Control of colloidal CaCO3 suspension by using biodegradable polymers during fabrication

Fabrication of homogenous CaCO3 particles is a significant step in assembling polyelectrolyte capsules. It is crucial to control the dimensions, the shape and the charge of the calcium carbonate particles in order to have homogenously separated and charged templates as final result. For this reason,...

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Main Authors: Nemany Abdelhamid Nemany Hanafy, Maria Luisa De Giorgi, Concetta Nobile, Ross Rinaldi, Stefano Leporatti
Format: Article
Language:English
Published: SpringerOpen 2015-03-01
Series:Beni-Suef University Journal of Basic and Applied Sciences
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2314853515000104
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author Nemany Abdelhamid Nemany Hanafy
Maria Luisa De Giorgi
Concetta Nobile
Ross Rinaldi
Stefano Leporatti
author_facet Nemany Abdelhamid Nemany Hanafy
Maria Luisa De Giorgi
Concetta Nobile
Ross Rinaldi
Stefano Leporatti
author_sort Nemany Abdelhamid Nemany Hanafy
collection DOAJ
description Fabrication of homogenous CaCO3 particles is a significant step in assembling polyelectrolyte capsules. It is crucial to control the dimensions, the shape and the charge of the calcium carbonate particles in order to have homogenously separated and charged templates as final result. For this reason, previously. hey have been deeply investigated. Recently, crystallization of CaCO3 was done by adding poly (sodium 4-styrenesulfonate) (PSS) as negatively charged polymer and poly (allylamine hydrochloride) (PAH) as positively charged polymer and the results were surprising. The homogenous particles were separated and they carried the same charge of the used polymer. The aim of this work was to investigate the synthesis process of CaCO3 particles in different experimental conditions: calcium carbonate was produced in presence and in absence of water and with addition of appropriate polymers. In particular, chitosan (CHI) and poly acrylic acid (PAA) were chosen as biodegradable polymers whereas PSS and PAH were chosen as non-biodegradable polymers. Shape and diameter of particles were investigated by using transmission and scanning electron microscopy, elemental composition was inferred by energy dispersive X-ray analyses whereas their charges were explored by using zeta potential.
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spelling doaj.art-862856519b3c40769066864b0d2909dd2022-12-21T19:56:02ZengSpringerOpenBeni-Suef University Journal of Basic and Applied Sciences2314-85352015-03-0141607010.1016/j.bjbas.2015.02.009Control of colloidal CaCO3 suspension by using biodegradable polymers during fabricationNemany Abdelhamid Nemany Hanafy0Maria Luisa De Giorgi1Concetta Nobile2Ross Rinaldi3Stefano Leporatti4NNL-Istituto Nanoscienze, CNR Via Arnesano 16, 73100 Lecce, ItalyDepartment of Mathematics and Physics “E. De Giorgi”, University of Salento, Via Monteroni, 73100 Lecce ItalyNNL-Istituto Nanoscienze, CNR Via Arnesano 16, 73100 Lecce, ItalyNNL-Istituto Nanoscienze, CNR Via Arnesano 16, 73100 Lecce, ItalyNNL-Istituto Nanoscienze, CNR Via Arnesano 16, 73100 Lecce, ItalyFabrication of homogenous CaCO3 particles is a significant step in assembling polyelectrolyte capsules. It is crucial to control the dimensions, the shape and the charge of the calcium carbonate particles in order to have homogenously separated and charged templates as final result. For this reason, previously. hey have been deeply investigated. Recently, crystallization of CaCO3 was done by adding poly (sodium 4-styrenesulfonate) (PSS) as negatively charged polymer and poly (allylamine hydrochloride) (PAH) as positively charged polymer and the results were surprising. The homogenous particles were separated and they carried the same charge of the used polymer. The aim of this work was to investigate the synthesis process of CaCO3 particles in different experimental conditions: calcium carbonate was produced in presence and in absence of water and with addition of appropriate polymers. In particular, chitosan (CHI) and poly acrylic acid (PAA) were chosen as biodegradable polymers whereas PSS and PAH were chosen as non-biodegradable polymers. Shape and diameter of particles were investigated by using transmission and scanning electron microscopy, elemental composition was inferred by energy dispersive X-ray analyses whereas their charges were explored by using zeta potential.http://www.sciencedirect.com/science/article/pii/S2314853515000104Calcium carbonatePoly (sodium 4-styrenesulfonate) (PSS)Poly (allylamine hydrochloride) (PAH)Chitosan (CHI)Poly acrylic acid (PAA)Biodegradable polymersNot biodegradable polymers
spellingShingle Nemany Abdelhamid Nemany Hanafy
Maria Luisa De Giorgi
Concetta Nobile
Ross Rinaldi
Stefano Leporatti
Control of colloidal CaCO3 suspension by using biodegradable polymers during fabrication
Beni-Suef University Journal of Basic and Applied Sciences
Calcium carbonate
Poly (sodium 4-styrenesulfonate) (PSS)
Poly (allylamine hydrochloride) (PAH)
Chitosan (CHI)
Poly acrylic acid (PAA)
Biodegradable polymers
Not biodegradable polymers
title Control of colloidal CaCO3 suspension by using biodegradable polymers during fabrication
title_full Control of colloidal CaCO3 suspension by using biodegradable polymers during fabrication
title_fullStr Control of colloidal CaCO3 suspension by using biodegradable polymers during fabrication
title_full_unstemmed Control of colloidal CaCO3 suspension by using biodegradable polymers during fabrication
title_short Control of colloidal CaCO3 suspension by using biodegradable polymers during fabrication
title_sort control of colloidal caco3 suspension by using biodegradable polymers during fabrication
topic Calcium carbonate
Poly (sodium 4-styrenesulfonate) (PSS)
Poly (allylamine hydrochloride) (PAH)
Chitosan (CHI)
Poly acrylic acid (PAA)
Biodegradable polymers
Not biodegradable polymers
url http://www.sciencedirect.com/science/article/pii/S2314853515000104
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AT marialuisadegiorgi controlofcolloidalcaco3suspensionbyusingbiodegradablepolymersduringfabrication
AT concettanobile controlofcolloidalcaco3suspensionbyusingbiodegradablepolymersduringfabrication
AT rossrinaldi controlofcolloidalcaco3suspensionbyusingbiodegradablepolymersduringfabrication
AT stefanoleporatti controlofcolloidalcaco3suspensionbyusingbiodegradablepolymersduringfabrication