Control of colloidal CaCO3 suspension by using biodegradable polymers during fabrication
Fabrication of homogenous CaCO3 particles is a significant step in assembling polyelectrolyte capsules. It is crucial to control the dimensions, the shape and the charge of the calcium carbonate particles in order to have homogenously separated and charged templates as final result. For this reason,...
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Format: | Article |
Language: | English |
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SpringerOpen
2015-03-01
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Series: | Beni-Suef University Journal of Basic and Applied Sciences |
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Online Access: | http://www.sciencedirect.com/science/article/pii/S2314853515000104 |
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author | Nemany Abdelhamid Nemany Hanafy Maria Luisa De Giorgi Concetta Nobile Ross Rinaldi Stefano Leporatti |
author_facet | Nemany Abdelhamid Nemany Hanafy Maria Luisa De Giorgi Concetta Nobile Ross Rinaldi Stefano Leporatti |
author_sort | Nemany Abdelhamid Nemany Hanafy |
collection | DOAJ |
description | Fabrication of homogenous CaCO3 particles is a significant step in assembling polyelectrolyte capsules. It is crucial to control the dimensions, the shape and the charge of the calcium carbonate particles in order to have homogenously separated and charged templates as final result. For this reason, previously. hey have been deeply investigated.
Recently, crystallization of CaCO3 was done by adding poly (sodium 4-styrenesulfonate) (PSS) as negatively charged polymer and poly (allylamine hydrochloride) (PAH) as positively charged polymer and the results were surprising. The homogenous particles were separated and they carried the same charge of the used polymer.
The aim of this work was to investigate the synthesis process of CaCO3 particles in different experimental conditions: calcium carbonate was produced in presence and in absence of water and with addition of appropriate polymers. In particular, chitosan (CHI) and poly acrylic acid (PAA) were chosen as biodegradable polymers whereas PSS and PAH were chosen as non-biodegradable polymers. Shape and diameter of particles were investigated by using transmission and scanning electron microscopy, elemental composition was inferred by energy dispersive X-ray analyses whereas their charges were explored by using zeta potential. |
first_indexed | 2024-12-20T02:50:41Z |
format | Article |
id | doaj.art-862856519b3c40769066864b0d2909dd |
institution | Directory Open Access Journal |
issn | 2314-8535 |
language | English |
last_indexed | 2024-12-20T02:50:41Z |
publishDate | 2015-03-01 |
publisher | SpringerOpen |
record_format | Article |
series | Beni-Suef University Journal of Basic and Applied Sciences |
spelling | doaj.art-862856519b3c40769066864b0d2909dd2022-12-21T19:56:02ZengSpringerOpenBeni-Suef University Journal of Basic and Applied Sciences2314-85352015-03-0141607010.1016/j.bjbas.2015.02.009Control of colloidal CaCO3 suspension by using biodegradable polymers during fabricationNemany Abdelhamid Nemany Hanafy0Maria Luisa De Giorgi1Concetta Nobile2Ross Rinaldi3Stefano Leporatti4NNL-Istituto Nanoscienze, CNR Via Arnesano 16, 73100 Lecce, ItalyDepartment of Mathematics and Physics “E. De Giorgi”, University of Salento, Via Monteroni, 73100 Lecce ItalyNNL-Istituto Nanoscienze, CNR Via Arnesano 16, 73100 Lecce, ItalyNNL-Istituto Nanoscienze, CNR Via Arnesano 16, 73100 Lecce, ItalyNNL-Istituto Nanoscienze, CNR Via Arnesano 16, 73100 Lecce, ItalyFabrication of homogenous CaCO3 particles is a significant step in assembling polyelectrolyte capsules. It is crucial to control the dimensions, the shape and the charge of the calcium carbonate particles in order to have homogenously separated and charged templates as final result. For this reason, previously. hey have been deeply investigated. Recently, crystallization of CaCO3 was done by adding poly (sodium 4-styrenesulfonate) (PSS) as negatively charged polymer and poly (allylamine hydrochloride) (PAH) as positively charged polymer and the results were surprising. The homogenous particles were separated and they carried the same charge of the used polymer. The aim of this work was to investigate the synthesis process of CaCO3 particles in different experimental conditions: calcium carbonate was produced in presence and in absence of water and with addition of appropriate polymers. In particular, chitosan (CHI) and poly acrylic acid (PAA) were chosen as biodegradable polymers whereas PSS and PAH were chosen as non-biodegradable polymers. Shape and diameter of particles were investigated by using transmission and scanning electron microscopy, elemental composition was inferred by energy dispersive X-ray analyses whereas their charges were explored by using zeta potential.http://www.sciencedirect.com/science/article/pii/S2314853515000104Calcium carbonatePoly (sodium 4-styrenesulfonate) (PSS)Poly (allylamine hydrochloride) (PAH)Chitosan (CHI)Poly acrylic acid (PAA)Biodegradable polymersNot biodegradable polymers |
spellingShingle | Nemany Abdelhamid Nemany Hanafy Maria Luisa De Giorgi Concetta Nobile Ross Rinaldi Stefano Leporatti Control of colloidal CaCO3 suspension by using biodegradable polymers during fabrication Beni-Suef University Journal of Basic and Applied Sciences Calcium carbonate Poly (sodium 4-styrenesulfonate) (PSS) Poly (allylamine hydrochloride) (PAH) Chitosan (CHI) Poly acrylic acid (PAA) Biodegradable polymers Not biodegradable polymers |
title | Control of colloidal CaCO3 suspension by using biodegradable polymers during fabrication |
title_full | Control of colloidal CaCO3 suspension by using biodegradable polymers during fabrication |
title_fullStr | Control of colloidal CaCO3 suspension by using biodegradable polymers during fabrication |
title_full_unstemmed | Control of colloidal CaCO3 suspension by using biodegradable polymers during fabrication |
title_short | Control of colloidal CaCO3 suspension by using biodegradable polymers during fabrication |
title_sort | control of colloidal caco3 suspension by using biodegradable polymers during fabrication |
topic | Calcium carbonate Poly (sodium 4-styrenesulfonate) (PSS) Poly (allylamine hydrochloride) (PAH) Chitosan (CHI) Poly acrylic acid (PAA) Biodegradable polymers Not biodegradable polymers |
url | http://www.sciencedirect.com/science/article/pii/S2314853515000104 |
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