Reheating of zinc-titanate sintered specimens

The scope of this work was observing dimensional and heat transfer changes in ZnTiO3 samples during heating in nitrogen and air atmosphere. Interactions of bulk specimens with gaseous surrounding induce microstructure changes during heating. Sintered ZnTiO3 nanopowder samples were submitted...

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Main Authors: Labus N., Mentus S., Rakić S., Đurić Z.Z., Vujančević J., Nikolić M.V.
Format: Article
Language:English
Published: International Institute for the Science of Sintering, Beograd 2015-01-01
Series:Science of Sintering
Subjects:
Online Access:http://www.doiserbia.nb.rs/img/doi/0350-820X/2015/0350-820X1501071L.pdf
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author Labus N.
Mentus S.
Rakić S.
Đurić Z.Z.
Vujančević J.
Nikolić M.V.
author_facet Labus N.
Mentus S.
Rakić S.
Đurić Z.Z.
Vujančević J.
Nikolić M.V.
author_sort Labus N.
collection DOAJ
description The scope of this work was observing dimensional and heat transfer changes in ZnTiO3 samples during heating in nitrogen and air atmosphere. Interactions of bulk specimens with gaseous surrounding induce microstructure changes during heating. Sintered ZnTiO3 nanopowder samples were submitted to subsequent heating. Dilatation curves and thermogravimetric with simultaneous differential thermal analysis TGA/DTA curves were recorded. Reheating was performed in air and nitrogen atmospheres. Reheated samples obtained at different characteristic temperatures in air were analyzed by X-ray diffraction (XRD). Microstructures obtained by scanning electron microscopy (SEM) of reheated sintered samples are presented and compared. Reheating in a different atmosphere induced different microstructures. The goal was indicating possible causes leading to the microstructure changes. [Projekat Ministarstva nauke Republike Srbije, br. OI172057 i br. III45014]
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spelling doaj.art-844dbf62f2dd45389de20086ee7cc6ef2022-12-22T00:31:35ZengInternational Institute for the Science of Sintering, BeogradScience of Sintering0350-820X1820-74132015-01-01471718110.2298/SOS1501071L0350-820X1501071LReheating of zinc-titanate sintered specimensLabus N.0Mentus S.1Rakić S.2Đurić Z.Z.3Vujančević J.4Nikolić M.V.5Institute of Technical Sciences of SASA, BeogradFaculty of Physical Chemistry, Belgrade + Serbian Academy of Sciences and Arts, BelgradeFaculty of Natural Sciences, Institute of Physics, Novi SadInstitute of Technical Sciences of SASA, BeogradInstitute of Technical Sciences of SASA, BeogradInstitute for Multidisciplinary Research, BeogradThe scope of this work was observing dimensional and heat transfer changes in ZnTiO3 samples during heating in nitrogen and air atmosphere. Interactions of bulk specimens with gaseous surrounding induce microstructure changes during heating. Sintered ZnTiO3 nanopowder samples were submitted to subsequent heating. Dilatation curves and thermogravimetric with simultaneous differential thermal analysis TGA/DTA curves were recorded. Reheating was performed in air and nitrogen atmospheres. Reheated samples obtained at different characteristic temperatures in air were analyzed by X-ray diffraction (XRD). Microstructures obtained by scanning electron microscopy (SEM) of reheated sintered samples are presented and compared. Reheating in a different atmosphere induced different microstructures. The goal was indicating possible causes leading to the microstructure changes. [Projekat Ministarstva nauke Republike Srbije, br. OI172057 i br. III45014]http://www.doiserbia.nb.rs/img/doi/0350-820X/2015/0350-820X1501071L.pdfdilatometrysintering
spellingShingle Labus N.
Mentus S.
Rakić S.
Đurić Z.Z.
Vujančević J.
Nikolić M.V.
Reheating of zinc-titanate sintered specimens
Science of Sintering
dilatometry
sintering
title Reheating of zinc-titanate sintered specimens
title_full Reheating of zinc-titanate sintered specimens
title_fullStr Reheating of zinc-titanate sintered specimens
title_full_unstemmed Reheating of zinc-titanate sintered specimens
title_short Reheating of zinc-titanate sintered specimens
title_sort reheating of zinc titanate sintered specimens
topic dilatometry
sintering
url http://www.doiserbia.nb.rs/img/doi/0350-820X/2015/0350-820X1501071L.pdf
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AT rakics reheatingofzinctitanatesinteredspecimens
AT đuriczz reheatingofzinctitanatesinteredspecimens
AT vujancevicj reheatingofzinctitanatesinteredspecimens
AT nikolicmv reheatingofzinctitanatesinteredspecimens