Assessment of the feasibility of determining the volume fraction and characteristics of the size, shape and distribution of γ’ phase precipitates in nickel-based superalloys

This overview presents a comprehensive exploration of the research methods employed for the precise assessment of volume fraction and the detailed characterisation of the size, shape and distribution of γ’ phase precipitates within Ni-based superalloys. These advanced materials exhibit exceptional m...

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Main Author: Szczotok Agnieszka
Format: Article
Language:English
Published: Sciendo 2023-01-01
Series:Technical Transactions
Subjects:
Online Access:https://doi.org/10.37705/TechTrans/e2023011
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author Szczotok Agnieszka
author_facet Szczotok Agnieszka
author_sort Szczotok Agnieszka
collection DOAJ
description This overview presents a comprehensive exploration of the research methods employed for the precise assessment of volume fraction and the detailed characterisation of the size, shape and distribution of γ’ phase precipitates within Ni-based superalloys. These advanced materials exhibit exceptional mechanical properties due to the presence of γ’ precipitates. The accurate quantification of precipitate parameters is crucial for understanding material behaviour and for the optimisation of alloy design. In this overview, a spectrum of techniques, including microscopy (SEM, TEM), diffraction (XRD), spectroscopy (EDS, EELS) and advanced imaging (3D-APT, STEM-HAADF, FIB-SEM) is discussed. Strengths, limitations and potential synergies among these methods are highlighted, offering researchers a comprehensive toolbox to advance their investigations of γ’ phase precipitates in Ni-based superalloys.
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spelling doaj.art-838a9e611a2c4acb90aa4b4496f93a212024-01-02T11:36:23ZengSciendoTechnical Transactions2353-737X2023-01-01120110.37705/TechTrans/e2023011Assessment of the feasibility of determining the volume fraction and characteristics of the size, shape and distribution of γ’ phase precipitates in nickel-based superalloysSzczotok Agnieszka01Silesian University of Technology, Faculty of Materials Engineering, Department of Materials Technology, Katowice, PolandThis overview presents a comprehensive exploration of the research methods employed for the precise assessment of volume fraction and the detailed characterisation of the size, shape and distribution of γ’ phase precipitates within Ni-based superalloys. These advanced materials exhibit exceptional mechanical properties due to the presence of γ’ precipitates. The accurate quantification of precipitate parameters is crucial for understanding material behaviour and for the optimisation of alloy design. In this overview, a spectrum of techniques, including microscopy (SEM, TEM), diffraction (XRD), spectroscopy (EDS, EELS) and advanced imaging (3D-APT, STEM-HAADF, FIB-SEM) is discussed. Strengths, limitations and potential synergies among these methods are highlighted, offering researchers a comprehensive toolbox to advance their investigations of γ’ phase precipitates in Ni-based superalloys.https://doi.org/10.37705/TechTrans/e2023011volume fractionsizeshapedistributionγ’ phase precipitatesni-based superalloysresearch methods
spellingShingle Szczotok Agnieszka
Assessment of the feasibility of determining the volume fraction and characteristics of the size, shape and distribution of γ’ phase precipitates in nickel-based superalloys
Technical Transactions
volume fraction
size
shape
distribution
γ’ phase precipitates
ni-based superalloys
research methods
title Assessment of the feasibility of determining the volume fraction and characteristics of the size, shape and distribution of γ’ phase precipitates in nickel-based superalloys
title_full Assessment of the feasibility of determining the volume fraction and characteristics of the size, shape and distribution of γ’ phase precipitates in nickel-based superalloys
title_fullStr Assessment of the feasibility of determining the volume fraction and characteristics of the size, shape and distribution of γ’ phase precipitates in nickel-based superalloys
title_full_unstemmed Assessment of the feasibility of determining the volume fraction and characteristics of the size, shape and distribution of γ’ phase precipitates in nickel-based superalloys
title_short Assessment of the feasibility of determining the volume fraction and characteristics of the size, shape and distribution of γ’ phase precipitates in nickel-based superalloys
title_sort assessment of the feasibility of determining the volume fraction and characteristics of the size shape and distribution of γ phase precipitates in nickel based superalloys
topic volume fraction
size
shape
distribution
γ’ phase precipitates
ni-based superalloys
research methods
url https://doi.org/10.37705/TechTrans/e2023011
work_keys_str_mv AT szczotokagnieszka assessmentofthefeasibilityofdeterminingthevolumefractionandcharacteristicsofthesizeshapeanddistributionofgphaseprecipitatesinnickelbasedsuperalloys