Research on Hydrothermal Decoration of TiO2 Nanotube Films with Nanoplatelet MoS2 Species
In this study, novel electrodes were prepared via decoration of nanotubed TiO2 (TiNT) films with crystalline two- dimensional (2D) MoS2 species by a one-step hydrothermal synthesis approach. Obtained products were characterized in detail by scanning electron microscopy, Raman spectro‐ scopy, U-I mea...
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Format: | Article |
Language: | English |
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Hindawi - SAGE Publishing
2016-06-01
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Series: | Nanomaterials and Nanotechnology |
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Online Access: | http://www.intechopen.com/journals/nanomaterials_and_nanotechnology/research-on-hydrothermal-decoration-of-tio2-nanotube-films-with-nanoplatelet-mos2-species |
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author | Jelena Kovger Arnas Naujokaitis Gediminas Niaura Jurga Juodkazyte Gintaras Valušis Arūnas Jagminas |
author_facet | Jelena Kovger Arnas Naujokaitis Gediminas Niaura Jurga Juodkazyte Gintaras Valušis Arūnas Jagminas |
author_sort | Jelena Kovger |
collection | DOAJ |
description | In this study, novel electrodes were prepared via decoration of nanotubed TiO2 (TiNT) films with crystalline two- dimensional (2D) MoS2 species by a one-step hydrothermal synthesis approach. Obtained products were characterized in detail by scanning electron microscopy, Raman spectro‐ scopy, U-I measurements and X-ray diffraction techniques. The influence of hydrothermal synthesis conditions on the composition and morphology of the products formed in the solution and within the TiNT film are also discussed. For the first time, acceptable decoration of TiNT films, by tethering 2D layered MoS2 leaflets onto the TiO2 nanotubes, and on the film surface was obtained in the low concentra‐ tion solutions, while the performance of these heterostruc‐ tures in relation to electrochemical hydrogen evolution reaction (HER) was tested. Stable catalytic activity of the obtained 2D MoS2-in-TiNT films was demonstrated under intense HER conditions within the potential window [-0.2 to - 0.4 V] vs. RHE with a notably low Tafel slope of 33 mV/ decade. |
first_indexed | 2024-03-09T09:13:58Z |
format | Article |
id | doaj.art-868332915c3a4c438fb3b28e95371348 |
institution | Directory Open Access Journal |
issn | 1847-9804 |
language | English |
last_indexed | 2024-03-09T09:13:58Z |
publishDate | 2016-06-01 |
publisher | Hindawi - SAGE Publishing |
record_format | Article |
series | Nanomaterials and Nanotechnology |
spelling | doaj.art-868332915c3a4c438fb3b28e953713482023-12-02T07:44:30ZengHindawi - SAGE PublishingNanomaterials and Nanotechnology1847-98042016-06-01637http://dx.doi.org/10.5772/6409451095Research on Hydrothermal Decoration of TiO2 Nanotube Films with Nanoplatelet MoS2 SpeciesJelena KovgerArnas NaujokaitisGediminas NiauraJurga JuodkazyteGintaras ValušisArūnas JagminasIn this study, novel electrodes were prepared via decoration of nanotubed TiO2 (TiNT) films with crystalline two- dimensional (2D) MoS2 species by a one-step hydrothermal synthesis approach. Obtained products were characterized in detail by scanning electron microscopy, Raman spectro‐ scopy, U-I measurements and X-ray diffraction techniques. The influence of hydrothermal synthesis conditions on the composition and morphology of the products formed in the solution and within the TiNT film are also discussed. For the first time, acceptable decoration of TiNT films, by tethering 2D layered MoS2 leaflets onto the TiO2 nanotubes, and on the film surface was obtained in the low concentra‐ tion solutions, while the performance of these heterostruc‐ tures in relation to electrochemical hydrogen evolution reaction (HER) was tested. Stable catalytic activity of the obtained 2D MoS2-in-TiNT films was demonstrated under intense HER conditions within the potential window [-0.2 to - 0.4 V] vs. RHE with a notably low Tafel slope of 33 mV/ decade.http://www.intechopen.com/journals/nanomaterials_and_nanotechnology/research-on-hydrothermal-decoration-of-tio2-nanotube-films-with-nanoplatelet-mos2-speciesNanoplatelet MoS2Hydrothermal SynthesisTitania Nanotube FilmHydrogen Evolution |
spellingShingle | Jelena Kovger Arnas Naujokaitis Gediminas Niaura Jurga Juodkazyte Gintaras Valušis Arūnas Jagminas Research on Hydrothermal Decoration of TiO2 Nanotube Films with Nanoplatelet MoS2 Species Nanomaterials and Nanotechnology Nanoplatelet MoS2 Hydrothermal Synthesis Titania Nanotube Film Hydrogen Evolution |
title | Research on Hydrothermal Decoration of TiO2 Nanotube Films with Nanoplatelet MoS2 Species |
title_full | Research on Hydrothermal Decoration of TiO2 Nanotube Films with Nanoplatelet MoS2 Species |
title_fullStr | Research on Hydrothermal Decoration of TiO2 Nanotube Films with Nanoplatelet MoS2 Species |
title_full_unstemmed | Research on Hydrothermal Decoration of TiO2 Nanotube Films with Nanoplatelet MoS2 Species |
title_short | Research on Hydrothermal Decoration of TiO2 Nanotube Films with Nanoplatelet MoS2 Species |
title_sort | research on hydrothermal decoration of tio2 nanotube films with nanoplatelet mos2 species |
topic | Nanoplatelet MoS2 Hydrothermal Synthesis Titania Nanotube Film Hydrogen Evolution |
url | http://www.intechopen.com/journals/nanomaterials_and_nanotechnology/research-on-hydrothermal-decoration-of-tio2-nanotube-films-with-nanoplatelet-mos2-species |
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