New Compounds from the Roots of Corsican <i>Calicotome Villosa</i> (Poir.) Link.: Two Pterocarpans and a Dihydrobenzofuran
Three new compounds, a dihydrobenzofuran (coumaran) derivative (compound <b>1</b>) and two pterocarpans (compounds <b>2</b> and <b>3</b>) were isolated from a root extract of <i>Calicotome villosa</i> growing wild in Corsica. Their structures were eluc...
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MDPI AG
2020-07-01
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author | Doreen Stacy Palu Mathieu Paoli Hervé Casabianca Joseph Casanova Ange Bighelli |
author_facet | Doreen Stacy Palu Mathieu Paoli Hervé Casabianca Joseph Casanova Ange Bighelli |
author_sort | Doreen Stacy Palu |
collection | DOAJ |
description | Three new compounds, a dihydrobenzofuran (coumaran) derivative (compound <b>1</b>) and two pterocarpans (compounds <b>2</b> and <b>3</b>) were isolated from a root extract of <i>Calicotome villosa</i> growing wild in Corsica. Their structures were elucidated using 1D and 2D NMR spectroscopy and MS/MS as 2-(1-methylethenyl)-5-hydroxy-6-carbomethoxy-2,3-dihydro-benzofuran, 4,9-dihydroxy-3-methoxy-2-dimethylallylpterocarpan, and 4,9-dihydroxy-3′,3′-dimethyl-2,3-pyranopterocarpan. |
first_indexed | 2024-03-10T18:06:16Z |
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id | doaj.art-8688bb2a622d4b8495a9d5ecd1e13214 |
institution | Directory Open Access Journal |
issn | 1420-3049 |
language | English |
last_indexed | 2024-03-10T18:06:16Z |
publishDate | 2020-07-01 |
publisher | MDPI AG |
record_format | Article |
series | Molecules |
spelling | doaj.art-8688bb2a622d4b8495a9d5ecd1e132142023-11-20T08:29:39ZengMDPI AGMolecules1420-30492020-07-012515346710.3390/molecules25153467New Compounds from the Roots of Corsican <i>Calicotome Villosa</i> (Poir.) Link.: Two Pterocarpans and a DihydrobenzofuranDoreen Stacy Palu0Mathieu Paoli1Hervé Casabianca2Joseph Casanova3Ange Bighelli4Department of Chemistry, Equipe Chimie-Biomasse, Université de Corse-CNRS, UMR 6134 SPE, Route des Sanguinaires, F- 20000 Ajaccio, FranceDepartment of Chemistry, Equipe Chimie-Biomasse, Université de Corse-CNRS, UMR 6134 SPE, Route des Sanguinaires, F- 20000 Ajaccio, FranceInstitut des Sciences Analytiques, Université de Lyon, CNRS, Université Claude Bernard Lyon 1, UMR 5280, 5 rue de la Doua, F-69100 Villeurbanne, FranceDepartment of Chemistry, Equipe Chimie-Biomasse, Université de Corse-CNRS, UMR 6134 SPE, Route des Sanguinaires, F- 20000 Ajaccio, FranceDepartment of Chemistry, Equipe Chimie-Biomasse, Université de Corse-CNRS, UMR 6134 SPE, Route des Sanguinaires, F- 20000 Ajaccio, FranceThree new compounds, a dihydrobenzofuran (coumaran) derivative (compound <b>1</b>) and two pterocarpans (compounds <b>2</b> and <b>3</b>) were isolated from a root extract of <i>Calicotome villosa</i> growing wild in Corsica. Their structures were elucidated using 1D and 2D NMR spectroscopy and MS/MS as 2-(1-methylethenyl)-5-hydroxy-6-carbomethoxy-2,3-dihydro-benzofuran, 4,9-dihydroxy-3-methoxy-2-dimethylallylpterocarpan, and 4,9-dihydroxy-3′,3′-dimethyl-2,3-pyranopterocarpan.https://www.mdpi.com/1420-3049/25/15/3467<i>Calicotome villosa</i>root extractpterocarpandihydrobenzofuran1D and 2D NMR |
spellingShingle | Doreen Stacy Palu Mathieu Paoli Hervé Casabianca Joseph Casanova Ange Bighelli New Compounds from the Roots of Corsican <i>Calicotome Villosa</i> (Poir.) Link.: Two Pterocarpans and a Dihydrobenzofuran Molecules <i>Calicotome villosa</i> root extract pterocarpan dihydrobenzofuran 1D and 2D NMR |
title | New Compounds from the Roots of Corsican <i>Calicotome Villosa</i> (Poir.) Link.: Two Pterocarpans and a Dihydrobenzofuran |
title_full | New Compounds from the Roots of Corsican <i>Calicotome Villosa</i> (Poir.) Link.: Two Pterocarpans and a Dihydrobenzofuran |
title_fullStr | New Compounds from the Roots of Corsican <i>Calicotome Villosa</i> (Poir.) Link.: Two Pterocarpans and a Dihydrobenzofuran |
title_full_unstemmed | New Compounds from the Roots of Corsican <i>Calicotome Villosa</i> (Poir.) Link.: Two Pterocarpans and a Dihydrobenzofuran |
title_short | New Compounds from the Roots of Corsican <i>Calicotome Villosa</i> (Poir.) Link.: Two Pterocarpans and a Dihydrobenzofuran |
title_sort | new compounds from the roots of corsican i calicotome villosa i poir link two pterocarpans and a dihydrobenzofuran |
topic | <i>Calicotome villosa</i> root extract pterocarpan dihydrobenzofuran 1D and 2D NMR |
url | https://www.mdpi.com/1420-3049/25/15/3467 |
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