Miniaturized Photo-Ionization Fourier Deconvolution Ion Mobility Spectrometer for the Detection of Volatile Organic Compounds

Because of its simplicity, reliability, and sensitivity, the drift tube ion mobility spectrometer (IMS) has been recognized as the equipment of choice for the on-site monitoring and identification of volatile organic compounds (VOCs). However, the performance of handheld IMS is often limited by the...

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Main Authors: Binwang Yang, Jianna Yu, Wen Liu, Guoxing Jing, Wenshan Li, Wenjie Liu
Format: Article
Language:English
Published: MDPI AG 2022-07-01
Series:Sensors
Subjects:
Online Access:https://www.mdpi.com/1424-8220/22/15/5468
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author Binwang Yang
Jianna Yu
Wen Liu
Guoxing Jing
Wenshan Li
Wenjie Liu
author_facet Binwang Yang
Jianna Yu
Wen Liu
Guoxing Jing
Wenshan Li
Wenjie Liu
author_sort Binwang Yang
collection DOAJ
description Because of its simplicity, reliability, and sensitivity, the drift tube ion mobility spectrometer (IMS) has been recognized as the equipment of choice for the on-site monitoring and identification of volatile organic compounds (VOCs). However, the performance of handheld IMS is often limited by the size, weight, and drift voltage, which heavily determine the sensitivity and resolving power that is crucial for the detection and identification of VOCs. In this work, we present a low-cost, miniaturized drift tube ion mobility spectrometer incorporated with a miniaturized UV ionization lamp and a relatively low drift voltage. The sensitivity and resolving power are boosted with the implementation of Fourier deconvolution multiplexing compared to the conventional signal averaging data acquisition method. The drift tube provides a high resolving power of up to 52 at a drift length of 41 mm, 10 mm ID dimensions, and a drift voltage of 1.57 kV. Acetone, benzene, dimethyl methyl phosphonate, methyl salicylate, and acetic acid were evaluated in the developed spectrometer and showed satisfactory performance.
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spelling doaj.art-835822367b89447dbecf6c8149575ca32023-12-03T12:59:29ZengMDPI AGSensors1424-82202022-07-012215546810.3390/s22155468Miniaturized Photo-Ionization Fourier Deconvolution Ion Mobility Spectrometer for the Detection of Volatile Organic CompoundsBinwang Yang0Jianna Yu1Wen Liu2Guoxing Jing3Wenshan Li4Wenjie Liu5College of Chemical Engineering, Xiangtan University, Xiangtan 411105, ChinaCollege of Chemical Engineering, Xiangtan University, Xiangtan 411105, ChinaCollege of Chemical Engineering, Xiangtan University, Xiangtan 411105, ChinaCollege of Chemical Engineering, Xiangtan University, Xiangtan 411105, ChinaCollege of Chemical Engineering, Xiangtan University, Xiangtan 411105, ChinaCollege of Chemical Engineering, Xiangtan University, Xiangtan 411105, ChinaBecause of its simplicity, reliability, and sensitivity, the drift tube ion mobility spectrometer (IMS) has been recognized as the equipment of choice for the on-site monitoring and identification of volatile organic compounds (VOCs). However, the performance of handheld IMS is often limited by the size, weight, and drift voltage, which heavily determine the sensitivity and resolving power that is crucial for the detection and identification of VOCs. In this work, we present a low-cost, miniaturized drift tube ion mobility spectrometer incorporated with a miniaturized UV ionization lamp and a relatively low drift voltage. The sensitivity and resolving power are boosted with the implementation of Fourier deconvolution multiplexing compared to the conventional signal averaging data acquisition method. The drift tube provides a high resolving power of up to 52 at a drift length of 41 mm, 10 mm ID dimensions, and a drift voltage of 1.57 kV. Acetone, benzene, dimethyl methyl phosphonate, methyl salicylate, and acetic acid were evaluated in the developed spectrometer and showed satisfactory performance.https://www.mdpi.com/1424-8220/22/15/5468multiplexingFourier deconvolutionminiaturized drift tubephotoionizationion mobility spectrometer
spellingShingle Binwang Yang
Jianna Yu
Wen Liu
Guoxing Jing
Wenshan Li
Wenjie Liu
Miniaturized Photo-Ionization Fourier Deconvolution Ion Mobility Spectrometer for the Detection of Volatile Organic Compounds
Sensors
multiplexing
Fourier deconvolution
miniaturized drift tube
photoionization
ion mobility spectrometer
title Miniaturized Photo-Ionization Fourier Deconvolution Ion Mobility Spectrometer for the Detection of Volatile Organic Compounds
title_full Miniaturized Photo-Ionization Fourier Deconvolution Ion Mobility Spectrometer for the Detection of Volatile Organic Compounds
title_fullStr Miniaturized Photo-Ionization Fourier Deconvolution Ion Mobility Spectrometer for the Detection of Volatile Organic Compounds
title_full_unstemmed Miniaturized Photo-Ionization Fourier Deconvolution Ion Mobility Spectrometer for the Detection of Volatile Organic Compounds
title_short Miniaturized Photo-Ionization Fourier Deconvolution Ion Mobility Spectrometer for the Detection of Volatile Organic Compounds
title_sort miniaturized photo ionization fourier deconvolution ion mobility spectrometer for the detection of volatile organic compounds
topic multiplexing
Fourier deconvolution
miniaturized drift tube
photoionization
ion mobility spectrometer
url https://www.mdpi.com/1424-8220/22/15/5468
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