the amplitude of the tuning fork vibration. In particular, we have devised a solution based on Additive Manufacturing (AM) for the Absorption Detection Module (ADM). The novelty of our solution is that the ADM is entirely built monolithically by Micro-Metal Laser Sintering (MMLS) or other AM techniques to achieve easier and more cost-effective customization, extreme miniaturization of internal volumes, automatic alignment of the tuning fork with the acoustic micro-resonators, and operation at high temperature. This paper reports on preliminary experimental results achieved with ammonia at parts-per-million concentration in nitrogen to demonstrate the feasibility of the proposed solution. Prospectively, the proposed TFEPAS solution appears particularly suited for hyphenation to micro-Gas Chromatography and for the analysis of complex solid and liquid traces samples, including compounds with low volatility such as illicit drugs, explosives, and persistent chemical warfare agents.
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spelling doaj.art-82e31aaecfd34017802c8b66afdaf05e2023-11-23T21:45:07ZengMDPI AGSensors1424-82202022-09-012219719310.3390/s22197193Additively Manufactured Detection Module with Integrated Tuning Fork for Enhanced Photo-Acoustic SpectroscopyRoberto Viola0Nicola Liberatore1Sandro Mengali2Consorzio CREO, 67100 L’Aquila, ItalyConsorzio CREO, 67100 L’Aquila, ItalyConsorzio CREO, 67100 L’Aquila, ItalyStarting from Quartz-Enhanced Photo-Acoustic Spectroscopy (QEPAS), we have explored the potential of a tightly linked method of gas/vapor sensing, from now on referred to as Tuning-Fork-Enhanced Photo-Acoustic Spectroscopy (TFEPAS). TFEPAS utilizes a non-piezoelectric metal or dielectric tuning fork to transduce the photoacoustic excitation and an optical interferometric readout to measure the amplitude of the tuning fork vibration. In particular, we have devised a solution based on Additive Manufacturing (AM) for the Absorption Detection Module (ADM). The novelty of our solution is that the ADM is entirely built monolithically by Micro-Metal Laser Sintering (MMLS) or other AM techniques to achieve easier and more cost-effective customization, extreme miniaturization of internal volumes, automatic alignment of the tuning fork with the acoustic micro-resonators, and operation at high temperature. This paper reports on preliminary experimental results achieved with ammonia at parts-per-million concentration in nitrogen to demonstrate the feasibility of the proposed solution. Prospectively, the proposed TFEPAS solution appears particularly suited for hyphenation to micro-Gas Chromatography and for the analysis of complex solid and liquid traces samples, including compounds with low volatility such as illicit drugs, explosives, and persistent chemical warfare agents.https://www.mdpi.com/1424-8220/22/19/7193gas analyzerPAStuning forkmicro additive manufacturinginterferometric readout
spellingShingle Roberto Viola
Nicola Liberatore
Sandro Mengali
Additively Manufactured Detection Module with Integrated Tuning Fork for Enhanced Photo-Acoustic Spectroscopy
Sensors
gas analyzer
PAS
tuning fork
micro additive manufacturing
interferometric readout
title Additively Manufactured Detection Module with Integrated Tuning Fork for Enhanced Photo-Acoustic Spectroscopy
title_full Additively Manufactured Detection Module with Integrated Tuning Fork for Enhanced Photo-Acoustic Spectroscopy
title_fullStr Additively Manufactured Detection Module with Integrated Tuning Fork for Enhanced Photo-Acoustic Spectroscopy
title_full_unstemmed Additively Manufactured Detection Module with Integrated Tuning Fork for Enhanced Photo-Acoustic Spectroscopy
title_short Additively Manufactured Detection Module with Integrated Tuning Fork for Enhanced Photo-Acoustic Spectroscopy
title_sort additively manufactured detection module with integrated tuning fork for enhanced photo acoustic spectroscopy
topic gas analyzer
PAS
tuning fork
micro additive manufacturing
interferometric readout
url https://www.mdpi.com/1424-8220/22/19/7193
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AT nicolaliberatore additivelymanufactureddetectionmodulewithintegratedtuningforkforenhancedphotoacousticspectroscopy
AT sandromengali additivelymanufactureddetectionmodulewithintegratedtuningforkforenhancedphotoacousticspectroscopy