One-Pot Facile Methodology to Synthesize Chitosan-ZnO-Graphene Oxide Hybrid Composites for Better Dye Adsorption and Antibacterial Activity

Novel chitosan–ZnO–graphene oxide hybrid composites were prepared using a one-pot chemical strategy, and their dye adsorption characteristics and antibacterial activity were demonstrated. The prepared chitosan and the hybrids such as chitosan–ZnO and chitosan–ZnO–graphene oxide were characterized by...

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Main Authors: Anandhavelu Sanmugam, Dhanasekaran Vikraman, Hui Joon Park, Hyun-Seok Kim
Format: Article
Language:English
Published: MDPI AG 2017-11-01
Series:Nanomaterials
Subjects:
Online Access:https://www.mdpi.com/2079-4991/7/11/363
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author Anandhavelu Sanmugam
Dhanasekaran Vikraman
Hui Joon Park
Hyun-Seok Kim
author_facet Anandhavelu Sanmugam
Dhanasekaran Vikraman
Hui Joon Park
Hyun-Seok Kim
author_sort Anandhavelu Sanmugam
collection DOAJ
description Novel chitosan–ZnO–graphene oxide hybrid composites were prepared using a one-pot chemical strategy, and their dye adsorption characteristics and antibacterial activity were demonstrated. The prepared chitosan and the hybrids such as chitosan–ZnO and chitosan–ZnO–graphene oxide were characterized by UV-Vis absorption spectroscopy, X-ray diffraction, Fourier transform infrared spectroscopy, scanning electron microscopy, and transmission electron microscopy. The thermal and mechanical properties indicate a significant improvement over chitosan in the hybrid composites. Dye adsorption experiments were carried out using methylene blue and chromium complex as model pollutants with the function of dye concentration. The antibacterial properties of chitosan and the hybrids were tested against Gram-positive and Gram-negative bacterial species, which revealed minimum inhibitory concentrations (MICs) of 0.1 µg/mL.
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spelling doaj.art-831c71e2075b47979e13694c104bd3412022-12-21T19:10:52ZengMDPI AGNanomaterials2079-49912017-11-0171136310.3390/nano7110363nano7110363One-Pot Facile Methodology to Synthesize Chitosan-ZnO-Graphene Oxide Hybrid Composites for Better Dye Adsorption and Antibacterial ActivityAnandhavelu Sanmugam0Dhanasekaran Vikraman1Hui Joon Park2Hyun-Seok Kim3Department of Chemistry (S&H), Vel Tech Multitech Dr.Rangarajan Dr.Sakunthala Engineering College, Chennai 600062, IndiaDivision of Electronics and Electrical Engineering, Dongguk University-Seoul, Seoul 04620, KoreaDepartment of Electrical and Computer Engineering, Ajou University, Suwon 16499, KoreaDivision of Electronics and Electrical Engineering, Dongguk University-Seoul, Seoul 04620, KoreaNovel chitosan–ZnO–graphene oxide hybrid composites were prepared using a one-pot chemical strategy, and their dye adsorption characteristics and antibacterial activity were demonstrated. The prepared chitosan and the hybrids such as chitosan–ZnO and chitosan–ZnO–graphene oxide were characterized by UV-Vis absorption spectroscopy, X-ray diffraction, Fourier transform infrared spectroscopy, scanning electron microscopy, and transmission electron microscopy. The thermal and mechanical properties indicate a significant improvement over chitosan in the hybrid composites. Dye adsorption experiments were carried out using methylene blue and chromium complex as model pollutants with the function of dye concentration. The antibacterial properties of chitosan and the hybrids were tested against Gram-positive and Gram-negative bacterial species, which revealed minimum inhibitory concentrations (MICs) of 0.1 µg/mL.https://www.mdpi.com/2079-4991/7/11/363nano hybrid compositesFTIRchitosandye adsorptionTEMantibacterial activity
spellingShingle Anandhavelu Sanmugam
Dhanasekaran Vikraman
Hui Joon Park
Hyun-Seok Kim
One-Pot Facile Methodology to Synthesize Chitosan-ZnO-Graphene Oxide Hybrid Composites for Better Dye Adsorption and Antibacterial Activity
Nanomaterials
nano hybrid composites
FTIR
chitosan
dye adsorption
TEM
antibacterial activity
title One-Pot Facile Methodology to Synthesize Chitosan-ZnO-Graphene Oxide Hybrid Composites for Better Dye Adsorption and Antibacterial Activity
title_full One-Pot Facile Methodology to Synthesize Chitosan-ZnO-Graphene Oxide Hybrid Composites for Better Dye Adsorption and Antibacterial Activity
title_fullStr One-Pot Facile Methodology to Synthesize Chitosan-ZnO-Graphene Oxide Hybrid Composites for Better Dye Adsorption and Antibacterial Activity
title_full_unstemmed One-Pot Facile Methodology to Synthesize Chitosan-ZnO-Graphene Oxide Hybrid Composites for Better Dye Adsorption and Antibacterial Activity
title_short One-Pot Facile Methodology to Synthesize Chitosan-ZnO-Graphene Oxide Hybrid Composites for Better Dye Adsorption and Antibacterial Activity
title_sort one pot facile methodology to synthesize chitosan zno graphene oxide hybrid composites for better dye adsorption and antibacterial activity
topic nano hybrid composites
FTIR
chitosan
dye adsorption
TEM
antibacterial activity
url https://www.mdpi.com/2079-4991/7/11/363
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