Farm-Scale Estimation of Total Nitrogen Content in Surface Paddy Soils by Extraction with Commercially Available Hydrogen Peroxide

We recently proposed a simple method for estimating total nitrogen content in paddy soil. In this method, soil is extracted with a commercial 3% hydrogen peroxide (H<sub>2</sub>O<sub>2</sub>) solution at 25 &#176;C for 40 h, and electrical conductivity (EC (H<sub>2&...

Full description

Bibliographic Details
Main Authors: Naoki Moritsuka, Hiroki Saito, Ryosuke Tajima, Yukitsugu Takahashi, Hideaki Hirai
Format: Article
Language:English
Published: MDPI AG 2019-12-01
Series:Agronomy
Subjects:
Online Access:https://www.mdpi.com/2073-4395/10/1/40
_version_ 1818426767015149568
author Naoki Moritsuka
Hiroki Saito
Ryosuke Tajima
Yukitsugu Takahashi
Hideaki Hirai
author_facet Naoki Moritsuka
Hiroki Saito
Ryosuke Tajima
Yukitsugu Takahashi
Hideaki Hirai
author_sort Naoki Moritsuka
collection DOAJ
description We recently proposed a simple method for estimating total nitrogen content in paddy soil. In this method, soil is extracted with a commercial 3% hydrogen peroxide (H<sub>2</sub>O<sub>2</sub>) solution at 25 &#176;C for 40 h, and electrical conductivity (EC (H<sub>2</sub>O<sub>2</sub>)) of the extract is measured. This study aimed to further evaluate the method&#8217;s applicability to soil samples collected at the farm scale by using the original and six additional H<sub>2</sub>O<sub>2</sub> solutions that are locally and commercially available. The results obtained with the original solution indicated that the determination coefficients between EC (H<sub>2</sub>O<sub>2</sub>) and total N were statistically significant at all farms examined: Moka, 0.78 (<i>n</i> = 13); Kyoto, 0.50 (<i>n</i> = 16); Kizu, 0.43 (<i>n</i> = 89); and Kawatabi, 0.25 (<i>n</i> = 18). The EC of the tested H<sub>2</sub>O<sub>2</sub> solutions varied from less than 0.05 to 1.4 mS cm<sup>&#8722;1</sup> because of the addition of different stabilizers. EC (H<sub>2</sub>O<sub>2</sub>) values obtained with the less stabilized H<sub>2</sub>O<sub>2</sub> solutions (one from Japan, one from USA, and the analytical grade 6% solution) agreed well with those obtained with the original solution. Thus, the proposed method can be useful for estimating the farm-scale variation in soil total N, provided a H<sub>2</sub>O<sub>2</sub> solution with a low EC (&lt;0.2 mS cm<sup>&#8722;1</sup>) is used for the extraction.
first_indexed 2024-12-14T14:35:03Z
format Article
id doaj.art-84d54fb52e254720a2f6236b2289e126
institution Directory Open Access Journal
issn 2073-4395
language English
last_indexed 2024-12-14T14:35:03Z
publishDate 2019-12-01
publisher MDPI AG
record_format Article
series Agronomy
spelling doaj.art-84d54fb52e254720a2f6236b2289e1262022-12-21T22:57:40ZengMDPI AGAgronomy2073-43952019-12-011014010.3390/agronomy10010040agronomy10010040Farm-Scale Estimation of Total Nitrogen Content in Surface Paddy Soils by Extraction with Commercially Available Hydrogen PeroxideNaoki Moritsuka0Hiroki Saito1Ryosuke Tajima2Yukitsugu Takahashi3Hideaki Hirai4Graduate School of Agriculture, Kyoto University, Kyoto 606-8502, JapanTropical Agriculture Research Front, Japan International Research Center for Agricultural Sciences, Okinawa 907-0002, JapanField Science Center, Tohoku University, Miyagi 989-6711, JapanUniversity Farm, Utsunomiya University, Tochigi 321-4415, JapanSchool of Agriculture, Utsunomiya University, Tochigi 321-8505, JapanWe recently proposed a simple method for estimating total nitrogen content in paddy soil. In this method, soil is extracted with a commercial 3% hydrogen peroxide (H<sub>2</sub>O<sub>2</sub>) solution at 25 &#176;C for 40 h, and electrical conductivity (EC (H<sub>2</sub>O<sub>2</sub>)) of the extract is measured. This study aimed to further evaluate the method&#8217;s applicability to soil samples collected at the farm scale by using the original and six additional H<sub>2</sub>O<sub>2</sub> solutions that are locally and commercially available. The results obtained with the original solution indicated that the determination coefficients between EC (H<sub>2</sub>O<sub>2</sub>) and total N were statistically significant at all farms examined: Moka, 0.78 (<i>n</i> = 13); Kyoto, 0.50 (<i>n</i> = 16); Kizu, 0.43 (<i>n</i> = 89); and Kawatabi, 0.25 (<i>n</i> = 18). The EC of the tested H<sub>2</sub>O<sub>2</sub> solutions varied from less than 0.05 to 1.4 mS cm<sup>&#8722;1</sup> because of the addition of different stabilizers. EC (H<sub>2</sub>O<sub>2</sub>) values obtained with the less stabilized H<sub>2</sub>O<sub>2</sub> solutions (one from Japan, one from USA, and the analytical grade 6% solution) agreed well with those obtained with the original solution. Thus, the proposed method can be useful for estimating the farm-scale variation in soil total N, provided a H<sub>2</sub>O<sub>2</sub> solution with a low EC (&lt;0.2 mS cm<sup>&#8722;1</sup>) is used for the extraction.https://www.mdpi.com/2073-4395/10/1/40electrical conductivityfarm-scale variationhydrogen peroxidenitrogenpaddy soilsimple method
spellingShingle Naoki Moritsuka
Hiroki Saito
Ryosuke Tajima
Yukitsugu Takahashi
Hideaki Hirai
Farm-Scale Estimation of Total Nitrogen Content in Surface Paddy Soils by Extraction with Commercially Available Hydrogen Peroxide
Agronomy
electrical conductivity
farm-scale variation
hydrogen peroxide
nitrogen
paddy soil
simple method
title Farm-Scale Estimation of Total Nitrogen Content in Surface Paddy Soils by Extraction with Commercially Available Hydrogen Peroxide
title_full Farm-Scale Estimation of Total Nitrogen Content in Surface Paddy Soils by Extraction with Commercially Available Hydrogen Peroxide
title_fullStr Farm-Scale Estimation of Total Nitrogen Content in Surface Paddy Soils by Extraction with Commercially Available Hydrogen Peroxide
title_full_unstemmed Farm-Scale Estimation of Total Nitrogen Content in Surface Paddy Soils by Extraction with Commercially Available Hydrogen Peroxide
title_short Farm-Scale Estimation of Total Nitrogen Content in Surface Paddy Soils by Extraction with Commercially Available Hydrogen Peroxide
title_sort farm scale estimation of total nitrogen content in surface paddy soils by extraction with commercially available hydrogen peroxide
topic electrical conductivity
farm-scale variation
hydrogen peroxide
nitrogen
paddy soil
simple method
url https://www.mdpi.com/2073-4395/10/1/40
work_keys_str_mv AT naokimoritsuka farmscaleestimationoftotalnitrogencontentinsurfacepaddysoilsbyextractionwithcommerciallyavailablehydrogenperoxide
AT hirokisaito farmscaleestimationoftotalnitrogencontentinsurfacepaddysoilsbyextractionwithcommerciallyavailablehydrogenperoxide
AT ryosuketajima farmscaleestimationoftotalnitrogencontentinsurfacepaddysoilsbyextractionwithcommerciallyavailablehydrogenperoxide
AT yukitsugutakahashi farmscaleestimationoftotalnitrogencontentinsurfacepaddysoilsbyextractionwithcommerciallyavailablehydrogenperoxide
AT hideakihirai farmscaleestimationoftotalnitrogencontentinsurfacepaddysoilsbyextractionwithcommerciallyavailablehydrogenperoxide