Green Preparation of Durian Rind-Based Cellulose Nanofiber and Its Application in Aerogel

In this study, a green, highly efficient and low energy consumption preparation method of cellulose nanofiber (CNF) was developed by using agricultural and forestry waste durian rinds as raw materials. The power of ultrasonic treatment was successfully reduced to only 360 W with low molecular weight...

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Main Authors: Huwei Xing, Yongsheng Fei, Jingru Cheng, Congcong Wang, Jingjing Zhang, Chenxi Niu, Qian Fu, Jiali Cheng, Lingbin Lu
Format: Article
Language:English
Published: MDPI AG 2022-10-01
Series:Molecules
Subjects:
Online Access:https://www.mdpi.com/1420-3049/27/19/6507
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author Huwei Xing
Yongsheng Fei
Jingru Cheng
Congcong Wang
Jingjing Zhang
Chenxi Niu
Qian Fu
Jiali Cheng
Lingbin Lu
author_facet Huwei Xing
Yongsheng Fei
Jingru Cheng
Congcong Wang
Jingjing Zhang
Chenxi Niu
Qian Fu
Jiali Cheng
Lingbin Lu
author_sort Huwei Xing
collection DOAJ
description In this study, a green, highly efficient and low energy consumption preparation method of cellulose nanofiber (CNF) was developed by using agricultural and forestry waste durian rinds as raw materials. The power of ultrasonic treatment was successfully reduced to only 360 W with low molecular weight liquid DMSO. The obtained durian rind-based CNF had a diameter of 8–20 nm and a length of several micrometers. It had good dispersion and stability in water, and could spontaneously cross-link to form hydrogel at room temperature when the concentration was more than 0.5%. The microscopic morphology and compressive properties of CNF aerogels and composite cellulose aerogels prepared from durian rind-based CNF were evaluated. It was found that CNF could effectively prevent the volume shrinkage of aerogel, and the concentration of CNF had a significant effect on the microstructure and mechanical properties of aerogel. The CNF aerogel with 1% CNF exhibited a sheet structure braced by fibers, which had the strongest compression performance. The porosity of CNF aerogels was high to 99%. The compressive strength of the composite cellulose aerogel with durian rind-based CNF was effectively enhanced.
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spelling doaj.art-82f2c66b1bf140e5a4833e6e9ca620462023-11-23T21:12:35ZengMDPI AGMolecules1420-30492022-10-012719650710.3390/molecules27196507Green Preparation of Durian Rind-Based Cellulose Nanofiber and Its Application in AerogelHuwei Xing0Yongsheng Fei1Jingru Cheng2Congcong Wang3Jingjing Zhang4Chenxi Niu5Qian Fu6Jiali Cheng7Lingbin Lu8Special Glass Key Lab of Hainan Province, School of Materials Science and Engineering, Hainan University, Haikou 570228, ChinaSpecial Glass Key Lab of Hainan Province, School of Materials Science and Engineering, Hainan University, Haikou 570228, ChinaSpecial Glass Key Lab of Hainan Province, School of Materials Science and Engineering, Hainan University, Haikou 570228, ChinaSpecial Glass Key Lab of Hainan Province, School of Materials Science and Engineering, Hainan University, Haikou 570228, ChinaSpecial Glass Key Lab of Hainan Province, School of Materials Science and Engineering, Hainan University, Haikou 570228, ChinaSpecial Glass Key Lab of Hainan Province, School of Materials Science and Engineering, Hainan University, Haikou 570228, ChinaSpecial Glass Key Lab of Hainan Province, School of Materials Science and Engineering, Hainan University, Haikou 570228, ChinaSpecial Glass Key Lab of Hainan Province, School of Materials Science and Engineering, Hainan University, Haikou 570228, ChinaSpecial Glass Key Lab of Hainan Province, School of Materials Science and Engineering, Hainan University, Haikou 570228, ChinaIn this study, a green, highly efficient and low energy consumption preparation method of cellulose nanofiber (CNF) was developed by using agricultural and forestry waste durian rinds as raw materials. The power of ultrasonic treatment was successfully reduced to only 360 W with low molecular weight liquid DMSO. The obtained durian rind-based CNF had a diameter of 8–20 nm and a length of several micrometers. It had good dispersion and stability in water, and could spontaneously cross-link to form hydrogel at room temperature when the concentration was more than 0.5%. The microscopic morphology and compressive properties of CNF aerogels and composite cellulose aerogels prepared from durian rind-based CNF were evaluated. It was found that CNF could effectively prevent the volume shrinkage of aerogel, and the concentration of CNF had a significant effect on the microstructure and mechanical properties of aerogel. The CNF aerogel with 1% CNF exhibited a sheet structure braced by fibers, which had the strongest compression performance. The porosity of CNF aerogels was high to 99%. The compressive strength of the composite cellulose aerogel with durian rind-based CNF was effectively enhanced.https://www.mdpi.com/1420-3049/27/19/6507durian rindcellulose nanofiberdimethyl sulfoxideultrasonicaerogel
spellingShingle Huwei Xing
Yongsheng Fei
Jingru Cheng
Congcong Wang
Jingjing Zhang
Chenxi Niu
Qian Fu
Jiali Cheng
Lingbin Lu
Green Preparation of Durian Rind-Based Cellulose Nanofiber and Its Application in Aerogel
Molecules
durian rind
cellulose nanofiber
dimethyl sulfoxide
ultrasonic
aerogel
title Green Preparation of Durian Rind-Based Cellulose Nanofiber and Its Application in Aerogel
title_full Green Preparation of Durian Rind-Based Cellulose Nanofiber and Its Application in Aerogel
title_fullStr Green Preparation of Durian Rind-Based Cellulose Nanofiber and Its Application in Aerogel
title_full_unstemmed Green Preparation of Durian Rind-Based Cellulose Nanofiber and Its Application in Aerogel
title_short Green Preparation of Durian Rind-Based Cellulose Nanofiber and Its Application in Aerogel
title_sort green preparation of durian rind based cellulose nanofiber and its application in aerogel
topic durian rind
cellulose nanofiber
dimethyl sulfoxide
ultrasonic
aerogel
url https://www.mdpi.com/1420-3049/27/19/6507
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