Influence of curing protocols on water sorption and solubility of a self-adhesive resin-cement

Aim: To evaluate the effect of different activation protocols on the polymerization of a self-adhesive dual cured resin-based cement. Methods: Thirty disc-shaped specimens were prepared with the resin cement RelyX U200 (3M ESPE) and divided according to three protocols: immediate light-activation fo...

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Main Authors: Dilcele Silva Moreira Dziedzic, João Paulo Stanislovicz Prohny, Gledson Luiz Picharski, Adilson Yoshio Furuse
Format: Article
Language:English
Published: Universidade Estadual de Campinas 2017-04-01
Series:Brazilian Journal of Oral Sciences
Subjects:
Online Access:https://periodicos.sbu.unicamp.br/ojs/index.php/bjos/article/view/8648766
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author Dilcele Silva Moreira Dziedzic
João Paulo Stanislovicz Prohny
Gledson Luiz Picharski
Adilson Yoshio Furuse
author_facet Dilcele Silva Moreira Dziedzic
João Paulo Stanislovicz Prohny
Gledson Luiz Picharski
Adilson Yoshio Furuse
author_sort Dilcele Silva Moreira Dziedzic
collection DOAJ
description Aim: To evaluate the effect of different activation protocols on the polymerization of a self-adhesive dual cured resin-based cement. Methods: Thirty disc-shaped specimens were prepared with the resin cement RelyX U200 (3M ESPE) and divided according to three protocols: immediate light-activation for 40 s, delayed light-activation (10 min after manipulation, for 40 s) or self-curing without light-activation. The specimens were desiccated, kept in water at 37 °C for 7 days and desiccated again to calculate water sorption, solubility and mass variation. Data were analyzed by Shapiro-Wilk Test and Wilcoxon tests (α=0.05). Images after the specimens’ final desiccation were also made. Results: The Wilcoxon test revealed a significant difference for sorption and mass variation (p<0.05) and the highest value was observed in self-curing or chemical activation group (CA), followed by delayed light-activation (DL) and immediate light-activation (IL). Besides the water sorption parameters, there were also microvoids on the discs from the delayed and no light-activation groups. Conclusions: The light-activation immediately after manipulation is recommended for the evaluated resin cement.
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spelling doaj.art-86a1b446a75f456c9c023dd833cdd78c2022-12-21T20:19:01ZengUniversidade Estadual de CampinasBrazilian Journal of Oral Sciences1677-32252017-04-0115210.20396/bjos.v15i2.8648766Influence of curing protocols on water sorption and solubility of a self-adhesive resin-cementDilcele Silva Moreira Dziedzic0João Paulo Stanislovicz Prohny1Gledson Luiz Picharski2Adilson Yoshio Furuse3Universidade PositivoUniversidade Federal do Rio Grande do SulUniversidade Federal do ParanáUniversidade de São PauloAim: To evaluate the effect of different activation protocols on the polymerization of a self-adhesive dual cured resin-based cement. Methods: Thirty disc-shaped specimens were prepared with the resin cement RelyX U200 (3M ESPE) and divided according to three protocols: immediate light-activation for 40 s, delayed light-activation (10 min after manipulation, for 40 s) or self-curing without light-activation. The specimens were desiccated, kept in water at 37 °C for 7 days and desiccated again to calculate water sorption, solubility and mass variation. Data were analyzed by Shapiro-Wilk Test and Wilcoxon tests (α=0.05). Images after the specimens’ final desiccation were also made. Results: The Wilcoxon test revealed a significant difference for sorption and mass variation (p<0.05) and the highest value was observed in self-curing or chemical activation group (CA), followed by delayed light-activation (DL) and immediate light-activation (IL). Besides the water sorption parameters, there were also microvoids on the discs from the delayed and no light-activation groups. Conclusions: The light-activation immediately after manipulation is recommended for the evaluated resin cement.https://periodicos.sbu.unicamp.br/ojs/index.php/bjos/article/view/8648766Resin cements. Solubility. Polymerization.
spellingShingle Dilcele Silva Moreira Dziedzic
João Paulo Stanislovicz Prohny
Gledson Luiz Picharski
Adilson Yoshio Furuse
Influence of curing protocols on water sorption and solubility of a self-adhesive resin-cement
Brazilian Journal of Oral Sciences
Resin cements. Solubility. Polymerization.
title Influence of curing protocols on water sorption and solubility of a self-adhesive resin-cement
title_full Influence of curing protocols on water sorption and solubility of a self-adhesive resin-cement
title_fullStr Influence of curing protocols on water sorption and solubility of a self-adhesive resin-cement
title_full_unstemmed Influence of curing protocols on water sorption and solubility of a self-adhesive resin-cement
title_short Influence of curing protocols on water sorption and solubility of a self-adhesive resin-cement
title_sort influence of curing protocols on water sorption and solubility of a self adhesive resin cement
topic Resin cements. Solubility. Polymerization.
url https://periodicos.sbu.unicamp.br/ojs/index.php/bjos/article/view/8648766
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AT gledsonluizpicharski influenceofcuringprotocolsonwatersorptionandsolubilityofaselfadhesiveresincement
AT adilsonyoshiofuruse influenceofcuringprotocolsonwatersorptionandsolubilityofaselfadhesiveresincement